钛酸酯催化环氧树脂固化动力学研究

用FTIR“原位”技术,研究了钛酸酯(Tc-114)偶联剂对环氧E-44和二氨基二苯基甲烷(DDM)固化反应的催化作用,得出固化程度与时间的关系曲线。又根据DSC曲线,分别算出加有Tc-114和不加Tc-114的两个固化体系的反应表观活化能和反应级数。结果表明,Tc-114的存在使环氧固化反应活化能降低,催化作用明显。     

Silicon doped carbon/Cu joints based on amorphous alloy brazing for first wall application

Amorphous ribbon-type filler-metals represent a promising selection for joining heterogeneous materials together. In this work, rapidly solidified ribbon-type Ti based amorphous filler with a melting temperature of 850 °C and a thickness up to 20 μm is used to join silicon doped carbon to pure copper. SEM examinations demonstrate that a high quality brazed joints could be acquired. The brazed seam has a uniform structure and pore free along its entire length. TiC and ZrC are formed near the interface of carbon and filler-metal when the brazing holds enough time. Using very thin Mo and Cu foil (0.2 mm in thickness) as multiple interlayer are very effective to mitigate the thermal stress occurred in the interface between carbon and copper. The shear strength of this carbon-multiple interlayer-copper joint is more than 20 MPa, and the rupture is mainly occurred on the carbon side.     

热能表中计算器非线性修正方法探讨

本文针对目前热能表中大量存在的计算器准确度较低的问题,提出了使用高次曲线拟合的非线性修正方法,提高了准确度.     

心得安新用10种

心得安的“学名”叫普萘洛尔，是β受体阻滞剂类的代表药物，临床应用已经有几十年的历史，常用来治疗心律失常、高血压、冠心病等。经临床实践，不断发现它有很多其他用途。[编者按]     

异丁醛氧化制丙酮热导气相色谱分析

本工作用２米４０１有机担体填充柱，在带四臂热导检测器的国产１０３型气相色谱仪上，仅８分钟将原料异丁醛、产物丙酮及水进行良好分离，并采用内标法定量，其最大平均偏差在±２％以内。方法简单、快速、准确     

双能X射线骨密度仪测定技术研究

以Ｌｕｎａｒ公司ＤＰＸ－Ｌ型双能Ｘ射线骨密度仪为例，研究引起测量误差的主要因素并提出质控措施。用自检模块、腰椎体膜评定仪器的体外测量精度好于１％。对１０位志愿者重复２次测量，体内精度对腰椎，ＭＰＤ（平均百分差）为０．４６，ＣＶ（变异系数）为０．７５；对股骨颈，ＭＰＤ为１．２６、ＣＶ为０．４７；Ｗａｒｄ’ｓ三角区ＭＰＤ为２．０１、ＣＶ为１．１４；大转子ＭＰＤ为１．６６、ＣＶ为０．７２。扫描图像由２位     

催化氧化法合成脂肪醇醚羧酸盐的研究进展

详细介绍了氮氧自由基催化氧化法和贵金属催化氧化法合成脂肪醇醚羧酸盐。氮氧自由基催化时,反应温度20～60℃,反应时间3～6 h,得到酸型产品。贵金属催化剂中,钯的催化活性比铂高。贵金属催化时,加入铅、铋等助催化剂,并以活性炭为载体,碱性条件下于50～90℃反应2～6 h,得到盐型产品。在适当的条件下,这两种方法均可使醇醚转化率达95％,选择性达90％以上。     

WiMax: The Emergence of Wireless Broadband

WiMax has changed the scene of wireless broadband from proprietary solutions to a standards-based industry. Authors discuss WiMax evolution, applications, spectrum issues, standards, and developments.     

一种测定深部岩体地应力的新方法——钻孔局部壁面应力全解除法

简要回顾了基于钻孔进行地应力测量的几种方法，并指出了这些方法自身存在的局限性。提出了一种测定深部岩体地应力的新方法-钻孔局部壁面应力全解除法。该方法的明显优点是，不需要套钻，而且在确定地应力的主值及其方向时也不需要作任何假定。从理论上讲，该方法将不受测量深度的限制，对于深钻孔是普遍适用的，这将为大陆科学钻探计划中深部岩体地应力测量提供一种新途径。     

Nonregular feedback linearization: a nonsmooth approach

In this note, we address the problem of exact linearization via nonsmooth nonregular feedback. A criterion of nonregular static state feedback linearizability is presented for a class of nonlinear affine systems with two control inputs, and its application to nonholonomic systems is briefly discussed.