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滴定分析法测定铜的改进 总被引:1,自引:0,他引:1
提出在NH4HF2介质中,有SCNˉ存在下,以Iˉ3—淀粉为指示剂,硫代硫酸钠滴定铜的分析方法 相似文献
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8-Hydroxyqunioline end-capped polystyrene was prepared through atom transfer free radical polymerization (ATRP) with 8-(5-chloromethyl) quinolyl acetate as initiator. The results indicated that this polymerization is a first order reaction with respect to monomer conversion. The molecular weight increased linearly with monomer consumption and very narrow distribution of molecular weight was obtained (polydispersity index less than 1.2). The FT-IR and NMR results show that the 8-hydroxyquinloine group was chemically bonded to the polymer end and there is nearly one 8-hydroxyquinoline group in per polymer chain. All those data show that polymerization of styrene at such conditions displayed living characters. The polymer with 8-hydroxyqquinoline end group reacted with triethylaluminum to form polymeric light-emitting complex and single layer LED was prepared by common spin-coating method. The peak wavelength of LED based on synthesized polymeric complex was around 570 nm. 相似文献
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Polypyrrole (PPY) and PPY/SBA‐15 host–guest composite materials have been prepared using chemical synthesis route and characterized by XRD, IR, N2 adsorption–desorption isotherms, and SEM. The humidity sensitive properties (HSP) of this kind of materials have been studied by analyzing the variation curve of impedance as a function of relative humidity. It was found that the PPY/SBA‐15 host–guest composites materials exhibit better HSP than that of the corresponding pure PPY. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3301–3305, 2006 相似文献
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Social networks often demonstrate a hierarchical organization, with communities embedded within other communities; moreover, nodes can be shared between different communities, i.e. communities in social networks may be overlapping. In this paper, we define a hierarchical overlapping community structure to present overlapping communities of a social network at different levels of granularity. Discovering the hierarchical overlapping community structure of a social network can provide us a deeper understanding of the complex nature of social networks. We propose an algorithm, called D-HOCS, to derive the hierarchical overlapping community structure of social networks. Firstly, D-HOCS generates a probability transition matrix by applying random walk to a social network, and then trains a Gaussian Mixture Model using the matrix. Further D-HOCS derives overlapping communities by analyzing mean vectors of the Gaussian mixture model. Varying the number of components, D-HOCS repeatedly trains the Gaussian mixture model, detecting the overlapping communities at different levels of granularity. Organizing the overlapping communities into a hierarchy, D-HOCS can finally obtain the hierarchical overlapping community structure of the social network. The experiments conducted on synthetic and real dataset demonstrate the feasibility and applicability of the proposed algorithm. We further employ D-HOCS to explore Enron e-mail corpus, and obtain several interesting insights. For example, we find out a coordinator who coordinated many sections of the Enron Corporation to complete an important task during first half of 2001. We also identify a community that corresponds to a real organization in Enron Corporation. 相似文献
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CacO3在PP和PP/mPE共混物基体中的作用比较 总被引:2,自引:0,他引:2
研究CaCO3填料在取丙烯(PP)和茂金属聚乙烯(mPE)弹性体增韧PP共混物(PP/mPE)2种基体中的不同作用。结果表明:在PP基体中,填料显著提高其刚性,而在共混物基体中,由于弹性体的存在,填料的增强作用减弱;弹性体能够改善填料粒子和基体的界面粘合,增大弹性体分散相的尺寸,使PP/mPE共混物的拉伸断裂韧性提高。低温下(-30℃)的Charpy缺口冲击实验表明:少量的CaCO3即可导致PP/mPE体系冲击强度的迅速下降。 相似文献
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