高功率双工旋转场移相器

旋转场移相器具有移相精度高(均方根误差可小于1°)和温度稳定性好等特点,通过改进射频传输结构,可大大提高他的功率容量。利用旋转场移相器的互易特性和铁氧体圆极化器的非互易特性,设计出高功率双工旋转场移相器。其双工特性可将收/发信号分开,实现移相器和环行器的双重功能,用于天线的收发通道等场合时,可省去一个高功率环行器,结构紧凑。分析了双工旋转场移相器的工作原理,阐述了高功率应用下的设计方法,推导出了管状铁氧体的相移量计算公式,按此方法设计了实用的器件,并给出了试验数据。     

放射性核素迁移的实验室研究——Ⅱ.用混合裂变产物溶液研究核素在地质材料上的吸附

应用裂变产物混合物做为示踪剂研究了~(137)Cs,~(141,144)Ce,~(103,106)Ru,~(103,106)Ru,~(95)Zr,~(95)Nb,~(89,90)Sr在花岗岩、凝灰岩、页岩上的吸附行为。应用批式技术测定了吸附比。核素的γ放射性是用连有SCORPIO-3000多道计算机系统的Ce(Li)探测器测量的。β放射性~(89,90)Sr是放化分离后在G-M计数器上测量的。结果表明:凝灰岩、页岩能强烈吸附Ce,Nb,Zr;吸附Cs居中;吸附Sr,Ru较差;花岗岩的吸附性能都差。     

TEM method for rapid and precise evaluation of continuous recrystallization

With the aid of a double-tilt holder in a transmission electron microscope, a new method for a rapid and precise determination of the misorientations of a large number of subgrain or grain boundaries is given in this article. By use of the method, the continuous recrystallization can be rapidly and precisely evaluated when compared to the other conventional methods.     

CdSe量子点的制备与荧光特性研究

主要讨论了CdSe量子点的制备及荧光特性。CdSe量子点由化学方法制备，通过选择不同的反应时间得到不同尺度的量子点样品。用荧光方法研究了量子点样品在石英衬底和有机溶剂中的荧光特性。实验表明，这些量子点都有良好的荧光特性。还用无限深球方势阱模型分析了量子点样品的电子态，并根据荧光参数估算了量子点的尺度．各样品荧光峰具有一致的半峰宽，表明CdSe量子点的成核过程在反应开始时同时完成。     

与商业比肩而行

“许多美术行为都是与商业客户相结合的。以商业的视角看待作品更重视在整个概念部分是不是能够从设计的观点很忠实地传达出商业诉求，并引起更大共鸣”。[编者按]     

Effect of polymerization conditions on o‐phenylenediamine and o‐phenetidine oxidative copolymers

A series of new o‐phenylenediamine (OPD)/o‐phenetidine (PHT) copolymers with partly phenazine‐like structures has been successfully synthesized at three polymerization temperatures by chemically oxidative polymerization in four different polymerization media. The molecular structures and properties of the resulting OPD/PHT polymers were investigated by IR, UV–vis and high‐resolution ¹H NMR spectroscopies, and DSC, in order to ascertain the effect of reaction temperature, comonomer ratio and acid medium. The copolymerization mechanism of OPD with PHT monomers has been proposed. It is found that the statistical OPD/PHT copolymer obtained at a temperature of 118 °C has a higher degree of polymerization than that obtained at 12–17 °C. The OPD content in the copolymers calculated from NMR spectroscopic analysis is higher than that in the feed OPD content, whereas the OPD content calculated from element analysis is slightly lower than the feed OPD content. It can be predicted that denitrogenation takes place in the OPD units during the polymerization process at OPD/PHT molar ratios of 90/10 and 100/0. These OPD/PHT copolymers exhibit a much better solubility than the OPD homopolymer, hence suggesting an incorporation of PHT units into the phenazine structure of the homopolymer. The thermal behavior of the copolymers was also studied. Copyright © 2004 Society of Chemical Industry     

俄气南供与天然气利用规划

介绍了俄气南供的供气方案，讨论了天然气的市场调查和价格的确定等问题。     

饲料机械的干油集中润滑系统

针对饲料机械采用人工加脂润滑存在的弊端,研究了自动集中润滑系统的工作原理及技术方案,提出了干油泵和压力表等关键部件的结构设计方法.应用性能考核表明,该干油集中润滑系统能满足60～100个润滑点的需求,干油泵的输出压力及输油脂量均达到设计标准.该系统工作稳定,性能可靠,达到了满意的应用效果.