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991.
992.
Xiaoliu Li Xinhao Yan Zhiwei Li Hua Chen Pingzhu Zhang 《Frontiers of Chemical Engineering in China》2010,4(3):342-347
The catalysis of montmorillonite K10 (MK10) for aryl O-glycosylation of glycosyl trichloroacetimidates was investigated. It was found that the catalyst MK10 is deactivated gradually in the recycle glycosylation. The fresh and the deactivated catalysts were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Thermogravimetric analysis (TGA), and N2 adsorption-desorption. The results show that the eliminated trichloroacetamide molecule deposits on the MK10, which blocks and poisons the active sites, resulting in the deactivation of the catalyst. The regeneration of the deactivated MK10 by calcination was studied preliminarily. 相似文献
993.
外过滤系统具有一定优点,它可以弥补内过滤系统不足。研制了大纳污容量、大流量的外循环过滤装置。 相似文献
994.
Lian Guo 《Electrochimica acta》2010,55(28):8416-8421
The nucleation potential for the deposition of copper on ruthenium oxide is very small and hence island growth can occur in the kinetic regime. Previously, we have reported on island growth in sulfate solution where anion adsorption results in the formation of hexagonal, disk-shaped islands. Here we report on island growth in perchlorate solution, in the absence of specific anion adsorption. All islands have a 〈1 1 1〉 surface orientation dictated by the amorphous substrate. The islands are hemispherical in shape and island growth follows power law kinetics in both lateral and vertical directions with exponents 0.50 and 0.26, respectively. From analysis of the time-dependent extended area using Avrami analysis, analysis of the near-neighbor distribution, and the correlation between the island size and the spatial distribution, we conclude that island growth is controlled by surface diffusion-mediated lateral growth. 相似文献
995.
996.
997.
通过铁离子还原法、DPPH自由基清除法、羟基自由基清除法、ABTS自由基清除法来探索阿魏酸的体外抗氧化活性;采用试探性试验与牛津杯法、琼脂培养基稀释法和液体培养法分别测定青麦麸阿魏酸对部分食品腐败菌的敏感性、最小抑菌浓度和最小杀菌浓度.试验结果表明,随着阿魏酸的质量浓度升高,其铁离子还原能力逐渐增大;随着摩尔浓度升高,其对DPPH自由基、羟基自由基和ABTS自由基清除能力逐渐增大.同时,阿魏酸对大肠杆菌、金黄色葡萄球菌和枯草芽孢杆菌有抑制效果,随着阿魏酸浓度的提升,其相对应的抑制作用逐渐增强,最低抑菌浓度分别为12.5 mg/mL、6.25 mg/mL、6.25 mg/mL,最低杀菌浓度分别为200 mg/mL、>400 mg/mL、200 mg/mL. 相似文献
998.
Huayou Si Zhong Chen Yong Deng Lian Yu 《Service Oriented Computing and Applications》2013,7(3):169-180
Semantic web services (SWS) technology is developed to overcome the shortcomings of traditional standards, such as WSDL and UDDI, and enable maximal automation in all aspects of web service. But great improvement of capability in SWS-based service discovery is still desired. To address this issue, we present a distributed and semantic-matching-based approach for SWS publication and discovery by leveraging structured P2P technology. In this paper, first, we present our service matching rule which focuses on the inputs and outputs of SWS. Then, to realize this rule in open distributed environment and achieve the optimal match between a query and its qualified services, we propose not only a concept of ordered-concept-tree (OCT) to semantically sort the relevant concepts for service matching, but also a method to publish ontologies on structured P2P network to freely share and make full use of the concepts defined in different ontologies for OCT construction. Finally, we present a method for SWS publication on P2P network and an algorithm for service discovery. We also conduct experiments to evaluate our approach and the experimental results demonstrate its scalability, effectiveness, and callback capability to discover semantic web services. 相似文献
999.
Jian-Xin Zhao Lian Yang Zhen-Nan Gu Hai-Qin Chen Feng-Wei Tian Yong-Quan Chen Hao Zhang Wei Chen 《International journal of molecular sciences》2011,12(1):1-11
The interdomain instability of single-chain fragment variable (scFv) might result in intermolecular aggregation and loss of function. In the present study, we stabilized H4—an anti-aflatoxin B1 (AFB1) scFv—with an interdomain disulfide bond and studied the effect of the disulfide bond on antibody affinity. With homology modeling and molecular docking, we designed a scFv containing an interdomain disulfide bond between the residues H44 and L100. The stability of scFv (H4) increased from a GdnHCl50 of 2.4 M to 4.2 M after addition of the H44-L100 disulfide bond. Size exclusion chromatography revealed that the scFv (H44-L100) mutant existed primarily as a monomer, and no aggregates were detected. An affinity assay indicated that scFv (H4) and the scFv (H44-L100) mutant had similar IC50 values and affinity to AFB1. Our results indicate that interdomain disulfide bonds could stabilize scFv without affecting affinity. 相似文献
1000.
A modified ultrasound-assisted extraction (MUAE) method and an HPLC technique were developed to identify and quantify simultaneously the amount of oleanolic acid (OA) and ursolic acid (UA) in Scutellaria barbata D. Don. The optimal conditions for MUAE were observed when the particle size was 0.2–0.5 mm, the duty cycle was 75%, the extraction temperature was 55°C, the ratio of solvent to raw material was 12.0:1 (mL:g), the ethanol concentration was 60%, and the extraction time was 25 min. Compared to the traditional extraction method, MUAE reduced the extraction time, extraction temperature, and solvent consumption and achieved superior yields of OA and UA. Furthermore, the combined MUAE-HPLC method was successfully applied for the first time to investigate and compare the amounts of OA and UA in samples obtained from different geographical regions. 相似文献