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LU Xili WU Ye CAI Wei TANG Wenjun 《武汉理工大学学报(材料科学英文版)》2005,20(B12):287-289
A series of random and block poly( L-lactide-co-e-caprolactone ) ( PCLA ) copolymers whh different composition are prepared using stannous octaoate as catalyst.The effects of the amount of initiator on the intrinsic viscosity have been investigated. The structure of the PCLA copolymers is characterized by means of nuclear magnetic resonance( NMR ), Fourier transform infrared spectrum ( FTIR ), differential scanning calorimetry ( DSC ) and X- ray diffraction ( XRD ) methods. It is shown that the synthesis condition and the composition of copolymers obrious influence on the structure of PCLA copolymers. Hydrolytic degradation of the copolymers in a PBS solution of pH 7.4 at 37.0℃ shows that the copolymers of different composhions degrade at different rates. 相似文献
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The composition of the Co-Cr-Mo alloy has been modified by additions of nickel and some trace elements aluminium, titanium and boron. In this paper, the first part of the present study, the effects of alloy additions on the microstructures and tensile properties of the as-cast Co-Cr-Mo alloy are discussed. The effects of alloy additions on the fatigue behaviour of the alloy will be discussed in the second part of the present study. It is found that alloy additions do not seem to result in changes in the nature of the casting structure. A directional, coarse dendritic cast structure is produced in the modified alloys as in the base alloY. However, the alloy additions affect the carbide precipitations and the formation of some fine details of the microstructure such as dislocations, stacking faults and twins produced during the solidification. A considerable improvement in the transient mechanical properties, especially in the tensile ductility, is achieved by modifying the base alloy with alloy additions. 相似文献
25.
Jianxin Wei Mark R Pickering Michael R Frater John F Arnold John A Boman Wenjun Zeng 《IEEE transactions on image processing》2005,14(8):1033-1042
It is well known that tile-boundary artifacts occur in wavelet-based lossy image coding. However, until now, their cause has not been understood well. In this paper, we show that boundary artifacts are an inescapable consequence of the usual methods used to choose tile size and the type of symmetric extension employed in a wavelet-based image decomposition system. This paper presents a novel method for reducing these tile-boundary artifacts. The method employs odd tile sizes (2N + 1 samples) rather than the conventional even tile sizes (2N samples). It is shown that, for the same bit rate, an image compressed using an odd tile length low-pass first (OTLPF) convention has significantly less boundary artifacts than an image compressed using even tile sizes. The OTLPF convention can also be incorporated into the JPEG 2000 image compression algorithm using extensions defined in Part 2 of this standard. 相似文献
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BaMgAl10O17∶Eu2 (BAM) was prepared in the microemulsion system and its phase behavior was studied. There exists a small region in the reverse microemulsion system where the dispersed particles are of spherical form. In this way, BAM blue phosphor with good dispersion can be synthesized. The microemulsion phase diagrams of the pseudo-ternary system (Triton X-100/cosurfactant-oil-BAM brine) were first established intuitively by the dilution method. The microstructure of microemulsions was determined through eyeballing, conductance technique, and polar optical microscopy. Its phase behavior is affected by various factors, such as temperature (room temperature, 30, 40 ℃), oil, surfactants, and cosurfactants in microemulsions. According to the phase diagrams, the microemulsion system of Triton X-100/1-hexanol-hexane-BAM brine was chosen to prepare the precursor. The BAM phosphor can be obtained via sintering the precursor at a comparatively low temperature. The phosphors were characterized by XRD and vacuum ultraviolet (VUV) spectra. 相似文献
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基体温度对磁控溅射沉积ZAO薄膜性能的影响 总被引:8,自引:2,他引:6
利用中频交流磁控溅射方法 ,采用氧化锌铝陶瓷靶材 [w(ZnO) =98%、w(Al2 O3 ) =2 % ]制备了ZAO(ZnO∶Al)薄膜 ,观察了基体温度对ZAO薄膜的晶体结构、电学和光学性能的影响 ,采用X射线衍射仪对薄膜的结构进行了分析 ,采用光学分度计和电阻测试仪测量了薄膜的光学、电学特性 ,采用霍尔测试仪测量了薄膜的载流子浓度和霍尔迁移率。结果表明 :沉积薄膜时的基体温度对薄膜的结构、结晶状况、可见光透射率以及导电性有较大的影响。当基体温度为 2 5 0℃ ,Ar分压为 0 8Pa时 ,薄膜的最低电阻率为 4 6× 10 -4Ω·cm ,方块电阻为 35Ω时 ,可见光 (λ =5 5 0nm)透射率高达 92 0 %。 相似文献
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本文用大视场光学显微镜、电子探针观察和分析了掺钛蓝宝石激光晶体中夹杂物的形状、尺寸大小及元素组成,并提出消除和减少这些夹杂物的方法. 相似文献
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以YAG为添加剂的气压烧结氮化硅 总被引:2,自引:1,他引:1
本文以添加YAG的反应烧结氮化硅(RBSN)为前驱体,采用气氛加压烧结的工艺,在0.5~9.0MPa氮气压力范围,研究了不同氮压对烧结体的密度、相组成、强度和显微结构的影响及其相互间的关系。研究表明,通过改变氮气压力能有效地调控材料的显微结构,材料的性能又受控于显微结构的变化。 相似文献
30.
国外工程公司的项目实施工作法是科技发展和经济发展的产物。公司为谋求生存和发展,必须采取先进的技术和科学管理,同时获得适当的利润回报。本文介绍美国UCC公司的项目工作八段法。 相似文献