由丙烯二聚制备2,3-二甲基丁烯技术的开发和工业化的研究

以杀螟硫磷(1)和氰戊菊酯(2)(图1)为代表的杀虫剂是住友公司农药事业的支柱。该公司竭力研制杀虫效果高、对环境无污染的安全杀虫剂。     

野生黑腹果蝇引种培养与唾腺染色体观察

对佳木斯地区的野生黑腹果蝇（Drosophila melanogaster）进行采集,并在实验室内进行培养训化,用常规果蝇培养基进行培养．选用卡宝品红染色法进行唾腺染色体临时装片的制备,观察其染色效果,与常规方法进行比较,效果比较好,并应用于遗传学教学．     

基于正交试验的簧片阀噪声优化研究北大核心CSCD

为研究簧片阀主要结构参数对压缩机整机噪声的影响规律,分析了簧片阀吸排气阀片厚度t、通流面积的S及升程高度h对气阀机械噪声和气动噪声的影响,采用正交试验方法对某微型活塞压缩机进行噪声试验。对试验结果进行极差分析并对簧片阀主要结构参数对压缩机整机噪声的影响进行排序,结果显示吸排气通道面积及排气升程为影响压缩机噪声的主要结构参数。对试验样机用簧片阀参数进行优选组合并进行验证,试验证明优选后气阀(t_(吸气)=0.4 mm、t_(排气)=0.32 mm、S_(吸气)=360.2 mm^(2)、S_(排气)=254.6 mm^(2)、h_(排气)=1.9 mm)相对于原始气阀使压缩机整机A计权声压级下降了2.4dB(A),由气阀引起的压缩机噪声增量降低了9.3 dB(A),有效地改善了压缩机整机噪声。本文研究结果可为低噪声气阀的设计及压缩机降噪提供依据。     

拟建鄱阳湖水利枢纽对湖区水环境容量的影响

采用水动力水质模型模拟了鄱阳湖在极端退水年(2016年)和一般退水年(2017年)两种退水工况下拟建鄱阳湖水利枢纽建设前后的水动力水质过程,并构建湖区水环境容量模型评估了鄱阳湖拟建水利枢纽对湖区水质和水环境容量的影响。模拟结果表明：枢纽建设运行能显著增加鄱阳湖的水体体积,每月最大可增加77%;在退水初期主要降低湖泊中部的TP质量浓度,在极端退水年的退水后期会导致闸上TP质量浓度升高,在一般退水年则会导致闸上TP质量浓度降低,但对COD_Mn和NH₃-N质量浓度空间分布无明显影响;在极端退水年,枢纽建设运行会导致COD_Mn、NH₃-N和TP质量浓度增大,而在一般退水年则会导致TP的质量浓度降低;枢纽建设运行能显著提升COD_Mn和NH₃-N的水环境容量,在一般退水年会增大TP的水环境容量,但在极端退水年TP的水环境容量可能降低。     

化工机械设备的管理措施分析与维修保养技术应用探究

在我国,化工企业作为起步较早的企业,随着其发展的不断深入,发展进程的不断加快,各方面基础技术已经趋于成熟,但企业的发展和经济效益的产生,依赖的因素较多,其中最基础的因素,就是化工设备的管理完整和维修保养的完善,从而使化工设备保持来良好的生产特性,而保持化工设备良好生产特性的根本,就是化工机械设备的有效应用,本文聚焦化工机械设备的管理与保养问题,通过剖析化工机械设备当下在化工企业中扮演的角色及存在的问题,力争为化工机械设备的管理与维修保养,提供可行的建议与办法。     

惠安女服饰纹样研究

惠安女服饰有独特的地域特点,被列入国家非物质文化遗产保护项目,其服饰纹样形式多样,内容丰富,色彩强烈,呈现出特定的文化内涵。通过实地调研惠安女服饰纹样的设计种类、表现手法、色彩运用,论述了惠安女服饰纹样的文化内涵,该服饰纹样的研究有利于文化遗产的保护。     

Microstructure characterization of reinforcements in in-situ synthesized composites of Al-Zr-O system

A novel in-situ reaction system Al-Zr-O was developed. In-situ Al3Zr and Al2O3 particulates reinforced aluminum matrix composites were fabricated by the direct melt reaction technique in the Al-Zr-O system. Microstructures of the composites and crystal morphology of in-situ formed Al3Zr and Al2O3 particulates were analyzed by scanning electron microscope (SEM) and transmission electron microscope (TEM). Results indicate that in-situ formed Al3 Zr and Al2O3 particles are finer and well distributed in aluminum matrix. Al3Zr particulates with a tetragonal structure are mainly in the shape of polyhedron. A few of them are in the form of rectangle. The length/width ratio of the rectangular Al3Zr is less than 2.0 and the maximum size is 2μm. In addition, a certain number of Al2O3 submicro particles with a hexagonal structure are also generated in this system. Furthermore, it is found that Al3Zr crystal grows by the mechanism of twinning. The twin plane is (114). The twinning direction is [221]. The tensile tests show that the composites synthesized in the Al-Zr-O system exhibits high strength and ductility. There are a lot of ripples with fine particles on the fracture. The principal strengthening mechanisms for (Al3Zr Al2O3 )p/Al composites may include Orowan strengthening, grain-refining strengthening, solid-solution strengthening and dislocation strengthening.     

炼钢脱氧用铝线的无结晶器水平连续铸造

介绍了用废旧纯铝料，在特殊的固体燃料反射炉中连续熔化，水平连铸成（３．０～９．５）ｍｍ铝线坯的工艺流程及设备。经过试验，确定是一种生产炼钢脱氧用铝线的经济、有效的工艺方法。     

Deformation behavior ofA6063 tube with initial thickness deviation in free hydraulic bulging

Experiment on seamless tubes of aluminum alloy A6063 with initial thickness deviation of 0-20% was conducted through a free hydraulic bulging with tube ends free. The influence of initial thickness deviation on the cross-section profile, thickness distribution, maximum internal pressure and maximum radial expansion was investigated. FEM simulation was also performed in order to examine and help explaining the experimental results. The results indicate that the internal pressure and maximum internal pressure appear to be little influenced by the initial thickness deviation, and that the cross-section profile of the bulged tube changes diversely and can not be a perfect circle. The results also suggest that the increase in initial thickness deviation may lead to a remarkable decrease in maximum radial expansion, and a rapid increase in thickness deviation and the center eccentricity of the inner and outer profiles.     

Effects of deformation on microstructures and properties of submicron crystalline Cu-5%Cr alloy

Warm extrusion of submicron crystalline Cu-5%Cr from 100 ℃ to 600 ℃ was investigated. The effects of different extrusion ratios and different extrusion temperatures on microstructures and properties of submicron crystalline Cu-5%Cr were studied. The microstructures of the extruded Cu-5%Cr were characterized by backscattered electron irnages（BSE） and transmission electron microscopy（TEM）. The mechanical properties of the extruded Cu-5%Cr were measured by means of microhardness and tension test. The results show that, the deformation, dynamic recovery and dynamic recrystallization of the extruded Cu-5%Cr are mainly produced in Cu matrix. The higher extrusion ratio leads to more uniform microstructure and finer Cu grains. When being extruded in the range of 100-600 ℃, dynamic recovery of Cu is the dominant process, and dynamic recrystallization of Cu occurred above 300 ℃ is far from end. The most part of microstructure of as-extruded Cu-5%Cr is subcrystaUines produced by dynamic recovery, only a few recrystallines exist, and the average size of these grains is not larger than 400 nm. With extrusion temperature rising, the tensile strength and microhardness of Cu-5%Cr decrease, and elongation increases gradually.