Microstructure refinement of Sn-Sb Peritectic alloy by power ultrasonic

Sn-Sb peritectic alloy was treated with 400 W, 600 W and 800 W ultrasonic, respectively, to study the effect of power ultrasonic on solidification microstructure. Results show that power ultrasonic can refine α phase and β phase of the alloy, as well as eliminate gravitational segregation. Moreover, 600 W ultrasonic demonstrated the best refining effect, not only homogenous and fine solidification microstructure can be obtained, the cubical β phase crystals can also be spheroidized.     

原子吸收分光光度法测定土壤中的镍的方法研究

本文对微波消解-原子吸收分光光度法测定土壤样品中的镍元素的分析方法进行了探讨,并对不同类型土壤消解后赶酸与不赶酸的测定结果进行了比较。结果表明,原子吸收法测定土壤中的镍必须赶酸,但赶酸的方法可以简化,并利用连续光源原子吸收光谱图进行了验证。     

中国传统"文荫思想"的启示——襄樊五中新校园文化空间规划设计体验

本文主要探讨传统文荫思想在中学新校区中的应用。针对襄樊五中这所百年名校，通过对老校园空间环境研究和老校区建筑的研究，探寻在新校医中的历史文脉设计方法，提升校园的空间品质，促进环境育人。     

Reaction of (C_5H_5)_2NdCl·2LiCl with n-Butyllithium: Formation and Crystal Structure of [Li(DME)_3][(C_5H_5)_3Nd(μ-H)Nd(C_5H_5)_3]

Reaction of (C_5H_5)_2NdCl·2LiCl with n-Butyllithium: Formation and Crystal Structure of [Li(DME)_3][(C_5H_5)_3Nd(μ-H)Nd(C_5H_5)_3]     

一种基于折叠计数器重新播种的确定自测试方案

提出了一种基于扫描自测试的确定与混合模式新方案,这种方案依赖于一个新型的模式生成器,它主要配备一个可编程的约翰逊计数器,称之为折叠计数器。这种新技术首先使用一个小的线性反馈移位寄存器（LFSR）,生成伪随机测试模式测试容易测试的故障,并且获得一个硬故障测试立方集T;其次采用经典的输入精简技术,集合T的测试立方宽度可以被压缩;最终为了能够找出合理的小数目折叠计数器种子,来生成这个确定的测试立方集T,给出了其理论背景和实用算法。试验结果表明,这个所建议的方案与先前所公布的基于线性反馈移位寄存器和约翰逊计数器的重新播种方法相比,具有非常出色的结果。因此它提供了一种有效的、弹性的基于扫描的自测试解。     

Preparation of liposome-coated oligonucleotide labeled with 99mTc and its uptake in vascular smooth muscle cells

To explore the preparation method of liposome-coated 99mTc-labeled antisense oligonucleotide (ASON),targeteing the proliferating cell nuclear antigen (PCNA), and to explore the biological characteristics and the uptake kinetics of a radiolabeled probe in vascular smooth muscle cells, an 18-base single-stranded antisense oligonucleotide targeting PCNA mRNA and the complementary strand (sense oligonucleotide, SON) were synthesized. The ASON (SON) was labeled with 99mTc, by conjugating the bifunctional chelator (hydrazino nicotinamide, HYNIC), and purified through a gel filtration column of Sephadex G-25. The product was then encapsulated in cationic liposome (oligofectamineTM). The radiolabeling efficiency, radiochemical purity, stability of the liposome-coated 99mTc-HYNIC-ASON in a phosphate buffered solution (PBS), and fresh human serum and its uptake rate were studied. There was no significant difference between the 99mTc radiolabeling efficiencies of HYNIC-ASON and HYNIC-SON, which were 60.04% ± 1.92% and 59.60% ± 2.53%, respectively (P ＞ 0.05, n = 5). The radiochemical purity of the liposome-coated 99mTc-HYNIC-ASON was 94.70% ± 1.90% (n = 5). And after incubation with PBS and fresh human seAt 90 min after transfection, the uptake rate of the liposome-coated 99mTc-HYNIC-ASON reached its peak of 83.8% ±5.92% in vascular smooth muscle cells (VSMCs) and was much higher than that of the nonliposome-coated 99mTc-HYNIC-ASON, which was 11.16% ± 0.54% (P ＜ 0.01, n = 4). The labeling method of PCNA ASON (SON) conjugated by HYNIC has been proved successful. The liposome was able to enhance the ASON (SON) uptake in VSMCs,and could be widely used as a safe, convenient, effective gene transfer carrier.     

脉冲中子伽马密度测井密度敏感度研究

地层密度敏感度是决定脉冲中子伽马密度测井仪器源距的一个重要参考指标,对源距的优化可以提高该仪器的地层密度分辨率。基于脉冲中子伽马密度测量中的中子伽马场耦合理论讨论仪器伽马响应与地层含氢指数和体积密度的关系,推导地层密度灵敏度与近源距及探测器间距之间的关系,并结合蒙特卡洛模拟计算结果加以验证。理论分析和模拟计算结果表明,当地层密度一定时,近、远非弹性散射伽马射线响应的对数随含氢指数的增加而增加,在相同含氢指数的情况下,近、远非弹性散射伽马射线响应随地层体积密度的增加而增加;探测器间距保持不变时,密度灵敏度随近源距的增加而降低;近源距保持不变时,密度灵敏度随探测器间距的增加而增加;探测器间距对仪器地层密度灵敏度的影响大于短源距。     

以文相地:一种人文视角考量城市建设用地的规划理念

<正>1.何谓"以文相地"中国规划对于城市建设用地的考量,不仅关注用地的安全性与实用功能,还特别关注用地的人文特性,累代形成了以人文视角考量城市建设用地,并将建设用地选位与城市人文空间格局塑造紧密联系的规划传统。"以文相地"便是这一传统的重要实践理念。从历史文献来看,"相地"即勘察土地,如《史记·周本纪》中的"相地之宜";"以文相地"重在从用地与城市历史、文化、理想、精神、风景相关联的视角识别和精选土地。例如"尊地""静地""严肃之地""仰     

Corrosion of two kinds of cast steels containing chromium in hot concentrated alkaline

A typical hot concentrated alkaline corrosion environment exists in alumina metallurgical industry, so that steel materials with outstanding alkaline corrosion resistance are strongly demanded for its processing equipment. In this paper, the corrosion resistance of two kinds of martensitic cast steels containing chromium in static 303g/L NaOH alkaline solution at 85℃ was studied through polarization and potential-time curves, corrosion weight loss and corrosion morphology analysis. Experimental results showed that protection effect by passive film of cast steel containing Cr was temporary. The low carbon steel without Cr content also exhibited chemical passivity in the same solution. The corrosion mode of the tested Cr-containing cast steel was composed of active dissolving corrosion and caustic embrittlement cracking. Dissolving corrosion was the primary mechanism for the induced weight loss, while severe caustic embrittlement cracking was secondary. With the increase of chromium content in the cast steel, the tendency of the caustic embrittlement cracking decreased, while the active dissolving corrosion increased.     

Electroless Ni-Co-P Coating of Cenospheres Using Ag(NH_3)_2~+ Activator

FLY ASH CENOSPHERES are primarily a by-productin power generation plants.Research is in progress toeffectively use this by-product to produce new usableand profitable materials as they pose major disposaland environmental problems.Fly ash cenospheres areunique,property stable,non-toxic,non-metallic hollowmicro-particles.Due to the unique hollow structure andphysical mechanics properties,Cu^Ag and other metalsare often coated on cenospheres to produce lightweightmetal matrix composites,w…