双膦胺镍-甲基铝氧烷体系催化苯乙烯聚合

研究了具有新型结构的双膦胺镍配合物N,N-双(二苯膦基)-对甲氧基苯胺二氯化镍-甲基铝氧烷(PNP-N i-MAO)催化体系对苯乙烯聚合的催化性能,考察了聚合温度、n(A l)∶n(PNP-N i)、PNP-N i的浓度和苯乙烯的浓度对催化活性、苯乙烯转化率、聚苯乙烯相对分子质量及其分布的影响,并用核磁共振和凝胶色谱对聚苯乙烯的结构进行了表征。实验结果表明,在聚合温度25℃、聚合时间1h、n(A l)∶n(PNP-N i)=300、c(苯乙烯)=2.3m ol/L、c(PNP-N i)=0.4mm ol/L、甲苯为溶剂的适宜条件下,苯乙烯的转化率可达95%以上,催化活性达到5×105g/(m ol.h)左右。核磁共振和凝胶色谱表征结果显示,所得聚苯乙烯为无规结构,重均相对分子质量约为1×104,相对分子质量分布Mw/Mn约为2。     

流变仪在覆铜板工序中的应用

本文简要叙述利用流变仪对覆铜箔层压板生产工序中的胶液和半固化片参数进行控制,从而更好地保证胶液和 半固化片性状的一致性,以有利于控制板材流胶和品质。     

论建立动态勘探目标评价体系的迫切必要性

从国际上通行的油气勘探评价工作重点,中国石油所面临的"已逐步进入一个不断在老区范围内开展精细勘探、在老区范围内开展新区块、新层系勘探以获得主要的储量增长"的新的勘探形势,现有地质研究中各专题研究与具体勘探目标评价脱节等多个方面,论述了在中国石油内部建立一套动态勘探目标评价体系的迫切必要性;并在此基础上阐述了一个完整的动态勘探目标评价体系应包括的主要内容;最后对该体系的建设进行了可行性分析。     

Anthocyanin composition of the red wine Babić affected by maceration treatment

Identification of anthocyanins in the wine made of the Croatian autochthonous grape variety of Babić (Vitis vinifera L.) was carried out and their profile was determined by means of high-performance liquid chromatography with diode array and mass spectrometric detection. Dependence of anthocyanins content and profile on maceration treatment conditions was investigated. Statistically significant differences of anthocyanins concentration in wines Babić produced by various maceration treatments were confirmed by the use of multivariate analysis of variances. The investigation results indicated that the maceration temperature exerts higher influence on anthocyanins concentration than the duration of maceration. In addition, on the basis of anthocyanin composition and using different multivariate statistical analyses, differentiation of wines Babić according to maceration treatments was procured.     

瞬态瑞利面波技术在地震勘探方面的应用研究

运用瞬态瑞利面小勘探方法可以在寻找激发岩性和提供静校正所需参数方面取得好的效果。     

硅钢片模具设计及其线切割加工

论述了电磁铁铁芯 (硅钢片 )模具的设计要点及其线切割加工的技巧 ,提出了提高模具加工精度和使用寿命的有效措施。     

共晶碳化物团球化对铸铁激光熔敷层抗裂性的影响

为提高铸铁表面大面积激光熔敷层抗裂性问题，通过冶金因元素控制熔敷层组织形态在熔敷材料中加入碱金属元素钾，研究了在激光快速加热条件下钾对铸铁激光熔敷层组织团球化的影响，进而分析了该球状组织对熔敷层抗裂性的影响，结果表明随熔敷金属内钾含量增多熔敷层内共晶碳化物组织呈球状及孤岛状，这种组织明显提高了熔敷层抗裂性，此外大量的渗碳体组织确保了熔敷层具有较高的耐磨性；获得了无裂纹的大面积搭接熔敷层，其对应合金系统为Fe-C-Si-Ni-K。     

复合乳化沥青的粘附性试验方法研究

鉴于目前使用的阳离子乳化沥青粘附性试验方法难以有效评价复合乳化沥青粘附性，通过试验研究并综合考虑乳化沥青施工和路用实际情况，提出了乳化沥青水煮法试验方法和采用该方法检验复合乳化沥青粘附性时的评定标准。     

Bücher

Ohne Zusammenfassung VDI     

On exploring inter-iteration parallelism within rate-balanced multirate multidimensional DSP algorithms

Although the notion of the parallelism in multidimensional applications has existed for a long time, it is so far unknown what the bound (if any) of inter-iteration parallelism in multirate multidimensional digital signal processing (DSP) algorithms is, and whether the maximum inter-iteration parallelism can be achieved for arbitrary multirate data flow algorithms. This paper explores the bound of inter-iteration parallelism within rate-balanced multirate multidimensional DSP algorithms and proves that this parallelism can always be achieved in hardware system given the availability of a large number of processors and the interconnections between them.