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51.
H. Fan A. Wright J. Gabaldon A. Rodriguez C.J. Brinker Y.‐B. Jiang 《Advanced functional materials》2006,16(7)
The synthesis of three‐dimensionally ordered, transparent gold‐nanocrystal (NC)/silica superlattice thin films using the self‐assembly (by spin‐coating) of water‐soluble gold nanocrystal micelles and soluble silica is reported by Fan and co‐workers on p. 891. The robust, 3D NC/silica superlattice films are of interest for the development of collective optical and electronic phenomena, and, importantly, for the integration of NC arrays into device architectures. Nanocrystals and their ordered arrays hold many important applications in fields such as catalysis, surface‐enhanced Raman spectroscopy based sensors, memory storage, and electronic and optical nanodevices. Herein, a simple and general method to synthesize ordered, three‐dimensional, transparent gold nanocrystal/silica superlattice thin films by self‐assembly of gold nanocrystal micelles with silica or organosilsesquioxane by spin‐coating is reported. The self‐assembly process is conducted under acidic sol–gel conditions (ca. pH 2), ensuring spin‐solution homogeneity and stability and facilitating the formation of ordered and transparent gold nanocrystal/silica films. The monodisperse nanocrystals are organized within inorganic host matrices as a face‐centered cubic mesostructure, and characterized by transmission electron spectroscopy and X‐ray diffraction. 相似文献
52.
Isabel Vega Emiliano Fernández Carmen Mijangos Norma D'Accorso Daniel López 《应用聚合物科学杂志》2008,110(2):695-700
The authors report on the viscoelastic characterization of guar hydrogels obtained through complexation reactions with borax ions. These gels are compared with hydrogels obtained from poly(vinyl alcohol) of different degree of hydrolysis through complexation reactions with congo red. The effect of the degree of hydrolysis and both, the concentration of PVA and the concentration of congo red, on the viscoelastic properties of the hydrogels is analyzed. The potential use of the PVA‐based hydrogels as hydraulic fracturing liquids is discussed in relation to the commonly used fracturing liquid based on the guar–borax system. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
53.
Placid Rodriguez 《Metallurgical and Materials Transactions A》2004,35(9):2697-2705
A critical review of available results on the dependence of grain size on the activation parameters for deformation, specifically,
the activation volume, V*, and the thermal component of flow stress, σ*, has been carried out with a view to verifying the Armstrong prediction that identifies the Hall-Petch (H-P) intercept with
the easy slip system and the H-P slope with the most difficult system in polycrystals. The influence of slip system choice
is demonstrated using results on Cd and Zr. The Armstrong prediction is valid for basal slip hcp metals, such as Cd and Zn,
with V* and σ* determined by the difficult pyramidal slip. For the prism slip metals such as Zr and Ti, V* and σ* are controlled by interstitial solutes and are independent of grain size. The results on Zr are used to highlight the influence
of dynamic strain aging on the H-P parameters. In bcc metals, in which the Peierls-Nabarro barrier is the rate-controlling
obstacle, V* and σ* are again independent of grain size. For fcc metals, correlation of the H-P slope with the cross-slip stress, predicted
by the Armstrong model, has been demonstrated for a few cases. The variation of V* with grain size in Ni as reported by Narutani and Takamura (Acta Metall. Mater., 1991, vol. 227, pp. 2037–49) is newly interpreted in terms of the Armstrong model that associates the H-P intercept in fcc
metals with dislocation intersections and the H-P slope with cross-slip, and provides realistic results for the activation
volumes for the two processes.
This article is based on a presentation given in the symposium “Dynamic Deformation: Constitutive Modeling, Grain Size, and
Other Effects: In Honor of Prof. Ronald W. Armstrong,” March 2–6, 2003, at the 2003 TMS/ASM Annual Meeting, San Diego, California,
under the auspices of the TMS/ASM Joint Mechanical Behavior of Materials Committee. 相似文献
54.
J.L. Fernández-Martínez J.P. Fernández-Alvarez L.M. Pedruelo-González 《Computers & Geosciences》2008,34(3):213-225
A MATLAB®-based computer code that analyses the traveltime distribution and performs quality analysis at the pre-inversion stage for 2D transmission experiments is presented. The core tools of this approach are the so-called mean traveltime curves. For any general recording geometry, the user may select any pair of subsets of contiguous sources and receivers. The portion of the domain swept by the implied rays defines a zone of analysis, and for each source (receiver) the outcoming (incoming) ray fan is named a source (receiver) gather. The empirical mean traveltime curves are constructed, for each zone, by assigning the average and the standard deviation of the traveltimes in the gathers to the positions of the sources (receivers).The theoretical expressions assume isotropic homogeneous velocity inside each zone. The empirical counterparts use the observed traveltimes and make no assumptions. Isotropic velocity in each zone is inferred by least-squares fitting of the empirical mean traveltime curves. The user may refine the analysis considering different zones (multi-zone analysis). Initially the whole domain is modelled as a single zone. The procedure compares empirical versus theoretical curves. In addition, residuals can be plotted using source–receiver positions as plane coordinates. The results are used to unravel the possible presence of anomalous gathers, heterogeneities, anisotropies, etc. Depending on the kind of anomalies, velocity estimation and mean time residuals are different in the source and receiver gather curves.This software helps to grasp a better understanding of the data variability before the inversion and provides to the geophysicist an approximate zonal isotropic model and a range of velocity variation that can be used in the inverse problem as a priori information (regularization term). Its use is described through tutorial examples. A guided user interface leads the user through the algorithm steps. 相似文献
55.
56.
The effect of heat-ageing on four bituminous roofing membranes, two modified with atactic polypropylene (APP) and two modified
with styrene-butadiene-styrene (SBS) was studied using tensile testing and dynamic mechanical thermals analysis (DMA). The
samples were heated at 80°C for 7, 28, 84 and 168 days and were tensile tested at 23, 0, −10, −20 and −30°C. Each heat-aged
sample was also subjected to thermomechanical testing to find its glass transition temperature T
g
. The results show significant variation in the effect of heat-ageing on tensile strength and elongation of membranes. T
g
values differ with the modifiers and other ingredients of the membranes and are affected by heat-ageing. The influence of
the glass transition zone measured by DMA is also reflected in the tensile test results.
Resume On a étudié l’influence du vieillissement par la chaleur sur quatre membranes d’étanchéité, deux d’entre elles étant traitées par APP (polypropylène atactique) et deux par SBS (styrène de styrène butadiène), à l’aide de l’essai en traction et de l’analyse thermique mécaniques (DMA). Les échantillons ont été chauffés à 80°C pendant 7, 28, 84 et 168 jours et essayés en traction à 23, 0, −10, −20 et −30°C. Chaque échantillon vieilli par la chaleur a été également soumis à un essai thermomécanique pour identifier sa température de passage à l’état vitreux T g . Les résultats montrent des différences importantes dans l’influence de la chaleur sur la résistance en traction et l’allongement des membranes. Les valeurs de T g diffèrent selon les traitements et les autres composants des membranes, et sont affectées par le vieillissement par la chaleur. L’influence de la zone de passage à l’état vitreux mesurée par l’analyse thermique mécainique se traduit aussi dans les résultats de l’essai en traction.相似文献
57.
A study has been made of the procedures used for the lap and butt welding of 0.62 and 1.16 mm thickness steel sheets coated with Al55-Zn alloy, using laser-beam technology. The main problems arise in lap welding as a result of zinc evaporation from the coating. The vapour pressures of this element lead to cratering and blistering of the welds which are visible from the external surface and imply severe weld defects. An efficient solution to this problem consists in leaving a gap between the internal faces, thus allowing the zinc vapours to escape. Excessive gaps, however, lead to the molten metal collapse and to lack of penetration. In the present work, acceptable results were obtained with a maximum interface separation of 0.1 mm. This allows excellent continuity of the joints, without cracks, pores or non-metallic inclusions and with moderate hardnesses, thus demonstrating the good laser weldability of the coated material. A difficulty arises, however, in relation to the coating in zones close to the weld. In these high-temperature zones the coating is lost, and in the immediately adjacent areas the coating microstructure and phases are altered, as was shown by scanning electron microscope analyses. 相似文献
58.
G Martín Carballo R Codoceo Alquila G Fernández Cano F Hawkins Carranza C Grande Aragón A Velasco Hernando R Gracia Bouthelier 《Canadian Metallurgical Quarterly》1997,47(3):302-310
OBJECTIVE: The objective of this study was to determine fibronectin levels in umbilical cord blood of infants of diabetic mothers (IDM) and evaluate a possible correlation with perinatal pathology. PATIENTS AND METHODS: A prospective study of 58 IDM (33 males and 25 females) and 58 control newborns (NB) (33 males and 25 females) was carried out. RESULTS: There were no differences in fibronectin levels between the two groups nor between the sexes. Perinatal morbidity was higher in the IDM group, but there was no correlation between fibronectin levels and the presence of perinatal pathology. CONCLUSIONS: Fibronectin levels are not useful in the perinatal evaluation of infants of diabetic mothers. 相似文献
59.
MJ Fernández Ace?ero J Farina González P Arangoncillo Ballesteros 《Canadian Metallurgical Quarterly》1997,142(5-6):289-296
We have performed immunohistochemical staining for p53 and c-erbB-2 on formaldehyde-fixed, paraffin-embedded primary invasive ductal carcinomas from 112 patients, with a minimal follow-up time of 60 months. All of them had received postoperative chemoradiation therapy. We have analyzed the association of these factors with epidemiologic risk factors, histopathologic features and hormonal receptor status and the influence on prognosis. Our results indicate that the expression of c-erbB-2 protein defines a group of node-negative patients with poor prognosis. The overexpression of c-erbB-2 has shown a significant association with estrogen receptor status (those tumors expressing c-erbB-2 are usually estrogen receptor negative), presence of fibrosis and lymphoplasmacytoid infiltrates. P53 expression has shown no relation either with prognosis or with any other histopathologic or clinical feature. The only factors with prognostic influence in our series have been tumor size, the presence of node metastases, TNM stage and the prognostic morphometric index (Baak's index), apart from c-erbB-2 in node-negative patients. However, only the TNM stage showed an independent association with prognosis after a multivariate analysis. In summary, in our experience the expression of p53 protein has no prognostic influence on breast carcinoma, and TNM stage remains to be as the most powerful prognostic factor in these patients. 相似文献
60.
MJ Castro P Morales V Fernández-Soria B Suarez MJ Recio M Alvarez M Martín-Villa A Arnaiz-Villena 《Canadian Metallurgical Quarterly》1996,43(6):327-336
The aim of this study was to determine whether bisaramil-an antiarrhythmic compound under clinical investigation-influences the reperfusion-induced arrhythmias and biochemical parameters characterizing occlusion-reperfusion-induced free-radical reactions. The left descending coronary artery (LAD) was occluded for 60 min in anaesthetized dogs followed by one hour of reperfusion. Blood samples were taken at different times of the occlusion and reperfusion for the determination of plasma concentration of malondialdehyde (MDA), reduced (GSH) and oxidized glutathione (GSSG); furthermore of the activity of catalase and superoxide dismutase (SOD). Free-radical generating capacity of polymorph neutrophil granulocytes (PMN) was also measured. At the end of the experiments heart tissue samples were excised from the injured areas and from the intact part of the left ventricular muscle. In tissues samples the concentrations of MDA and GSH and the activity of SOD were determined. Bisaramil was given as an i.v. bolus injection at a dose of 2 mg kg-1 several minutes prior to the end of LAD-occlusion; then the administration was repeated in the 30th minute of reperfusion. In the control group (10 dogs) ventricular fibrillation (VF) occurred in seven cases which resulted in death in three. In the bisaramil-treated group, however. VF was seen in three cases and no death was recorded. Bisaramil inhibited the elevation of the plasma concentration of MDA and GSSG during the reperfusion and abolished the decrease in the plasma concentration of GSH during the occlusion and reperfusion. The activity of SOD and catalase in plasma was much better preserved in the bisaramil-treated group then in the controls. Bisaramil significantly inhibited the increase of the superoxide-radical generating capacity of PMNs during the reperfusion. The data obtained from myocardial tissue samples supported the cardioprotective effect of bisaramil. The biochemical investigation of ischemic-reperfused myocardium showed that bisaramil promoted preservation of SOD-activity and of tissue glutathione. Results of this study clearly showed that bisaramil has a significant effect on ischemiareperfusion injury. Besides its inhibitory effects on ischaemia-reperfusion induced arrhythmias it has a special benefit in influencing free-radical mediated damage leading to better preservation of membranes and to limitations of irreversible cell injuries. 相似文献