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排序方式: 共有2433条查询结果,搜索用时 31 毫秒
31.
Maria?Antonietta BresciaEmail author Vincenzo?Mazzilli Angela?Sgaramella Stefano?Ghelli Francesco?Paolo Fanizzi Antonio?Sacco 《Journal of the American Oil Chemists' Society》2004,81(5):431-436
Characterization of the lipid fraction of raw cow and buffalo milk samples, collected in different breeding areas in Apulia,
a region of southern Italy, were performed by means of 1H NMR. The aim of this work was to establish whether FA composition data obtained by 1H NMR can be used in the differentiation of buffalo and cow milk samples according to species. A complete assignment of the
signals present in the spectrum was attempted by COSY, heteronuclear coherence spectra. Quantification of FA was carried out
by inserting the integrals of particular peaks in suitable calculations. Multivariate statistical analysis, conducted on the
results of the quantification, permitted buffalo and cow milks to be distinguished. 相似文献
32.
Angela S. Rocha Arnaldo C. Faro Jr. Laetitia Oliviero Jacob Van Gestel Franoise Maug 《Journal of Catalysis》2007,252(2):321-334
The activity of NiMoS catalysts supported on niobia, alumina, and niobia/alumina was compared for the thiophene hydrodesulfurization (HDS) and 2,6-dimethylaniline (2,6-DMA) hydrodenitrogenation (HDN) reactions. To evaluate the acidity of the supports and identify the nature of the sulfide sites, adsorption of 2,6-dimethylpyridine, pyridine, and CO was performed and followed by IR spectroscopy. This study has shown that with niobia as a support, the activity of NiMoS catalysts in thiophene HDS and in HDN of 2,6-DMA was no longer promoted by the synergy between Ni and Mo. The absence of synergy between molybdenum and nickel on niobia can be explained by the strong interaction of each metal with niobia at the expense of interaction with each other. Moreover, it has been shown that on a niobia/alumina support, the formation of the NiMoS phase can be directly linked to the presence of alumina not covered by niobia. However, niobia is an interesting support for the HDN of 2,6-DMA, because it favors the formation of xylene through direct ammonia elimination involving low H2 consumption. The activity for xylene formation on niobia is linked to the electron-deficient nature of the Mo sulfide site, as demonstrated by CO adsorption followed by IR. 相似文献
33.
Flavonoid pigments in chalkhill blue (Lysandra coridon Poda) and other lycaenid butterflies 总被引:1,自引:0,他引:1
Angela Wilson 《Journal of chemical ecology》1987,13(3):473-493
Nine flavonoids, namely, kaempferol, kaempferol 7-rharanoside, kaempferol 3-rhamnoside, kaempferol 3-glucoside, kaempferol 3-glucoside, 7-rhamnoside, quercetin 3-glucoside, quercetin 3,7-diglucoside, isorhamnetin 3-glucoside, and isorhamnetin 3,7-diglucoside, have been identified in the body and wings of the chalkhill blue butterflyLysandra coridon Poda. Flavonoids have also been found in 15 of a further 17 lycaenid species examined. Analysis of the two-dimensional paper chromatographic flavonoid patterns and aglycone results has shown that the flavonoid content ofL. coridon and the other lycaenids is dependent on the flavonoid content of the larval diet. Differences in the flavonoid patterns ofL. coridon and its leguminous larval food plantsHippocrepis comosa, Anthyllis vulneraria, andLotus corniculatus, indicate that the ingested flavonoids are metabolized byL. coridon or its gut flora before sequestration. Despite the presence of fiavones, glycoflavones, and isoflavones in the larval food plant species, only flavonols are sequestered by the lycaenid species examined. The relationship between lycaenid butterflies and their larval food plants, and the possible role(s) of flavonoids in lycaenids has been discussed. Interactions between ants, plants, flavonoids, and myrmecophilous lycaenids have also been considered. 相似文献
34.
Chao AC Ziadeh BI Diau GY Wijendran V Sarkadi-Nagy E Hsieh AT Nathanielsz PW Brenna JT 《Lipids》2003,38(4):425-429
One of the major survival challenges of premature birth is production of lung surfactant. The lipid component of surfactant,
dipalmitoyl PC (DPPC), increases in concentration in the period before normal term birth via a net shift in FA composition away from unsaturates. We investigated the influence of dietary DHA and arachidonic acid (AA)
on lung FA composition and DPPC concentration in term and preterm baboons. Pregnant animals/neonates were randomized to one
of four groups: breast-fed (B), term formula-fed (T−), preterm formulafed (P−), and preterm fed formula supplemented with DHA-AA (P+). Breast milk contained 0.68%wt DHA and the P+ group formula contained 0.61%wt DHA. In the preterm groups (P− and P+), pregnant females received a course of antenatal corticosteroids. At the adjusted age of 4 wk, neonate lung tissue was harvested,
and FA composition and DPPC were analyzed. Palmitate was ∼28%wt of lung total FA and no significant differences were found
among the four treatment groups. In contrast, DPPC in the B group lung tissue was significantly greater than DPPC in the unsupplemented
groups, but not compared with the P+ group. The B and P+ groups were not significantly different in DHA and AA, but were different compared with the unsupplemented (T, P−) groups. These results indicate that LCP supplementation increases lung DHA and AA, without compromising overall lung 16∶0
or DPPC. The shift in FA composition toward greater unsaturation in the groups consuming LCP supported improved surfactant
lipid concentration in preterm neonate lungs. 相似文献
35.
(Z)-11-Octadecenyl acetate (Z11–18Ac) and (Z)-11-eicosenyl acetate (Z11–20Ac) were identified as the aggregation pheromones ofDrosophila ananassae, andZ11–20Ac was identified as the aggregation pheromone ofDrosophila bipectinata. Z11–18Ac andZ11–20Ac were not attractive alone; however, in combination with fermenting food odors, the acetates attracted flies of both sexes in a wind-tunnel olfactometer. The pheromones were present in the ejaculatory bulb of sexually mature male flies and transferred to the female during mating. MaleD. bipectinata released little if anyZ11–20Ac to the food; however, recently mated females releasedZ11–20Ac to the surrounding surfaces in just a few hours after mating.D. ananassae males, on the other hand, appeared to release moreZ11–18Ac andZ11–20Ac to the surroundings than mated females. AlthoughD. bipectinata males had noZ11–18Ac, flies were as attracted toZ11–18Ac as to an equal quantity ofZ11–20Ac.D. ananassae were attracted toZ11–18Ac but not toZ11–16Ac orZ11–20Ac. However,Z11–20Ac in combination withZ11–18Ac was significantly more attractive thanZ11–18Ac alone. 相似文献
36.
Angela Goodrum 《Information & Communications Technology Law》2015,24(2):164-182
The advent of the Internet and social media has revolutionized the way society communicates, the speed in which news is disseminated, and the approach that people take in their daily decision-making. Online reviews are now common place on nearly every consumer-related website. Consequently, attorneys are also being publicly scrutinized by their clients on a range of topics from price, competence, satisfaction, personality, communication, and effectiveness. On one side of the coin, this new phenomenon can be very rewarding since attorneys were previously limited to receiving a small number of referrals from the word-of-mouth promotion before the creation of online reviews. However, the exact opposite is true. Negative online reviews, whether accurate or not, may deter potential clients from even giving the attorney a second thought. As a result, a firm's business can feel the immediate impact of negative reviews. Attorneys, who legitimately need and want to protect their business and reputation, cannot speak freely online to defend their honor. Rather, an attorney must be mindful of not disclosing confidential client information or crossing other ethical lines that may then expose the attorney to potential discipline. There are several interests that must be considered such as allowing attorneys to exercise their First Amendment right to free speech, respect and adherence to the ethical rules of non-disclosure of confidential information, allowing attorneys to preserve their reputation, and protecting an attorney's marketability and means of generating income. This article explores the trend in offering reviews online in a variety of industries, including legal services, the statistical findings regarding the prevalence of this information and consumers' reliance on the information while making a purchasing decision. This article also considers the positive and negative implications of the reviews being so widely spread, while highlighting unique considerations as it relates to the practice of law and factors that may greatly skew a reviewer and reader's perceptions. Next, this article outlines the ethical considerations of attorneys if they want to respond to negative online feedback, such as disclosure of confidential information. Then, this article analyzes the American Bar Association (ABA) and several US states' ethics opinions for guidance for attorneys who wish to respond negative reviews. Finally, this article details the author's recommendations for attorneys, the ABA, and the US states and propose the areas where additional ethics opinions, rules and guidelines should be focused to establish a proper balance between the valuable insights discovered from a client's review and attorneys' legitimate interests in protecting their reputation and livelihood from inaccurate, malicious, or erroneous postings. 相似文献
37.
Nazanin Pourmand Vijay Parsa Angela Weaver 《International Journal of Speech Technology》2013,16(4):363-379
The performance of several noise reduction algorithms intended for wideband telephony was evaluated both subjectively and objectively. The chosen algorithms were based on statistical modeling, spectral subtraction, Wiener filtering, or subspace modelling principles. A customized wideband noise reduction database containing speech samples corrupted by three types of background noises at three SNR levels, along with their enhanced versions was created. The overall quality of the speech samples in the database was subsequently rated by a group of listeners with normal hearing capabilities. Comprehensive statistical analyses were performed to assess the reliability of the subjective data, and to assess the performance of noise reduction algorithms across varied noisy conditions. The subjective quality ratings were then used to investigate the performance of several auditory model-based objective quality metrics. Key results from these investigations include: (a) there was a high degree of inter- and intra-subject reliability in the subjective ratings, (b) noise reduction algorithms enhance speech quality for only a subset of the noise conditions, and (c) auditory model-based metrics perform similarly in predicting speech quality ratings, when speech quality scores pertaining to a particular noise condition were averaged. 相似文献
38.
39.
This paper introduces a tabu search heuristic for a production scheduling problem with sequence-dependent and time-dependent
setup times on a single machine. The problem consists in scheduling a set of dependent jobs, where the transition between
two jobs comprises an unrestricted setup that can be performed at any time, and a restricted setup that must be performed
outside of a given time interval which repeats daily in the same position. The setup time between two jobs is thus a function
of the completion time of the first job. The tabu search heuristic relies on shift and swap moves, and a surrogate objective
function is used to speed-up the neighborhood evaluation. Computational experiments show that the proposed heuristic consistently
finds better solutions in less computation time than a recent branch-and-cut algorithm. Furthermore, on instances where the
branch-and-cut algorithm cannot find the optimal solution, the heuristic always identifies a better solution. 相似文献
40.
Angela Schipper 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1994,199(6):437-441
Zusammenfassung Kornpartien verschiedener Winterweizensorten wurden in verschiedenen Reifestadien auf ihre Theologischen Eigenschaften und ihre Backqualität untersucht. Die Rohproteingehalte sind zu Beginn bzw. in der Mitte der Milchreife des Kornes sehr hoch, gehen dann aber deutlich zurück. Auch die Sedimentationswerte liegen in früheren Reifestadien höher als in der Vollreife. In den frühen Reifestadien liegen auch die relativen Sedimentationswerte (=Sed.-Wert: Rohproteingehalt des Kornes) am höchsten. Der Aschegehalt der Körner sinkt, die Mehlausbeute an Type 550 steigt mit fortschreitender Kornentwicklung und größeren Tausendkorngewichten.-Die im Farinographen und Extensographen ermittelten Teigeigenschaften der Mehle des unreifen und reifen Kornes unterscheiden sich meist deutlich; Art und Ausmaß dieser Veränderungen sind sortenabhängig.-Die bei vier Sorten in verschiedenen Reifestadien durchgeführten Backversuche lassen sowohl bei der Teigbeschaffenheit als auch bei den Gebäckeigenschaften deutliche, z. T. sortenspezifische Veränderungen in Abhängigkeit vom Reifestadium des Kornes erkennen. Spätestens ab der Teigreife weisen die geprüften Winterweizensorten dem reifen Korn vergleichbare Gebäckeigenschaften auf.
Rheological properties and baking quality of winter wheat in dependence on the stage of grain maturity
Grains of several wheat varieties in different stages of maturity were investigated for rheological properties and baking quality. Crude protein content was found to be very high at the beginning and in the middle of milk ripeness of the grain; later crude protein decreases strongly. Sedimentation values and relative sedimentation values (sed.-val.: protein content of the grain) are higher in the earlier stages of grain development, too. Mineral content of the grain decreases, flour yield (type 550) increases with processing grain development and increasing thousand kernel weights.-The dough properties (farinograph and extensiograph) of the flours of the unripe and the full ripe grains mostly differed markedly; type and extent of this changes are in dépendance on the genotype. For instance genotype Monopol with a genetical caused excellent baking quality has the best rheological properties in the flour of the full ripe grain. On the other hand the genotypes in the flour of the full ripe grain. On the other hand the genotypes Benno and Clement with genetical caused adhesive doughs and poorer baking quality develop their very negative rheological properties primarily in the later stages of ripeness.-Baking tests with four other cultivars demonstrate genotypical differences in sensory determined dough properties and in bread quality in dependence on stage of grain maturity. These four genotypes show comparable baking results for flours from grains in the wax-ripe stage and in the full ripeness.相似文献