Preparation of Oil-Encapsulated Microcapsules and Tribological Property of Ni Composite Coating

Microcapsules containing oil are potential candidate materials for preparing electrocomposite coatings with excellent tribological properties. In the present study, the preparation of oil-encapsulated microcapsules and electrodeposition of Ni-microcapsule composite coating are presented along with the properties of the coating. In situ interfacial polymerization method was used for the preparation of lubricating oil-encapsulated urea-formaldehyde microcapsules. The synthesized microcapsules were incorporated into the nickel matrix by electrodeposition using Ni-Watts bath. The Ni-composite coating containing microcapsules exhibited smaller Ni grain size, higher microhardness and lower surface roughness compared to plain Ni coating. Electrodeposited Ni coating containing oil-encapsulated microcapsules exhibited improved tribological properties with lower wear loss and coefficient of friction compared to plain nickel coating.     

Performance of Recalibrated Equations for the Estimation of Daily Reference Evapotranspiration

An accurate estimation of reference evapotranspiration (ET₀) is of paramount importance for many studies such as hydrologic water balance, irrigation system design and management, crop yield simulation, and water resources planning and management. In the present study, Blaney-Criddle, Jensen-Haise and Hargreaves (temperature based), Priestley-Taylor, Radiation and Makkink (radiation based) and, Pan Evaporation and Christiansen (pan evaporation based) methods have been evaluated and recalibrated with respect to FAO-56 Penman-Monteith method for estimating daily ET₀ in the semi-arid Tirupati, Nellore, Rajahmundry, Anakapalli and Rajendranagar sites of Andhra Pradesh, India. Recalibrated Blaney-Criddle (temperature based), Radiation (Radiation based) and Christiansen (Pan evaporation based) methods showed a satisfactory performance at the sites. Further, recalibrated Blaney- Criddle method showed relatively better performance than Radiation and Christiansen methods in the daily ET₀ estimation. Recalibrated Blaney- Criddle method may therefore be adopted at the sites selected for the present study and also at the sites with similar climatic conditions for satisfactory daily ET₀ estimation.     

An improved iterative finite element solution for pin joints

Accurate, reliable and economical methods of determining stress distributions are important for fastener joints. In the past the contact stress problems in these mechanically fastened joints using interference or push or clearance fit pins were solved using both inverse and iterative techniques. Inverse techniques were found to be most efficient, but at times inadequate in the presence of asymmetries. Iterative techniques based on the finite element method of analysis have wider applications, but they have the major drawbacks of being expensive and time-consuming. In this paper an improved finite element technique for iteration is presented to overcome these drawbacks. The improved iterative technique employs a frontal solver for elimination of variables not requiring iteration, by creation of a dummy element. This automatically results in a large reduction in computer time and in the size of the problem to be handled during iteration. Numerical results are compared with those available in the literature. The method is used to study an eccentrically located pin in a quasi-isotropic laminated plate under uniform tension.     

Behaviour of Al-Mg alloys at high temperature

The behaviour of a few Al-Mg alloys (up to 7.1 wt% Mg) has been studied on heating in air at 500°C for 8 h or more. The precipitation of a spinel phase, MgAl₂O₄, is found to take place on the surface and along the transverse section (depth) of the specimen. The alloys seem to be resistant to internal oxidation below 4.5% Mg and thereafter prone to it. Beryllium modification does not suppress the progress of internal oxidation taking place in the Al-Mg alloys. The results have been interpreted on the basis of anodized photomicrographs and X-ray diffraction data.     

Macro-to-micro porous special bioactive glass and ceftriaxone-sulbactam composite drug delivery system for treatment of chronic osteomyelitis: an investigation through in vitro and in vivo animal trial

A systematic and extensive approach incorporating in vitro and in vivo experimentation to treat chronic osteomyelitis in animal model were made using antibiotic loaded special bioactive glass porous scaffolds. After thorough characterization for porosity, distribution, surface charge, a novel drug composite were infiltrated by using vacuum infiltration and freeze-drying method which was subsequently analyzed by SEM-EDAX and studied for in vitro drug elution in PBS and SBF. Osteomyelitis in rabbit was induced by inoculation of Staphylococcus aureus and optimum drug-scaffold were checked for its efficacy over control and parenteral treated animals in terms of histopathology, radiology, in vivo drug concentration in bone and serum and implant-bone interface by SEM. It was optimized that 60P samples with 60-65% porosity (bimodal distribution of macro- to micropore) with average pore size ~60 μm and higher interconnectivity, moderately high antibiotic adsorption efficiency (~49%) was ideal. Results after 42 days showed antibiotic released higher than MIC against S. aureus compared to parenteral treatment (2 injections a day for 6 weeks). In vivo drug pharmacokinetics and SEM on bone-defect interface proved superiority of CFS loaded porous bioactive glass implants over parenteral group based on infection eradication and new bone formation.     

Electronic absorption spectrum of Cu2 ions doped in lithium ammonium sulphate crystal

Single crystals of Lithium Ammonium Sulphate doped with Cu²⁺ ions were grown by slow evaporation technique. Electronic absorption spectra have been recorded at room and liquid nitrogen temperatures on Cary-2390 spectrophotometer. The spectrum is characteristic of a Cu²⁺ ion in octahedral symmetry. From the magnitude and and relative position of the bands a successful interpretation of all the observed bands has been made. The crystal field and tetragonal field parameters are derived. The observed and calculated energies are in good agreement.     

A Reversible Data Hiding Scheme for Interpolated Images Based on Pixel Intensity Range

Multimedia Tools and Applications - In this paper, we propose a novel interpolation and a new reversible data hiding scheme for upscaling the original image and hiding secret data into the...     

Analysis and classification of malignancy in pancreatic magnetic resonance images using neural network techniques

Computer-aided diagnosis (CAD) is a computerized way of detecting tumors in MR images. Magnetic resonance imaging (MRI) has been generally used in the diagnosis and detection of pancreatic tumors. In a medical imaging system, soft tissue contrast and noninvasiveness are clear preferences of MRI. Inaccurate detection of tumor and long time consumption are the disadvantages of MRI. Computerized classifiers can greatly renew the diagnosis activity, in terms of both accuracy and time necessity by normal and abnormal images, automatically. This article presents an intelligent, automatic, accurate, and robust method to classify human pancreas MRI images as normal or abnormal in terms of pancreatic tumor. It represents the response of artificial neural network (ANN) and support vector machine (SVM) techniques for pancreatic tumor classification. For this, we extract features from MR images of pancreas using the GLCM method and select the best features using JAFER algorithm. These features are analyzed by five classification techniques: ANN BP, ANN RBF, SVM Linear, SVM Poly, and SVM RBF. We compare the results with benchmark data set of MR brain images. The analytical outcome presents that the two best features used to classify the MR images using ANN BP technique have 98% classification accuracy.     

Antenna Design: Micro Strip Patch for Spectrum Utilization in Cognitive Radio Networks

Wireless Personal Communications - A micro strip patch antenna with multiple parasitic patches for Cognitive Radio Network applications is presented to enhance the bandwidth. Multiple resonances...     

Sorption of Tertiary Butyl Mercaptan to Indoor Materials in Contact with Air or Water

This study reports sorption of the malodorant 2-methyl-2-propanethiol, commonly known as tertiary butyl mercaptan (TBM), to selected indoor materials. The phase distribution of TBM in gas-solid and aqueous-solid systems was evaluated using batch reactors. Sorbents used in the study included two carpets, two wallpapers, a soil, and granular activated carbon (GAC). Sorption was studied for gaseous and aqueous TBM concentrations spanning three orders of magnitude and contact times ranging from 1 to 28 days. The phase distribution data were plotted and fitted using linear and Freundlich relationships. Results indicated that all solids sorbed environmentally significant quantities of TBM, with the likelihood of producing concentrations above the odor threshold during subsequent remediation using mechanical ventilation. TBM retention by sorbents was greater from air than from water. The malodorant partitioned readily into wallpapers and slowly into the carpet materials. Sorption was nonlinear in the case of GAC and the nonlinearity appeared to increase with sorption contact time. GAC sorbed TBM strongly from both air and water.