湿化学法制备纳米ATO导电粉

采用非均相成核法 ,在Sn(OH) 4 晶种上均匀生长Sb掺杂Sn(OH) 4 ,制备纳米ATO粉末。以电阻测定系统研究了合成条件如掺杂浓度、反应温度、pH值、SnCl4浓度等对最终粉末电阻性能的影响。以TG DSC热分析、XRD、TEM等手段研究了晶粒生长过程 ,XRD显示为四方金红石型结构 ,平均粒径为15nm。当Sb/Sn(mol比 ) =0 .0 5 ,pH =2 ,T =60℃ ,SnCl4=1.2～ 1.8mol·L-1时 ,粉体电阻小于 0 .5Ω。     

KINETICS FOR LOW TEMPERATURE PYROLYSIS OF BLACK LIQUOR

A kinetic study of pyrolysis of dried black liquor was performed using a Netzsch 429 Thermogravimetric Analyzer. It was found that as conversion increases from 10 to 45% the apparent pyrolysis activation energy for black liquor increases from 77.20 to 112.74 KJ/mol. For black liquor the order of reaction was found to be first-order. The reaction rate constant was found to be 2.12×10⁹ min. These results are in agreement with the data reported by other investigators on biomass pyrolysis.     

Continuous Separation of Inclusions from Aluminum Melt Flowing in a Circular Pipe using a High Frequency Magnetic Field

The continuous separation of inclusions from aluminum melt flowing in a circular pipe using a high frequency magneticfield was investigated both theoretically and experimentally The separation efficiency was calculated based on thetrajectory method and compared with experimental results. It is found that the separation efficiency is a functilnondimensional parameters t_i·d_p~2B_e~2/μ_fμ_eα~2 and α/δ.The effective way to improve the separation efficiency is to increasethe effective magnetic flux density and decrease the pipe radius. and the value of α/δ should be kept about 2 in orderto obtain the optimum separation efficiency.     

反应结合氧化铝陶瓷制备新工艺

本文评述了反应结合氧化铝陶瓷的制备工艺原理，配料组成，研磨与原料细度，成形压力和升温速率等对陶瓷性能的影响。介绍了几种反应结合氧化铝陶瓷制造实例。     

用于一维图像识别的支撑矢量机方法

研究了支撑矢量机的分类机理,并利用支撑矢量机对雷达目标一维像进行了识别.识别的结果表明了该方法的优越性,并显示它可以对残缺不全的样本进行识别.     

大型钢制焊接双层低温储罐设计建造

介绍了大型钢制焊接双层低温储罐的结构形式、选材、建造、检验及保冷要求 ,结合所设计的低温液氨储罐 ,对设计建造这类储罐必须考虑的一些问题作了分析     

Adhesive Contact of a Membrane with a Hemispherical Indenter: Theoretical Analysis and Model Liquid System

The axisymmetric Laplace equation is solved numerically to extract contact-angle data for a flat liquid/vapor interface contacting a submerged hemispherical solid. The liquid/vapor interface is treated as a membrane, with a membrane tension equal to the surface energy of the liquid. By measuring the vertical displacement of the membrane and the projected contact area the membrane makes with the hemisphere, the contact angle and correspondingly the driving force for motion of the contact line can be measured. We show that characteristic receding and advancing contact angles can be obtained by measuring the contact radii formed upon initial contact between the interface and hemisphere and final contact just prior to detachment of the interface, respectively. Use of the technique is illustrated with a model experiment involving the contact of an air/water interface with a poly(methyl methacrylate) surface.     

The effect of partial substitution of nb for v on austenite grain size and hardness of a tool steel

In the present work, the composition of H- 13 tool steel was modified with respect to the vanadium content to include an addition of niobium to obtain improved austenite grain size control without altering the tempering response of the steel. Optical metallography and transmission electron microscopy (TEM) observation of extraction replicas showed that the new steel had a smaller austenite grain size and a finer carbide size distribution than the vanadium steel, which indicates a higher potential toughness.     

皇甫川流域水沙特性分析及其治理对策

作者对皇甫川流域从径流泥沙来源、水沙特性、水沙变化趋势等方面进行了较为深入地分析和研究，据此提出皇甫川流域近期治理方略是：以沟道坝系建设为切入点；积极推进林草植被建设；对砒砂岩地区实行大面积封禁治理。流域近期至2010年，治理的重点建议放在十里长川、沙圪堵至皇甫区间和沙圪堵以上的纳林川左岸。