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排序方式: 共有353条查询结果,搜索用时 15 毫秒
21.
22.
Investigation of miscibility and phase structure of a novel blend of poly(lactic acid) (PLA)/acrylic rubber (ACM) and its nanocomposite with nanosilica
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In this work, a novel polymer blend containing poly(lactic acid) (PLA) as a biocompatible and biodegradable thermoplastic and acrylic rubber (ACM) is prepared and the miscibility and phase structure of the blend and its nanocomposite (PLA/ACM/nanosilica) are investigated through theoretical and experimental methods. To predict the phase diagram of the blend, a compressible regular solution model was employed, in which an upper critical solution temperature was observed. The model predicted that PLA/ACM blends are immiscible over the whole composition range at temperatures below 260 °C. Performing scanning force microscopy on the blend showed phase separated structures for the blends containing different amounts of the PLA and ACM. This was in accordance with the results of dynamic mechanical analysis, which revealed two distinct glass transition temperatures for the studied blends. The effect of nanometer sized silica particle on morphology and rheological properties of these blends was also investigated. Scanning force microscopy results showed much reduction of droplet size in the blends containing 2 wt % nanosilica. This was attributed to the suppression effect of nanosilica on the droplets coalescences. Rheological measurements confirmed the interaction of both components with the silica nanofiller. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017 , 134, 45499. 相似文献
23.
Azam Tafreshi 《Engineering Analysis with Boundary Elements》2009,33(2):215-224
This paper presents the application of the boundary element method to the shape sensitivity analysis of two-dimensional composite structures in contact. A directly differentiated form of boundary integral equation with respect to geometric design variables is used to calculate shape design sensitivities for anisotropic materials with frictionless contact. The selected design variables are the coordinates of the boundary points either in the contact or non-contact area. Three example problems with anisotropic material properties are presented to validate the applications of this formulation. 相似文献
24.
The main objective of this paper was to study the effect of precipitation on the geological development of badlands in arid
regions. Field observations and laboratory investigations were carried out to characterize the surface soils of the Avonlea
badlands in southern Saskatchewan, Canada, which is currently experiencing a rapid development in infrastructure. Three distinct
surface sediments were identified: an upper slope of cemented sandstone, a mid-slope on weathered mudrock and a relatively
flat basal pediment. Each of these soils reacts differently to rainfall events. Precipitation results in grain size reduction
which, together with the consistency limits, explains the water sensitivity of the soils; the fines increased by 16% in the
cemented sandstone, 78% in the weathered mudrock and 33% in the basal pediment. Erosion susceptibility was highest in the
basal pediment (2% clays) followed by cemented sandstone (cementation by 6% active clays) and then by weathered mudrock (cohesion
due to the 40% clay). 相似文献
25.
DOE applied to multi-response optimisation study on performance,combustion and emission characteristics of a VCR diesel engine 总被引:1,自引:0,他引:1
Syed Azam Pasha Quadri M. Masood Tabish Wahidi Mohd Ghouse Sundkey Mohd Wajid 《国际自然能源杂志》2017,38(8):759-764
There are various parameters which may influence the IC engine performance. The trial and error method is a technique used to identify the best parameters. However, this method demands extensive experimental work and results in a great waste of time and resources. Thus, the design of experiments (DOEs) developed by Taguchi is employed. The multi-responses which need to be maximised are brake thermal efficiency, mechanical efficiency, cylinder pressure and cumulative heat release rate, whereas the responses which are to be minimised are specific fuel consumption, oxides of nitrogen and carbon monoxide. In the present study, an optimised DOE(L9) orthogonal array based on the Taguchi statistical method was formulated and a series of experiments were conducted under controlled supervision by considering three different injection operating pressures (IOPs) (200, 220 and 240 bar) and three different compression ratios (CRs) (16.5, 17.5 and 18.5). The main objective of this paper is to find the best suited IOP and CR values which obtain higher performance, better combustion and lower emissions. 相似文献
26.
Delmar-Greenberg D Azam Ali M Gonsalves KE 《Journal of materials science. Materials in medicine》2003,14(10):833-841
The aim of this study is to design an effective hydrogel, which has good potential for application in the field of tissue regeneration. Ultimately, the polymeric biomaterial will be used as a bottom, non-cell adhering layer of a polymeric scaffold, which will inhibit the adhesion and proliferation of fibroblast cells. A series of terpolymer hydrogels were prepared from MMA/HPOEM/MePOEM monomers based on varying formulations. The gels were polymerized via free radical polymerization under UV and characterized by TGA, DSC and FTIR studies. Furthermore, the double bond conversion, gel content and swelling properties of the polymer were analyzed and correlated to its crosslinking density, which revealed details about the hydrogels character. Finally, cell culture experiments were used to compare the UV-cured polymer to its thermally derived non-functionalized polymer of the same formulation. Inverted optical microscopy was used to demonstrate cell-resistance of both materials with respect to a control Tissue Culture PolyStyrene plate. ©2003 Kluwer Acadamic Publishers 相似文献
27.
Azam Sobhani Masoud Salavati-Niasari 《Journal of Materials Science: Materials in Electronics》2016,27(4):3271-3280
In this article, the synthesis and characterization of Co2P/Co nanocomposites are reported. Three kinds of precursors are studied: bis(salicylidene)cobalt(II) [Co(sal)2], bis(salicylate)cobalt(II) [Co(Hsal)2] and cobalt oxalate [Co(O4C2)·4H2O]. The cobalt(II) acetate tetrahydrate Co(CH3COO)2·4H2O is used as reference. The nanocomposites are prepared by thermal decomposition method using triphenylphosphine as a surfactant solvent and phosphorus precursor. A possible mechanism of the formation of the nanocomposites is put forward to explain the experimental observations. This is the first time that Co2P/Co nanocomposites are synthesized. To study the crystalline structure, composition, size, morphology and magnetic property of the products, characterization techniques including XRD, SEM, TEM, FT-IR and VSM are employed. 相似文献
28.
Metallic nickel (Ni) was successfully dispersed onto a polyaniline (PANI) matrix by a simple one‐step electrochemical method. Ni particles as deposited onto the polymer seemed to be much smaller compared to those deposited onto bare Pt. The size of the Ni deposits was found to be influenced by the electrolytic bath composition and potential sweep rate. The PANI matrix thus dispersed with Ni particles exhibited ferromagnetic behavior and a lower electrical conductance. The decrease in conductivity may be attributed to the partial blockage of the conductive path by the Ni particles thus embedded in the polymer matrix. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 321–327, 2006 相似文献
29.
Attempts have been made to use different amount of ground tire rubber (GTR) powder as a partial substitute for natural rubber (NR) in thermoplastic elastomer based on linear low‐density polyethylene (LLDPE, 60 wt%) and NR (40wt%). Maleic anhydride (MA) and dicumyl peroxide (DCP) were used, during melt mixing of the compound, to modify GTR and vulcanize the rubber phases of the blends. Morphology of the blends was studied by scanning electron microscopy and rheological behavior investigated through rheomechanical spectroscopy. Mechanical properties of the blends were also measured, and the effect of GTR concentration on properties was evaluated. Obtained results showed that modification of GTR with MA and using DCP in the blends containing GTR improves the bonding between GTR and matrix. This leads to a distinctive rheological behavior and enhances tensile strength and elongation at break compared to its corresponding simple blend. It can be said that using of MA and DCP during melt mixing of thermoplastic elastomers based on LLDPE/NR containing GTR, concludes to a better dispersion of GTR and formation of morphology similar to that of a dynamic vulcanized thermoplastic elastomer, which improves interfacial bonding between phases and causes a dramatically increase in mechanical properties. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 相似文献
30.
S. Azam 《Bulletin of Engineering Geology and the Environment》2000,59(3):211-217
The geological, climatic and environmental conditions have resulted in the formation of calcareous deposits along the Arabian
Gulf coast. Anhydrous calcium sulphate, which commonly occurs in such soils, is notorious for gypsification and dissolution
and adds to the potential hazards of indigenous sediments. This paper discusses the properties of the sediments and the compressibility
of the calcareous soil formations of eastern Saudi Arabia.
Received: 24 June 1999 · Accepted: 26 November 1999 相似文献