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排序方式: 共有10000条查询结果,搜索用时 312 毫秒
921.
J. M. Zaldivar E. Molga M. A. Al s H. Hern ndez K. R. Westerterp 《Chemical Engineering and Processing: Process Intensification》1995,34(6):543-559
Aromatic nitrations by mixed acid have been selected as a specific case of a heterogeneous liquid-liquid reaction. An extensive experimental programme has been followed using adiabatic and heat-flow calorimetry and pilot reactor experiments, supported by chemical analysis. A series of nitration experiments has been carried out to study the influences of different initial and operating conditions such as temperature, stirring speed and sulphuric acid concentration. In parallel, a mathematical model to predict the overall conversion rate has been developed. In this paper the mathematical modelling and the implementation and experimental validation for benzene, toluene and chlorobenzene mononitration in the kinetic control regime (slow liquid-liquid reaction) are presented and discussed. 相似文献
922.
923.
924.
The optical method of caustics has been utilised to measure both the stress intensity factor for a crack lying along the interface of an aluminium/epoxy bimaterial specimen, and the mode mixity arising from the difference in the elastic properties across the interface. Measurements were carried out by using a novel modification to the method whereby caustics are produced and measured from both sides of the specimen, so compensating automatically for the distortion induced in the specimen due to misaligned loading fixtures. A flat reflective surface across the interface was obtained by adhering a reflective coating to the specimen. Verification that this coating does not affect measurement accuracy was obtained by comparing stress intensity factors measured from coated and uncoated monolithic aluminium specimens where good agreement was found to exist between both measurements. 相似文献
925.
A limited selection of samples of small and medium size air-conditioning equipment being marketed or manufactured in Kuwait was tested in an internationally reputed laboratory. The actual performance results obtained from laboratory tests were analyzed and compared with the commercially available information from the manufacturers for the same selected units. The analysis indicated the quality of air-conditioning equipment available to the Kuwaiti user. 相似文献
926.
927.
928.
Rate (n -1)/n punctured convolutional codes are very effective in conjunction with embedded differential pulse code modulation (EDPCM) in variable-bit-rate speech transmission. The authors investigate the performance of this variable-bit-rate EDPCM system in terms of probability of bit error and audio signal-to-noise ratio (SNR) versus channel SNR in an additive white Gaussian noise and Rayleigh fading channel using soft-decision decoding for specific sets of code generators of punctured convolutional codes. The results show that different sets of code generators affect the performance in terms of both the probability of bit error and the audio SNR. Improvements were obtained in the cases of Gaussian nonfading and Rayleigh fading channels using soft-decision decoding 相似文献
929.
H. Hou J. C. Holste
B. E. Gammon
K. N. Marsh 《International Journal of Refrigeration》1992,15(6):365-371This paper reports densities of compressed R134a (1,1,1,2-tetrafluoroethane) determined by using a contiuously weighed pycnometer at 20 K intervals between 180 and 380 K at pressures from slightly greater than the vapour pressure to 70 MPa. The results are accurate to within ±0.1%. Saturated liquid densities derived by extrapolation from the experimental values agree with other reported values to within ±0.3%. 相似文献
930.
I. Kashif H. Farouk S. A. Aly A. M. Sanad M. H. El-Kottamy E. E. Assem 《Journal of Materials Science: Materials in Electronics》1992,3(3):144-146
The effect of the addition of Fe2O3 and heat treatment duration on the magnetic susceptibility of vanadium borophosphate glass were studied. The magnetic susceptibility of glass samples was found to increase with increasing Fe2O3 content, which may be explained by the formation of the FeO6 group and the change of Fe2+ to Fe3+ which has higher paramagnetic properties. No detectable changes in the magnetic susceptibility with heat treatment for the samples containing 0.0, 0.5 and 1.0 mol% Fe2O3 was observed. The magnetic susceptibility for the heat treated samples containing 2.5, 5.0 and 7.5 mol% Fe2O3 decreases sharply with increasing duration of heat treatment up to 6 h and then remains almost constant. The sharp decrease in magnetic susceptibility of 2.5 mol% Fe2O3 is attributed to the increase in the number of ferrous ions. The sharp decrease for samples containing 5.0 and 7.5 mol% Fe2O3 is attributed to the increase in the number of Fe3+ in tetrahedral co-ordination. The rate of crystallization owing to the heat treatment was calculated and was found to increase with increasing iron oxide content. The geometry of crystallization was found to be in three-, two-and one-dimension(s) for samples containing 2.5, 5.0 and 7.5 mol% Fe2O3, respectively. 相似文献