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排序方式: 共有684条查询结果,搜索用时 656 毫秒
61.
Seema Verma S. D. Pradhan Renu Pasricha S. R. Sainkar P. A. Joy 《Journal of the American Ceramic Society》2005,88(9):2597-2599
Nanosized NiZn ferrite powder is synthesized by a low-temperature method, using a unique combination of citric acid and glycine. An appropriate molar ratio of both citric acid and glycine offers a low-temperature synthetic route by incorporating the complexation behavior of citric acid and the combustion nature of glycine. Thermal decomposition/controlled autocatalytic combustion of the composite gel occurs at a low temperature of around 175°C, with the evolution of a large amount of gases. Transmission electron microscopic studies showed that the average particle size of the ferrite obtained is ∼2.5 nm, with a narrow size distribution. Uniformly distributed fine-grained microstructure with low porosity is obtained for a sample sintered at 1000°C. 相似文献
62.
Epoxidation of Canola Oil with Hydrogen Peroxide Catalyzed by Acidic Ion Exchange Resin 总被引:2,自引:0,他引:2
Rubeena Mungroo Narayan C. Pradhan Vaibhav V. Goud Ajay K. Dalai 《Journal of the American Oil Chemists' Society》2008,85(9):887-896
Canola oil with an iodine value of 112/100 g, and containing 60% oleic acid and 20% linoleic acid, was epoxidised using a
peroxyacid generated in situ from hydrogen peroxide and a carboxylic acid (acetic or formic acid) in the presence of an acidic
ion exchange resin (AIER), Amberlite IR 120H. Acetic acid was found to be a better oxygen carrier than formic acid, as it
produced about 10% more conversion of ethylenic unsaturation to oxirane than that produced by formic acid under otherwise
identical conditions. A detailed process developmental study was then performed with the acetic acid/AIER combination. The
parameters optimised were temperature (65 °C), acetic acid to ethylenic unsaturation molar ratio (0.5), hydrogen peroxide
to ethylenic unsaturation molar ratio (1.5), and AIER loading (22%). An iodine conversion of 88.4% and a relative conversion
to oxirane of 90% were obtained at the optimum reaction conditions. The heterogeneous catalyst, AIER, was found to be reusable
and exhibited a negligible loss in activity. 相似文献
63.
64.
Removal of p-nitrophenol using hydrodynamic cavitation and Fenton chemistry at pilot scale operation
Amey A. Pradhan Parag R. Gogate 《Chemical engineering journal (Lausanne, Switzerland : 1996)》2010,156(1):77-82
In the current work removal of p-nitrophenol has been investigated using hydrodynamic cavitation, either operated individually or in combination with H2O2 and conventional Fenton process. In hydrodynamic cavitation, two different cavitating devices viz. orifice plate and venturi have been used. Effect of different operating parameters such as initial concentration (5 g/l and 10 g/l), inlet pressure (over a range 5.7–42.6 psi) and pH (over a range 2–8) on the extent of removal has been investigated. In conventional Fenton process two loadings of FeSO4, 0.5 g/l and 1 g/l were investigated and three ratios of FeSO4:H2O2 viz. 1:5, 1:7.5 and 1:10 were used. Removal observed with venturi was higher than with orifice plate in combination with Fenton chemistry. For 5 g/l initial concentration of p-nitrophenol, maximum removal of 63.2% was observed whereas for 10 g/l solution it was 56.2%. 相似文献
65.
66.
Debabrata Pradhan Akshya Kumar Guin Pankaj Raju Manindra Manna Monojit Dutta T. Venugopalan 《Journal of Materials Engineering and Performance》2014,23(9):3336-3346
Galvannealed steel sheets (GA) have become the mainstream steel sheet for automobile applications because of their superior corrosion resistance, paintability, and weldability. To impart specific properties, different coatings on GA steel sheet were reported to improve properties further. In this context, we have developed an electroplating process (flash coating) for bright and adherent Fe-Zn alloy coating on GA steel sheet to enhance performances such as weldability, frictional behavior, phosphatability, and defect coverage. A comparative study with bare GA steel sheet was carried out for better elastration. The electroplating time was reduced below 10 s for practical applicability in an industrial coating line by modulating the bath composition. Electroplating was performed at current density of 200-500 A/m2 which yielded with higher cathode current efficiency of 85-95%. The performance results show that Fe-10 wt.% Zn-coated GA steel sheet (coating time 7 s) has better spot weldability, lower dynamic coefficient of friction (0.06-0.07 in lubrication), and better corrosion resistance compared to bare GA steel sheet. Uniform phosphate coating with globular crystal size of 2-5 µm was obtained on Fe-Zn flash-coated GA steel sheet. Hopeite was the main phosphate compound (77.9 wt.%) identified along with spencerite (13.6 wt.%) and phosphophyllite (8.5 wt.%). 相似文献
67.
Subir Kr. Bhandari Siddhartha Mandal Santanu Pradhan Biswajit Ghosh 《Sequential Analysis》2013,32(3):394-405
Abstract In this article on sequential adaptive testing, we have studied the optimal allocation between two populations for testing a composite hypothesis involving the parameters, with the goal of decreasing allocation of one of the treatments to the order of the logarithm of the sample size while decreasing the probability of incorrect selection to zero. We have proved the result for large sample sizes both mathematically and by simulation studies. 相似文献
68.
Keka Ojha Narayan C Pradhan Amar Nath Samanta 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2006,81(4):659-666
The alkylation of phenol with tert‐butyl alcohol was carried out in a continuous flow reactor over a catalyst synthesized from fly ash. The activity of the synthesized catalyst was compared with those of other conventional zeolite catalysts such as 13X (NaX) and Hβ. Of all the catalysts tested, zeolite Hβ showed the highest activity in phenol conversion followed by the synthesized zeolite (HZOP‐31). The activity of commercial 13X zeolite was found to be same as that of HZOP‐31. Ce‐exchanged catalyst (CeZOP‐31) showed even better performance than 13X in the alkylation of phenol. The effects of different parameters such as reactant mole ratio, temperature and space velocity on phenol conversion and tert‐butyl phenol selectivity were studied. The effect of mass transfer resistance was found to be negligible within the feed rate range and particle size range studied. The apparent activation energy for the reaction of tert‐butyl alcohol over HZOP‐31 was determined as 30.1 kJ mol?1. Copyright © 2006 Society of Chemical Industry 相似文献
69.
M.M. Mahapatra G.L. Datta B. Pradhan N.R. Mandal 《International Journal of Pressure Vessels and Piping》2006
Achieving adequate top and bottom reinforcement is important to minimize angular distortions in single-pass submerged arc welded (SAW) butt joints. This is achieved in the present work by using a reusable flux-filled backing strip and proper SAW process parameters without resorting to costly distortion mitigation techniques. The butt joints were made without edge (square butts) preparation. The process was also modeled by using three-dimensional finite element analysis by incorporating the top and bottom reinforcements into the modeling. Filler material deposition was also simulated. Temperature distributions and angular distortions obtained from the modeling closely matched with the experimental values. Thus, the cost effective experimental methodology established in the present work can be utilized for minimizing angular distortions in SAW square butts. The modeling methodology adopted can be used for predicting the angular distortions in SAW square butts with top and bottom reinforcements. 相似文献
70.
We tackle the problem of efficient layered or multiresolution (MR) data transmission over multicarrier modulation (MCM) systems. We treat the source as being characterized by multiple layers of importance, i.e., having different bit error rate (BER) requirements. First we consider the MCM systems in a multiresolution framework using multiplexing techniques. Then we present the idea of embedded multicarrier modulation (E-MCM) as an effective way of achieving this, and introduce a fast table-lookup-based power allocation algorithm that optimizes the multicarrier constellation design in terms of maximizing the deliverable throughput bit-rate, subject to a total power constraint. Simulation results of our E-MCM system reveal substantial gains (up to about 25%) in deliverable bit-rates over optimized time-division-multiplexed-based designs 相似文献