Spark Plasma Sintering of Nanostructured Aluminum: Influence of Tooling Material on Microstructure

The influence of tooling material, i.e., graphite and WC-Co, on the microstructure of a spark plasma sintering (SPS) consolidated, nanostructured aluminum alloy is studied in this paper. The results show that tooling selection influences microstructure evolution, independent of process parameters. The influence of tooling on microstructure is rationalized on the basis of the following factors: heating rate, electrical current density, localized heating, and imposed pressure. A theoretic framework, based on the physical properties of graphite and WC-Co, is formulated to explain the observed behavior.     

云环境驱动全新安全方法

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AC-coupled front-end for biopotential measurements

AC coupling is essential in biopotential measurements. Electrode offset potentials can be several orders of magnitude larger than the amplitudes of the biological signals of interest, thus limiting the admissible gain of a dc-coupled front end to prevent amplifier saturation. A high-gain input stage needs ac input coupling. This can be achieved by series capacitors, but in order to provide a bias path, grounded resistors are usually included, which degrade the common mode rejection ratio (CMRR). This paper proposes a novel balanced input ac-coupling network that provides a bias path without any connection to ground, thus resulting in a high CMRR. The circuit being passive, it does not limit the differential dc input voltage. Furthermore, differential signals are ac coupled, whereas common-mode voltages are dc coupled, thus allowing the closed-loop control of the dc common mode voltage by means of a driven-right-leg circuit. This makes the circuit compatible with common-mode dc shifting strategies intended for single-supply biopotential amplifiers. The proposed circuit allows the implementation of high-gain biopotential amplifiers with a reduced number of parts, thus resulting in low power consumption. An electrocardiogram amplifier built according to the proposed design achieves a CMRR of 123 dB at 50 Hz.     

Influence of sulfur and Mn/S ratio on the hot ductility of steels during continuous casting

The influence of S and (Mn/S) on the crack susceptibility of continuous casting steels was studied. It is theoretically demonstrated that there is a critical value of the (Mn/S) ratio, (Mn/S)_c, under which a high susceptibility to cracking, during casting or deformation of as-cast material, is expected. The value of (Mn/S)_c increases as the S content of the steel decreases. Based on literature data and results from rolling continuous casting billets the following experimental equation has been found: (Mn/S)_c = 1.345 · S^?0.7934. A high similarity between this experimental equation and the theoretical one is achieved. A comparison between the equation found and previous expressions from literature was carried out. The MSC index as the ratio between the (Mn/S) ratio of a steel and the corresponding critical one was defined. The MSC index is a useful tool for the analysis of experimental results from literature.     

The syntactic role of pauses in the speech of schizophrenic patients with alogia.

Examined the relation between alogia and pausing. The authors analyzed the flow of speech of 17 male schizophrenic patients during an interview, particularly the pauses that occurred within and between syntactic clauses and those that occurred as the turn switched from the interviewer's question to the patient's response. The strongest predictor of alogia ratings was the duration of switching pauses; the frequency of long within-clause pauses was also significantly related to alogia, but the frequency of between-clause pauses showed a trend toward a negative relation with alogia. Words following within-clause pauses were more likely to be content words than function words, and the content words were less frequent in the English language than the speaker's other words. This suggests that alogic patients have difficulty in word finding and in thought formulation, as well as a general increase in the duration of all pauses. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

On the behavior of microstructures with multiple length scales

The current study aims to provide fundamental insight into the behavior of microstructures containing grain sizes that span multiple length scales. A commercial 5083 Al alloy was selected as the material of interest to facilitate comparison with recently published data. The materials studied here were prepared via the thermal consolidation of powders that were cryomilled for different times (i.e., 0, 2, 4, and 8 hours). Following consolidation, the resultant microstructure was characterized by an equiaxed grain morphology with a size distribution centered around 200∼300 nm. Dispersed among the 200- to 300-nm grains were coarse-grained regions or ligaments with a grain size ranging from 600 nm to 2 μm. The occurrence of coarse-grained regions is rationalized on the basis of recrystallization or subgrain coarsening, whereas the occurrence of equiaxed fine regions is proposed to be a result of continuous grain growth. Two types of microstructures were selected for study, containing coarse-grained volumes of approximately 28 pct and 43 pct that corresponded to an ultimate tensile strength (UTS) of 566 MPa and 535 MPa, and a fracture strain of 3.2 pct and 3.5 pct, respectively. The observed ductility and the relevant toughening mechanisms were discussed in light of the presence of multiple length scales.     

Thermal stability in bulk cryomilled ultrafine-grained 5083 Al alloy

Thermal stability in bulk ultrafine-grained (UFG) 5083 Al that was processed by gas atomization followed by cryomilling, consolidation, and extrusion, and that exhibited an average grain size of 305 nm, was investigated in the temperature range of 473 to 673 K (0.55 to 0.79 T _m , where T _m is the melting temperature of the material) for different annealing times. Appreciable grain growth was observed at temperatures > 573 K, whereas there was limited grain growth at temperatures < 573 K even after long annealing times. The values of the grain growth exponent, n, deduced from the grain growth data were higher than the value of 2 predicted from elementary grain growth theories. The discrepancy was attributed to the operation of strong pinning forces on boundaries during the annealing treatment. An examination of the microstructure of the alloy suggests that the origin of the pinning forces is most likely related to the presence of dispersion particles, which are mostly introduced during cryomilling. Two-grain growth regimes were identified: the low-temperature region (<573 K) and the high-temperature region (>573 K). For temperatures lower than 573 K, the activation energy of 25 ± 5 kJ/mol was determined. It is suggested that this low activation energy represents the energy for the reordering of grain boundaries in the UFG material. For temperatures higher than 573 K, an activation energy of 124 ± 5 kJ/mol was measured. This value of activation energy, 124 ± 5 kJ/mol, lies between that for grain boundary diffusion and lattice diffusion in analogous aluminum polycrystalline systems. The results show that the strength and ductility of bulk UFG 5083 Al, as obtained from tensile tests, correlate well with substructural changes introduced in the alloy by the annealing treatment.     

The transient to steady-state transition during the spray-rolling process

From the geometrical standpoint, this article presents a qualitative theoretical analysis and prediction of the transient to steady-state transition during the spray-rolling process, a novel manufacturing technique for aluminum strips. The analytical results indicate that, when the deposited materials at the specific points on one roll surface overlap their counterparts on the other roll surface, spray rolling transits from the transient state to the steady state. The specific points are the limiting deposition positions of the atomized droplets on the roll surface initially.     

Role of Bioflocculation on Chemical Oxygen Demand Removal in Solids Contact Chamber of Trickling Filter/Solids Contact Process

The trickling filter/solids contact (TF/SC) process was developed in the late 1970s to improve the quality of the final effluent from existing trickling filter plants, to be able to meet stricter Environmental Protection Agency effluent requirements. Although this process has successfully achieved this objective, it is still not completely understood, there is limited information regarding the flocculation phenomena occurring in the solids contact chamber (SCC), and no information could be found on the relationship between flocculation and organic matter removal kinetics. To better understand the kinetics of biological flocculation in a continuous flow SCC, a long-term experimental program was conducted using a TF/SC pilot plant constructed at the Marrero, La., wastewater treatment plant. This program started in January 1998 and has continued through date. The present article will focus on two major areas: (1) the kinetics of bioflocculation in the SCC; and (2) effect of bioflocculation on chemical oxygen demand (COD) removal. Analysis of the wastewater composition revealed that, on the average, only 18.7% of the total COD in the SCC influent is truly dissolved. Therefore, most of the total COD removal observed in the SCC must be due to a physical process, such as flocculation. The experimental data confirmed that flocculation of the particulate COD contained in the trickling filter effluent explains the high total COD removal observed at the SCC. Both total and colloidal COD removals are well explained by the first-order flocculation model.