Structure and properties of CE/CTBN/EP blends: II. Effect of EP on the mechanical properties and thermostability of the CE/CTBN system

Carboxyl‐terminated butadiene‐acrylonitrile rubber (CTBN) has often been used to improve the toughness of cyanate ester (CE) resin while sacrificing modulus and thermostability. In this paper, the addition of the appropriate amount of epoxy resin (EP) to the CE/CTBN system is shown to not only increase the modulus and thermostability of the blend, but also improve the toughness. The values of impact strength showed a maximum for the CE/CTBN/EP 100/5/5 blend. The temperature of 10 % weight loss (T₁₀) improves from 376 °C for CE/CTBN 100/5 to 407 °C for the CE/CTBN/EP 100/5/2.5 blend. It is proposed that addition of the appropriate amount of EP can decrease the mobility and increase the stability of CTBN via the reaction between the terminal carboxyl group of CTBN and the hydroxyl group of EP. But a very high EP concentration will decrease the crosslinking density of CE, consequently reducing the mechanical properties and thermostability of the blends. Copyright © 2004 Society of Chemical Industry     

常用小水电工程地面控制测量方法

测量工作在小水电工程建设中起着重要的作用。小水电工程按其布置的方式分为堤坝式、引水式和混合式三种。堤坝式电站的测量工作比较简单,而引水式和混合式电站是高水头式,这类电站传统的地面控制测量方法是建立小三角网,但目前由于GPS和全站仪的全面普及,传统的小三角网控制已完全被GPS测量或与EDM导线结合的方法所代替。文章着重介绍引水式或混合式高水头小水电工程的地面控制测量。     

MIL-STD-1553B总线测试仪软件开发

充分利用1553B总线和USB总线的特点,研制了一种USB总线接口的MIL-STD-1553B总线测试仪,该测试仪通过USB总线来控制1553B总线,使得计算机通过USB总线便可与各种1553B总线的设备进行数据通信,从而使得1553B总线测试更加方便快捷.文中介绍了测试仪的软硬件系统结构,详细讨论了测试仪通用驱动程序和应用程序的体系结构、开发中使用的数据结构,以及应用程序的函数接口和开发流程,最后给出软件测试方法.     

狭小场地条件下大跨度预应力混凝土拱板的运输及吊装

介绍了大跨度预应力混凝土拱板在狭小场地条件下的起模、运输及空间滑移吊装的方法，经在众多中直粮库中的应用，证明该方法简单、适用、经济。     

The Effect of the Estimation on Goodness‐of‐Fit Tests in Time Series Models

Abstract. We analyze, by simulation, the finite‐sample properties of goodness‐of‐fit tests based on residual autocorrelation coefficients (simple and partial) obtained using different estimators frequently used in the analysis of autoregressive moving‐average time‐series models. The estimators considered are unconditional least squares, maximum likelihood and conditional least squares. The results suggest that although the tests based on these estimators are asymptotically equivalent for particular models and parameter values, their sampling properties for samples of the size commonly found in economic applications can differ substantially, because of differences in both finite‐sample estimation efficiencies and residual regeneration methods.     

Preparation and photochromism of nanocomposite thin film based on polyoxometalate and polyethyleneglycol

A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism.     

DSP技术在声强测试系统中的应用

根据声强测试过程中对数据处理系统的需求,提出了以数字信号处理器(DSP)TMS320C5409与A/D转换器芯片MAX125为核心构建高速多通道声强数据采集处理系统的方案,并结合它们的特点对该方案进行了论证.同时,详细介绍了TMS320C5409与MAX125之间的硬件接口电路的设计和软件编程的方法.实验表明,该数据采集处理系统具有速度快、可靠性高、结构简单等特点,满足声强测试过程的技术要求.     

自适应传输速率MAC层协议的探讨

随着无线通信技术的发展和器件性能的提高,无线网络有能力支持更高的数据传输速率.随之而来的问题是如何提高网络的性能,即根据无线信道的状况而自适应地改变传输参数.文中讨论了媒体访问控制(MAC)层协议上多跳无线网络自适应传输速率的技术方案.该方案运用自适应调制和编码技术,可以最大限度地利用信道的容量,根据不同终端报告的信道情况提供个性的调制与编码选择;对位置较好的用户提供高速率的数据服务,增加系统的吞吐率;并且由于信道的自适应是通过改变调制和编码的方式,而不是像功率控制那样改变发射功率,因此系统中干扰变化很小.     

改革组织结构实现科学管理

介绍了现代企业的组织结构的类型与阶段，提出可为国有企业改革可借鉴的经验。