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81.
Experimental evidence of concurrent compositional and structural instabilities leading to ω precipitation in titanium-molybdenum alloys 总被引:1,自引:0,他引:1
A. DevarajS. Nag R. SrinivasanR.E.A. Williams S. BanerjeeR. Banerjee H.L. Fraser 《Acta Materialia》2012,60(2):596-609
The ω phase is commonly observed in many commercial β or near-β titanium alloys on rapidly cooling from the single β phase field and also during subsequent isothermal annealing. However, the crystallographic formation mechanism for the ω particles is hitherto unclear/under discussion. The present study primarily focuses on ω precipitation within the β (body-centered cubic (bcc)) matrix of simple model binary titanium-molybdenum (Ti-Mo) alloys. It provides direct experimental evidence of the formation of ω-like embryos from competing compositional and structural instabilities arising in the bcc lattice of Ti-Mo alloys during rapid cooling from the high-temperature single β phase field. The displacive partial collapse of the {1 1 1} planes of the parent bcc structure within compositionally phase-separated regions containing several at.% less of Mo, forming ω-like embryos, has been conclusively shown by coupling aberration-corrected high-resolution scanning transmission electron microscopy with atom probe tomography observations. Growth and coarsening of these ω-like embryos take place during subsequent isothermal annealing, accompanied with both a completion of the collapse of the {1 1 1} β planes leading to a fully developed ω structure as well as rejection of Mo from these precipitates, resulting in near-equilibrium compositions. 相似文献
82.
The Cr:Fe ratio (chromium-to-iron mass ratio) of chromite affects the production of chrome-based ferroalloys. Although the lit-erature contains numerous reports related to the magnetic separation of di... 相似文献
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Ashish Nadar Atindra Mohan Banerjee M.R. Pai R.V. Pai Sher Singh Meena R. Tewari A.K. Tripathi 《International Journal of Hydrogen Energy》2018,43(1):37-52
Supported iron oxides have been established as an important class of catalyst for high temperature sulfuric acid decomposition. With an objective to elucidate the role of support in modifying the overall catalytic properties of dispersed iron oxide catalysts, a series of supported iron oxide based catalysts, Fe2O3 (15 wt%)/MO2 (M = Zr, Ce, Ti and Si), synthesized by adsorption-equilibrium method, is investigated for sulfuric acid decomposition reaction. The structure of dispersed iron oxide phases largely depended on the nature of the support oxide as revealed by the XRD and Mössbauer studies. α-Fe2O3 is found to be present as a major phase on ZrO2 and CeO2 support while ε-Fe2O3 was the major phase on silica supported iron oxide. On the other hand, presence of mixed oxide Fe2TiO5 was revealed over TiO2 support. Strong dispersed metal oxide-support interactions inhibited the total reduction of the dispersed phase on SiO2 and TiO2 as compared to complete reduction of dispersed iron oxide on CeO2 and ZrO2 supports during temperature programmed reduction upto 1000 °C. The order of catalytic activity at a temperature of ~750 °C is observed as Fe2O3/SiO2 > Fe2TiO5/TiO2 > Fe2O3/ZrO2 > Fe2O3/CeO2, while at higher temperatures of ~900 °C the SO2 yield is found to be comparable for all catalysts. A relationship between the rate of sulfate decomposition and catalytic activity is established through detailed TG-DTA investigations of sulfated catalyst and support. Considerable influence of the support oxide on the composition, structure, redox properties, morphology and catalytic activities of the active iron oxide dispersed phase has been observed. Thus, the support oxides operate as a critical component in the complex supported metal oxide catalysts and these findings might influence the design and development of future high temperature sulfuric acid decomposition catalysts. 相似文献
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A Combinatorial Approach for Assessing the Magnetic Properties of High Entropy Alloys: Role of Cr in AlCoxCr1–xFeNi
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Debasis Das Adhikary Goutam Kumar Bose Dipak Kumar Jana Dipankar Bose Souren Mitra 《Quality Engineering》2016,28(3):352-357
This article presents a multi-objective (maximization of availability and minimization of maintenance cost) preventive maintenance (PM) scheduling model for a continuous operating series system (COSS) which do not provide an off-working period for PM. The objective functions are optimized by using a Multi-Objective Genetic Algorithm (MOGA). The effectiveness of the model is demonstrated through a coal-fired boiler-tube. The case study shows that the model can improve the availability along with profound reduction of the maintenance cost, i.e., increases the profit of the plant. 相似文献
90.
Atindra Mohan Bandyopadhyay Aritra Acharyya J. P. Banerjee 《Journal of Computational Electronics》2014,13(3):769-777
A large-signal method based on non-sinusoidal voltage excitation model is used to study the DC and RF characteristics of Double Avalanche Region (DAR) Silicon Transit Time diode. A large-signal simulation program based on drift-diffusion model is developed for this study. The simulation results show the existence of several distinct negative conductance bands in the admittance characteristics separated by positive conductance. Thus the DAR device is capable of delivering RF power not only at the design frequency but also at several frequency bands higher than the design frequency band in the mm-wave regime. A comparative study with DDR Si device designed to deliver RF power at a particular mm-wave frequency band shows that DAR Si device is capable of delivering significantly higher RF power not only at the designed mm-wave frequency band, but also at higher frequency bands. 相似文献