压入深度与膜厚对薄膜与基体复合硬度及弹性模量的影响

根据高华建的复合弹性模量模型，提出了用一个测点的载荷-位移曲线计算整个压入深度内薄膜和基体复合硬度分布的方法，探讨了压入深度与膜厚对硬度与弹性模量测量值的影响，指出可由膜-基复合性能反推膜本身的性能。     

双金属盘式制动器的试制与研究

汽车工业的发展对刹车系统的关键零部件——刹车盘的抗冲击韧性提出了更高的要求。研究结果表明，把灰铸铁(HT250)与用优质碳素结构钢25Mn预先冲压成型的钢件镶铸在一起制成的1种新型刹车盘，既具有灰铸铁良好的抗磨、减震、尺寸稳定等性能，又具有较高的抗冲击韧性，能够满足汽车工业高速化、轻量化对刹车盘的综合要求。     

Al-Pb-Si-Sn-Cu轴瓦合金的微观结构及特征

采用机械合金化、冷压与热挤压法制备了Al-15％Pb-4％Si—1％Sn—1．5％Cu(质量分数，％)轴瓦合金。试验结果表明，块体材料的组织分布很均匀。Pb粒子细小均匀弥散分布在Al基体上，呈纳米晶粒。Al基体晶粒大小约1．2μm，在其晶界和晶粒内都有粒子析出。在Al基体上还分布着由非晶和亚微米晶粒构成的混合相。研究表明，该工艺是制备Al-Pb系列轴瓦合金的较佳方法；并为制备室温不互溶、高温存在很宽固溶间隙、有较大密度差异的合金组元且组织均匀的合金奠定了工艺基础。     

金属塑性成形过程的微观组织模拟与优化技术研究现状

介绍了金属塑性成形过程中微观组织演变的数学模型和常用的微观组织优化目标函数 ,给出了金属塑性成形微观组织模拟和优化的主要方法———微观遗传算法和灵敏度分析方法的基本原理 ,叙述了近年来国内外金属塑性成形微观组织模拟与优化研究概况。     

钨极氩弧焊逆变电源系统PI控制的Simulink仿真整定

钨极氩弧焊(GTAW)逆变电源系统是典型的大信号非线性系统，很难用线性化小信号的解析方法进行近似估计，作者利用Matlab中具有建模、分析和仿真等多功能的Simulink工具包，根据逆变电源的控制结构及GTAW电弧负载的特点，建立了由PI调节的GTAW逆变电源-电弧闭环系统的模型，在此基础上，进行了Simulink仿真研究，并进行了PI参数的调整。研究表明，PI调节的比例系数对系统的e动态响应有较大的影响，积分系数对消除系统的稳态误差起着较大的作用，同时，若这两个参数选择不当，将会造成系统的不稳定。     

飞边槽结构形式对模锻成形的影响

开式模锻中飞边槽的形式对锻件成形过程的影响较大。本文通过大型体积成形有限元模拟软件DEFORM对采用不同形式飞边槽的锻件锻造过程进行了模拟，通过比较模拟结果得出不同形式飞边槽对模锻成形的影响，并就不同形式飞边槽在开式模锻中对模具型腔的填充性和模锻力的影响进行了详细分析。     

壳聚糖微细粉末化研究

本文研究了壳聚糖在乙酸水溶液中滴加H2O2的氧化降解条件与相对分子量的关系及结晶的影响因素，结果表明适当降低相对分子质量和添加成核剂，并在低温下干燥，才能得到高度结晶的微细粉状微晶壳聚糖。     

Effect of miscibility and forced compatibility on damping properties of CIIR/PAc blend

In this study, a kind of novel damping materials was prepared based on the blend of chlorinated butyl rubber (CIIR) and polyacrylate (PAc) synthesized by different molar ratio of butyl methacrylate and ethyl acrylate. Research results from experiments and analyses by employing DMA, TEM, and FTIR show that whether at a cocured system or noncocured system, it can be achieved to shift a loss peak of CIIR towards a higher temperature region and to keep the damping value from markedlly decreasing, which broadens the effective damping function area of CIIR to the vicinity of ambient temperature. In the former system, the thermodynamical miscibility of CIIR and PAc, to some extent, is predominated by the molecular design of PAc, while in the latter system, covulcanized networks play a more significant role in improving compatibility and abating the peak split, though the suppression effect of thermal stress on the transition of CIIR T_ll transition still can not be neglected. Furthermore, transition state derived from the cocuring CIIR and PAc cannot make the phase separation completely take place, and consequently results in the deformation of phase morphology of the cocured CIIR/PAc blend. It is the influence of thermodynamics miscibility and forced compatibility in different size that makes the suppression effect of foreign PAc on CIIR T_ll transition be controllable. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3127–3133, 2006     

4-氟-2-氯苯胺的合成研究

介绍了以 4 氟苯胺为原料 ,通过乙酰化、氯代、水解三步制备 4 氟 2 氯苯胺的方法 ,对主要的影响因素作了考察并得出结论 :乙酰化反应温度应小于 30℃ ;氯代中 2 /SO2 Cl2为 1∶0 9(mol/mol)时较好 ;在水解阶段盐酸浓度控制在 4mol/L较佳 ,4 氟 2 氯苯胺的纯度大于 99% ,总收率达到 70 %     

An Attractive Synthetic Approach to Methyl Formate from Methanol via Methyl Nitrite

Catalytic synthesis of methyl formate has been investigated by a novel route starting from methyl nitrite in vapor phase. The acidic sites of the catalysts play a crucial role for the catalytic activity and the selectivity of formation of methyl formate. The H-Y zeolite catalyst gave higher yield and selectivity of the target product. This study provides a new approach for the synthesis of methyl formate from methanol via methyl nitrite.