表征PAN纤维和炭纤维微细结构的HRTEM样品制备方法

为用高分辨透射电子显微术(HRTEM)表征聚丙烯腈(PAN)纤维和炭纤维的微细结构，从纤维性能出发，探讨研碎、离子束减薄和超薄生物切片三种制备方法及其工艺步骤，结合实验结果，对比了三种制备方法的原理、优缺点，提出了制备方法的适用范围和选择原则，并推断适于表征预氧化纤维微细结构的样品制备方法。与生物样品的制备方法类似，把超薄生物切片法引入到纤维材料HRTEM样品制备领域，为系统研究炭纤维微细结构的演变提供了线索。     

DWT－Based Watermarking Scheme for Digital Images

A watermarking scheme for digital images is introduced. This method is based on discrete wavelet transform and spread spectrum technique. A discrete wavelet transformed binary signature image is expanded by an m-sequence and added to the large wavelet coefficients of a host image with a scale factor. Good balance be-tween transparency and robustness is achieved by the selection of the scale factor. In addition, the spread spec-trum technique is adopted to increase the robustness of this watermarking scheme. The experimental results show that the proposed method is of good performance and robustness for common image operations such as JPEG lossy compression, etc.     

土壤样品的微波消解及其痕量铀的分析

对3个土壤样和2个放射性河床沉积物的国家标准物质进行了微波消解，又采用TOPO萃取和液体荧光法分析了样品中的铀含量，并将分析结果与国家标准方法GB11220．2-89的分析结果进行了比较。结果表明，微波消解法与国家标准方法一样，均不能实现土壤的全部消解，但与国家标准方法相比较，微波消解速度快，所需试剂量少，且易于实现定量控制，铀回收率高，分析精度高。对不溶物进行X射线能谱分析发现，其主要组成为铝、钛及过渡金属的氟化物或氧化物。同位素质谱分析表明，国家标准物质GBW08304中的^234U，^235U均比天然丰度低，另一个国家标准物质GBW08304a中铀的同位素分布与天然组成基本一致。     

用同步辐射X荧光分析血浆蛋白质的微量元素

用同步辐射X荧光(SRXRF)分析技术与凝胶色谱生化分离相结合，分析了用抗肿瘤药物顺铂处理过的和未处理过的小鼠血浆的大分子蛋白质。对以轻元素为基体的小量样品，用X荧光谱中的康普顿散射强度作为质量的因子，获得了在大于22ku分子量的蛋白质中Pt、S、Ca、Fe、Ni、Cu、Zn、Se、Br和Sr等元素含量在不同样品问的相对变化。由此推测，经顺铂处理后，Pt元素可与血浆中的大分子蛋白结合，含CM和S的大分子蛋白含量明显升高，而含Zn的减少。     

飞行时间质谱峰形分析

从离子运动方程出发，用峰形分析方法离子的质谱峰进行数据再处理，首次从飞行时间质谱峰峰形中获得离子产生时的空间分布信息。这种峰形分析方法可以广泛应用于分析飞行时间质谱的各种离子源中离子的分布。     

On the order of stable compensators for a class of time-delay system

The stabilization using a stable compensator does not introduce additional unstable zeros into the closed-loop transfer function beyond those of the original plant, so it is a desirable compensator, the price is that the compensator‘s order will go up. This note considered the order of stable compensators for a class of time-delay systems. First, it is shown that for single-loop plants with at most one real fight-half plane zero, a special upper bound for the minimal order of a strongly stabilizing compensator can be obtained in terms of the plant order; Second, it is shown that approximate unstable pole-zero cancellation does not occur,and the distances between distinct unstable zeroes are bounded below by a positive constant, then it is possible to find an upper bound for the minimal order of a strongly stabilizing compensator.     

0Cr15Ni5Cu2Ti合金持久强度极限和曲线的测定

叙述了0Cr15Ni5Cu2Ti合金性能测试,在试验时间有限,试样数量有限并兼顾测定σ-t曲线的情况下,如何测定持久强度极限σtτ的方法.     

当代信息传播设计的趋势和走向

通过信息社会人类对信息感知的扩展性研究 ,从信息感知方式及思维形态的差异性来分析传统印刷文化与当代视屏文化的异同 ,以图形语言的变化来揭示当代视觉传播设计技术特征、视觉特征、多元化语言特征以及发展趋势     

产氚聚变堆概念设计系统研究

提出了基于球环类型的先进氚生产堆概念设计,它是聚变能发展的中间应用。与传统托卡马克氚生产堆不同,设计中利用了球形环的先进等离子体物理性能和紧凑的结构特征,并尽量利用真空室内的空间安置氚生产包层以减少氚泄露而增加氚增殖率,达到年生产氚1000 g的目标,相应的堆利用因子为40％。在2D中子学计算的基础上提出了较为完整的初步概念设计。逐项进行了分析,同时对设计的风险、不确定性和后备方案也做了概括的解释。为下一步更详细、具体的概念设计提供了直接的依据和重要的参考价值。     

Recovery of indium and lead from lead bullion

Lead and indium were recovered by electrolysis and nonequilibrium solvent extraction process from lead bullion.The effects of current density,electrolytic period and circle amnant of electrolyte on the electrochemical dissolution of lead and indium were investigated.The effects of extraction phase ratio and mixing time on solvent extraction of indium and striping phase ratio and stripping stage on the loaded organic phase stripping were also investigated.The experimental results indicate that under optimum conditions,the purity of lead deposited on cathode is 98.5% and the deposit rate of lead is 99.9%,the dissolution rate of indium is 94.28%,the extraction rate of indium is 98.69%,the stripping rate of indium is almost 100%,and the impurity elements,such as Zn,Fe and Sn can be removed.