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111.
Miniaturisation and simplification are novel approaches in clinical bioanalysis, especially in therapeutic drug monitoring (TDM). These contemporary trends are related to the sampling, pre-treatment, and analysis of biological fluids. Currently, dried blood spot (DBS), one of the most popular microsampling techniques, is feasible and inexpensive. However, obtaining reliable results with sample homogeneity and volume variability is difficult. Volumetric Absorptive Microsampling (VAMS) has recently enabled the accurate and precise collection of a fixed blood volume. It reduced the hematocrit effect, improved volumetric accuracy, and generated results correlating with the dose and drug exposure from wet blood. This review focuses on VAMS-Mitra™ devices, which have become increasingly important since 2014, mainly for TDM and toxicology studies. First, the current literature has been reviewed based on immunosuppressants and their determination in samples obtained using Mitra™. Second, the critical points, weaknesses, and strengths have been characterized in contrast to classic venipuncture and other microsampling methods. Finally, we indicate the points of attention according to the perspective of Mitra™ as well as its usefulness in clinical practice. VAMS is currently state-of-the-art in microsampling and seems to be a good instrument for improving adherence to immunosuppressive therapy, especially in the pediatric population. 相似文献
112.
Artur Bekaa Wodzimierz Potek Dorota Siwicka-Gieroba Joanna Soek-Pastuszka Romuald Bohatyrewicz Jowita Biernawska Katarzyna Kotfis Magdalena Bielacz Andrzej Jaroszyski Wojciech Dabrowski 《International journal of molecular sciences》2022,23(13)
Brain injury, especially traumatic brain injury (TBI), may induce severe dysfunction of extracerebral organs. Cardiac dysfunction associated with TBI is common and well known as the brain–heart crosstalk, which broadly refers to different cardiac disorders such as cardiac arrhythmias, ischemia, hemodynamic insufficiency, and sudden cardiac death, which corresponds to acute disorders of brain function. TBI-related cardiac dysfunction can both worsen the brain damage and increase the risk of death. TBI-related cardiac disorders have been mainly treated symptomatically. However, the analysis of pathomechanisms of TBI-related cardiac dysfunction has highlighted an important role of melatonin in the prevention and treatment of such disorders. Melatonin is a neurohormone released by the pineal gland. It plays a crucial role in the coordination of the circadian rhythm. Additionally, melatonin possesses strong anti-inflammatory, antioxidative, and antiapoptotic properties and can modulate sympathetic and parasympathetic activities. Melatonin has a protective effect not only on the brain, by attenuating its injury, but on extracranial organs, including the heart. The aim of this study was to analyze the molecular activity of melatonin in terms of TBI-related cardiac disorders. Our article describes the benefits resulting from using melatonin as an adjuvant in protection and treatment of brain injury-induced cardiac dysfunction. 相似文献
113.
The LC–MS/MS technique was applied to the stability study of several flavonoids and phenolic acids in honey samples during the ultrasonic extraction (USE) and microwave-assisted extraction (MAE). Phenolic compounds from the standard mixture were stable under ultrasounds action with the mean recovery of (90.4% ± 7.1%), but during microwave-assisted extraction the benzoic acid derivatives and aglycones of flavonoids showed lower recovery (70–80%). In honey matrix, the phenolic acids and the glycosides exhibited the high stability for MAE and USE treatments. However, the recoveries of tested aglycones were below 10%. In the presence of an artificial sugar matrix, flavonols were almost completely degraded after successive treatment under MAE and USE conditions. The obtained results indicated that standard addition method for flavonoids quantification in honey samples should not be recommended. Application of the USE conditions provided higher and/or similar extraction yields for phenolic acids than usually applied shaking with solvent. It also allowed shortening the time required for the whole sample preparation procedure. Phenolic acids and glycosides such as quercetrin, rutin and hesperidin appeared to be stable under such conditions. 相似文献
114.
M. Palasiski 《Starch - St?rke》1980,32(12):405-408
On the Phoshoric Acid in Potato Starch. Potato starch contains chemically linked ortho-phosphoric acid (30 to 175 mg% P). Among the physico-chemical properties of potato starch effected by the phosphoric acid the most important are ion exchange and selfhydrolysis. By the ability of ion exchange it is possible to produce the salts of the pure esters of amylo-phosphoric acid (cationic starches). Sodium, potassium, ammonium, calcium and magnesium starches differ in rheological properties. The hydrogen ions of amylophosphoric acid are able to effect the hydrolytic splitting of the starch. This hydrolysis consists of two different processes: the splitting of the glucosidic linkages and the splitting of the ester linkage between the phosphoric acid and the glucose unit. Velocity of self-hydrolysis is dependent on the hydrogen ion concentration. The self-hydrolysis of hydrogen starch offers the possibility of producing degraded starch products with different technical properties without any addition of chemicals and/or enzymes. 相似文献
115.
116.
石玉龙 《青岛科技大学学报(自然科学版)》1994,(1)
运用射频等离子体化学气相沉积在Si(100)P进行外延试验,并用四极质谱仪(QMS)进行监测,得出了SiH4浓度的变化规律。试验结果表明在600℃,压力为300mTorr时,外延生长率最高,为450/min,膜中H含量也较低,为1.5%[at]。在压力为30mTorr,700℃时,外延生长率为59.6/min,膜中H含量降至2.75%[at]。 相似文献
117.
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119.
We present an overview of some recent developments in the area of mathematical modeling of maintenance decisions for multi-unit systems. The emphasis is on three main groups of multicomponent maintenance optimization models: the block replacement models, group maintenance models, and opportunistic maintenance models. Moreover, an example of a two-unit system maintenance process is provided in order to compare various maintenance policies. 相似文献
120.