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41.
Processing of wood plastic composites: The influence of feeding method and polymer melt flow rate on particle degradation 下载免费PDF全文
Spruce wood particle (WP)/polypropylene (PP) compounds were prepared in an internal mixer using different rotor speeds. To analyze the effect of feeding method on particle degradation, WP and PP were either fed as dry‐blend or WP was fed into the PP melt. To prevent melt freezing, pre‐heated WP were used as comparison to cold WP. In addition, WPs were compounded with different grades of PP or high‐density polyethylene (HDPE) to analyze the effect of polymer matrix melt flow rate (MFR) on particle degradation. Mixing behavior of compounds containing 30% and 70% (w/w) WP depended on feeding method, represented by a changing relation of final torque values. Feeding as dry‐blend and using pre‐heated particles led to stronger WP degradation. Degradation decreased with increasing polymer MFR. For PP compounds, particle degradation was stronger when containing 70% WP, for HDPE the difference due to WP content was only marginal. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43231. 相似文献
42.
Synthesis and Biopharmaceutical Evaluation of Imatinib Analogues Featuring Unusual Structural Motifs 下载免费PDF全文
Prof. Kyriacos C. Nicolaou Dr. Dionisios Vourloumis Dr. Sotirios Totokotsopoulos Dr. Athanasios Papakyriakou Dr. Holger Karsunky Hanan Fernando Dr. Julia Gavrilyuk Dr. Damien Webb Dr. Antonia F. Stepan 《ChemMedChem》2016,11(1):31-37
A convenient synthesis of imatinib, a potent inhibitor of ABL1 kinase and widely prescribed drug for the treatment of a variety of leukemias, was devised and applied to the construction of a series of novel imatinib analogues featuring a number of non‐aromatic structural motifs in place of the parent molecule's phenyl moiety. These analogues were subsequently evaluated for their biopharmaceutical properties (e.g., ABL1 kinase inhibitory activity, cytotoxicity). The bicyclo[1.1.1]pentane‐ and cubane‐containing analogues were found to possess higher themodynamic solubility, whereas cubane‐ and cyclohexyl‐containing analogues exhibited the highest inhibitory activity against ABL1 kinase and the most potent cytotoxicity values against cancer cell lines K562 and SUP‐B15. Molecular modeling was employed to rationalize the weak activity of the compounds against ABL1 kinase, and it is likely that the observed cytotoxicity of these agents arises through off‐target effects. 相似文献
43.
44.
Efficient Engineering and Production Concepts for Products in Regulated Environments – Dream or Nightmare? 下载免费PDF全文
Prof. Jochen Strube Dr. Reinhard Ditz Holger Fröhlich Dr. Dirk Köster Dr. Thomas Grützner Dr. Jörg Koch Dr. Rüdiger Schütte 《化学,工程师,技术》2014,86(5):687-694
Manufacturing of chemical‐pharmaceutical products is moving increasingly fast on a global scale. Therefore, developing and starting up production facilities fast, with high quality, and at reasonable costs has become extremely challenging. Engineering concepts like modularization, standardization and simultaneous/parallel engineering are discussed as methods for speeding up process design and filing for regulatory approval. Transfer from batch to continuous operation mode of production is pointed out as the key‐issue in such strategies. 相似文献
45.
Effect of Constant‐Rate Reduction on the Performance of a Ternary Cu/ZnO/Al2O3 Catalyst in Methanol Synthesis 下载免费PDF全文
A multi‐functional flow set‐up was developed for the rate‐ and temperature‐controlled reduction of copper catalysts, their application in high‐pressure methanol synthesis and the determination of the copper surface area by N2O frontal chromatography. The influence of constant‐rate reduction on the catalytic properties of a ternary Cu/ZnO/Al2O3 catalyst was investigated. The temperature during the constant‐rate reduction was found to decrease, indicating autocatalytic kinetics, but no significant catalytic effect of the milder reduction conditions was observed compared with a slow linear heating ramp. 相似文献
46.
Damage evolution of the alloy IN 738 LC at high temperature low cycle fatigue Herrn Professor K.-T. Rie zum 60. Geburtstag Interrupted Low-Cycle-Fatigue tests have been carried out with IN 738 LC at 850°C. The specimens were extensively examined by SEM to quantify the evolution of fatigue damage. Surface crack nucleation at oxidized grain boundaries occured during the whole experiments. The coalescence of cracks was the dominant mechanism which lead to macro crack evolution and the final fracture. 相似文献
47.
Kathrin Landgraf Andreas Kühnapfel Maria Schlanstein Ronald Biemann Berend Isermann Elena Kempf Holger Kirsten Markus Scholz Antje Krner 《International journal of molecular sciences》2022,23(8)
Obesity develops early in childhood and is accompanied by early signs of adipose tissue (AT) dysfunction and metabolic disease in children. In order to analyse the molecular processes during obesity-related AT accumulation in children, we investigated genome-wide expression profiles in AT samples, isolated adipocytes, and stromal vascular fraction (SVF) cells and assessed their relation to obesity as well as biological and functional AT parameters. We detected alterations in gene expression associated with obesity and related parameters, i.e., BMI SDS, adipocyte size, macrophage infiltration, adiponectin, and/or leptin. While differential gene expression in AT and adipocytes shared an enrichment in metabolic pathways and pathways related to extracellular structural organisation, SVF cells showed an overrepresentation in inflammatory pathways. In adipocytes, we found the strongest positive association for epidermal growth factor-like protein 6 (EGFL6) with adipocyte hypertrophy. EGFL6 was also upregulated during in vitro adipocyte differentiation. In children, EGFL6 expression was positively correlated to parameters of AT dysfunction and metabolic disease such as macrophage infiltration into AT, hs-CRP, leptin levels, and HOMA-IR. In conclusion, we provide evidence for early alterations in AT gene expression related to AT dysfunction in children and identified EGFL6 as potentially being involved in processes underlying the pathogenesis of metabolic disease. 相似文献
48.
Mödlinger Marianne Cziegler Andreas Macció Daniele Schnideritsch Holger Sabatini Benjamin 《Metallurgical and Materials Transactions B》2018,49(5):2505-2513
Metallurgical and Materials Transactions B - Understanding the effects of impurities, segregation, undercooling, and solidification velocity is necessary to reconstruct prehistoric As-Cu alloy... 相似文献
49.
Volkan Kumtepeli Yulong Zhao Maik Naumann Anshuman Tripathi Youyi Wang Andreas Jossen Holger Hesse 《国际能源研究杂志》2019,43(9):4127-4147
The rapid increase of renewable energy sources made coordinated control of the distributed and intermittent generation units a more demanded task. Matching demand and supply is particularly challenging in islanded microgrids. In this study, we have demonstrated a mixed‐integer quadratic programming (MIQP) method to achieve efficient use of sources within an islanded microgrid. A unique objective function involving fuel consumption of diesel generator, degradation in a lithium‐ion battery energy storage system, carbon emissions, load shifting, and curtailment of the renewable sources is constructed, and an optimal operating point is pursued using the MIQP approach. A systematic and extensive methodology for building the objective function is given in a sequential and explicit manner with an emphasis on a novel model‐based battery aging formulation. Performance of the designed system and a sensitivity analysis of resulting battery dispatch, diesel generator usage, and storage aging against a range of optimization parameters are presented by considering real‐world specifications of the Semakau Island, an island in the vicinity of Singapore. 相似文献
50.
Vineyards are an intensive cultivation system and expose the soil to long-lasting stress. Many vineyard areas already show high degrees of soil degradation. To prevent further soil erosion, cover crops, which have various positive effects on the environment, are highly recommended. But, depending on the climatic conditions, cover crops can reduce grape yields and are sometimes more work intensive than bare soil management. In some areas cover crops are already widespread while in others bare soil is dominant. In this qualitative study, we explore the attitudes of European winegrowers towards cover crops and determine the background for differences in the adoption of greened vineyards. Thus, we conducted focus groups with winegrowers in two different regions, namely Coteaux du Layon in France and Montilla-Moriles in Spain. In this setting, the transregional differences are mainly based on the climatic conditions but also on different business structures and knowledge levels. Direct sellers seem to be more attentive to the environment and use cover crops more often than farmers which sell their grapes to cooperatives. 相似文献