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91.
92.
Akihiro Orita Shoko Tanabe Tatsuhiko Ono Junzo Otera 《Advanced Synthesis \u0026amp; Catalysis》2010,352(9):1419-1423
Fluorous distannoxanes (XRf2SnOSnRf2X)2⋅n H2O (Rf=C6F13C2H4) ( 1 : X=C8F17SO3, n=10; 4 : X=Cl, n=0) ( 1 ) catalyze the Mukaiyama aldol reaction and the allylation of aldehydes with tetraallyltin at room temperature in fluorous/organic biphasic solvent systems, in which the reactions proceed more rapidly than in a single organic or fluorous solvent. Due to the unique surface activity of 1 , the catalyst, organic substrate(s), and reagent(s) are distributed in both organic and fluorous phases to facilitate smooth reactions. Upon dilution with toluene after the reaction, the catalyst concentrates to the fluorous phase, while the organic substances migrate to the organic phase to effect facile catalyst recovery and recycling. By virtue of such a unique solvophilicity, a new version of fluorous biphase technology has been developed. 相似文献
93.
The feasibility of using loofa sponge for immobilization of cellulase-producing microorganisms was investigated by acetylating loofa sponge. Acetylation was achieved by autoclaving process of loofa sponge immersed in acetic anhydride at various temperatures for various times. The degree of acetylation, as inferred by the weight percentage gain (WPG), was enhanced by increasing both temperature and the duration of acetylation. The acetylation of a piece of loofa sponge in an autoclave at 120 degrees C for 20 min resulted in a WPG of about 8%, which was sufficient to protect the loofa sponge against cellulose degradation. The acetylated loofa sponge prepared under this condition was not decomposed by commercial cellulase and its structure was maintained for more than 720 h during repeated-batch treatments with commercial cellulase. A flocculating yeast (Saccharomyces cerevisiae IR-2) and a fungus (Trichoderma reesei QM9414) were successfully immobilized in the acetylated loofa sponge. In each case, the percentage of immobilized cells was as high as that obtained using nonacetylated loofa sponge. Acetylation had no adverse effects on cell growth and immobilization of T. reesei QM9414, as well as on cell growth and ethanol production by S. cerevisiae IR-2. T. reesei QM9414 immobilized on an acetylated loofa sponge was successfully used for repeated-batch cellulase production from commercial cellulose powder. Although the acetylated loofa sponge showed a slight weight loss, it was not disintegrated by activated sludge. The results obtained in this study showed that acetylated loofa sponge is suitable as an immobilization carrier for bioprocesses involving cellulase. 相似文献
94.
Shingo Hirose Akihiro Yoshida Masaaki Yamaura Nobuo Kano Hiro Munekata 《Journal of Materials Science: Materials in Electronics》2000,11(1):7-10
We demonstrate a method for successfully controlling carbon incorporation in AlAs layers grown by atomic layer epitaxy (ALE) using various GaAs substrates with different orientations. The number of alkyl radicals attached to an Al atom at the surface, which is a main factor in carbon incorporation, can be intentionally controlled by changing substrate orientation. We found that the carbon incorporation in ALE-AlAs using the (3 1 1)B surface is 2 x 1017,cm-3, which is the lowest value ever reported for ALE-AlAs that satisfies one-monolayer self-limiting growth conditions. 相似文献
95.
Correction and evaluation of the effect due to parasitic motion on primary accelerometer calibration 总被引:1,自引:0,他引:1
Primary accelerometer calibration is carried out under the assumption that a vibration exciter gives a rectilinear motion to an accelerometer to be calibrated. However practical vibration given by the vibration exciter includes parasitic motion such as transverse, rocking, and bending motion. Such parasitic motion would give two serious effects on primary calibration results, transverse motion effect and vibration distribution effect. Transverse motion effect is caused by an inner product of the vectors of both transverse motion and transverse sensitivity. On the other hand, the vibration distribution effect is caused by relative motion between a sensing point of accelerometer and a spot sensed by the interferometer. As these effects have close interaction between parasitic motion and measuring instruments, it would be very difficult to evaluate them by measuring independently each component. 相似文献
96.
Takuhei Hashiguchi Masayuki Watanabe Akihiro Matsushita Yasunori Mitani Osamu Saeki Kiichiro Tsuji Masahide Hojo Hiroyuki Ukai 《Electrical Engineering in Japan》2008,163(3):10-18
Electric power systems in Japan are composed of remote and distributed location of generators and loads mainly concentrated in large‐demand areas. The structures having long‐distance transmission tend to produce heavy power flow with increasing electric power demand. In addition, some independent power producers (IPP) and power producer and suppliers (PPS) are participating in the power generation business, which makes power system dynamics more complex. However, there was little observation as a whole power system. In this paper the authors present a global monitoring system of power system dynamics by using the synchronized phasor measurement of demand‐side outlets. Phasor Measurement Units (PMU) are synchronized based on the global positioning system (GPS). The purpose of this paper is to show oscillation characteristics and methods for processing original data obtained from PMU after certain power system disturbances triggered by accidents. This analysis resulted in the observation of the lowest and the second lowest frequency mode. The derivation of eigenvalue with the two‐degree‐of‐freedom model brings a monitoring of two oscillation modes. Signal processing based on wavelet analysis and simulation studies to illustrate the obtained phenomena are presented in detail. © 2008 Wiley Periodicals, Inc. Electr Eng Jpn, 163(3): 10– 18, 2008; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20316 相似文献
97.
To investigate whether monkeys perceive relative pitch, the author trained 3 Japanese monkeys (Macaca fuscata) to detect changes from rising to falling contours of 3-tone sequences. Tone sequences were presented serially with transposition, so monkeys were urged to attend to cues other than the absolute frequency of a component tone. Results from probe tests with novel sequences showed that monkeys discriminated by the relative pitch when the frequency ranges of sequences were within the training range, showing a similar tendency as birds in previous studies (e.g., S. H. Hulse, J. Cynx, & J. Humpal, 1984). (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
98.
99.
Design methodology for a braided cylinder 总被引:1,自引:0,他引:1
Asami Nakai Akihiro Fujita Atsushi Yokoyama Hiroyuki Hamada 《Composite Structures》1995,32(1-4):501-509
In this study, the design methodology for a braided cylinder was presented. The concept of an analytical model which involved both micro model and macro model was proposed. The analytical method was applied to estimate the rigidity and elastic limit of a braided cylinder subjected to bending and torsional load independently and as combined load. Using the analysis method, the design of a braided cylinder would be carried out in consideration of the factors that decide the mechanical properties of braided cylinder. This method has the possibility to be useful for structural design of braided composites and can be included as a unit in CAE systems for braided composites. 相似文献
100.
Shoya Uchida Akihiro Sato Mamiko Inamori Yukitoshi Sanada Mohammad Ghavami 《Wireless Personal Communications》2014,79(2):987-1002
Overlapped FFT has been proposed as a signal detection scheme in dynamic spectrum access to reduce the variance of the noise and improve the detection probability. However, the improvement of the detection probability in the conventional overlapped FFT is bounded with the upper limit of the overlap ratio. This paper proposes a new overlapped FFT scheme using additional frames. In the proposed scheme, in addition to the original FFT frames, new frames that consist of multiple subframes with non-continuous samples are constructed and included. It can realize the increase of the number of the FFT frames and the improvement of the detection probability compared with the conventional scheme. Numerical results through computer simulation show that the proposed scheme improves the detection probability by up to 0.07. On indoor channel models the proposed scheme also improves the detection probability. In addition, it is clarified that as the delay spread increases the detection probability reduces due to the correlation between the frames. 相似文献