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71.
A tertiary amine functionalized 4-nitro-4′-alkoxy azobenzene mesogen with a 10 or 12 carbon spacer (azo-nN) was synthesized and complexed in equimolar proportions with poly(acrylic acid) (PA-H) and poly(sulfonic acid) (PSS-H), and investigated by thermogravimetric analysis, differential scanning calorimetry, polarizing optical microscopy, Fourier transform infrared spectroscopy and X-ray diffraction. The neat azo-nN is characterized by a partial bilayer SA mesophase at higher temperatures, and a highly ordered phase, in which the molecules are stacked orthogonally in bilayers, at lower temperatures. As supported by infrared analysis, for the azo-nN/PA-H mixture, the complexation is partial while for the same azo-nN/PSS-H mixture, complete proton transfer occurs. When the azo-nN is blended with the PA-H, regarded as a weak acid, a biphasic system is generated and the thermotropic behavior of neat mesogen is not significantly affected. In contrast, by mixing the same mesogen with a PSS-H (regarded as a strong acid), the thermotropic behavior is significantly influenced: the complexation generated a partial or interdigitated smectic A or tilted smectic C lamellar phase. 相似文献
72.
Fabrication of alumina-aluminium titanate laminates that combine high strength external layers with flaw tolerant internal
layers is limited by the difficulty of the co-sintering of layers with large differences in the green state. This work describes
a new method to obtain alumina-aluminium titanate layered materials constituted by layers with large differences in terms
of grain size starting from green bodies with similar microstructures. The approach is based on the effect of small amounts
of titania (TiO2) as agents for alumina grain growth enhancement. Starting from a fine grained green body that combined alumina layers with
composite layers made of mixtures of alumina and titania, a two step sintering schedule led to a layered structure with external
layers of small grain sized alumina combined with internal alumina layers with large grain size due to the diffusion of titanium.
The large grain sized alumina layers conferred flaw tolerant behaviour to the laminate due to crack branching and bridging. 相似文献
73.
Raphaëlle Savoire Jean‐Louis Lanoisellé Hélène Ducatel Eugène Vorobiev 《European Journal of Lipid Science and Technology》2008,110(8):725-734
Seven linseed varieties were harvested at seven times before complete maturity. Microscale oilseed expressions were subsequently carried out on it. A pressure of 10 MPa was applied for 1 h under uniaxial stress. The results were characterized in terms of oil, water and mucilage content, harvest date and oil yield. The piston displacement versus time (creep curves) was described by a four‐Kelvin‐Voigt elements viscoelastic model. Parameters were derived from the model, such as the mechanical properties of seeds (compressibility moduli), showing that the viscoelastic model fits well the experimental data (R² ≈ 0.999). The modeling parameters were combined with some biochemical data in order to predict the kinetics of oil extraction. 相似文献
74.
Psychological health-sickness (PHS) as a predictor of outcomes in dynamic and other psychotherapies.
Luborsky Lester; Diguer Louis; Luborsky Ellen; McLellan A. Thomas; Woody George; Alexander Leslie 《Canadian Metallurgical Quarterly》1993,61(4):542
This is the first dedicated review of quantitative studies on Freud's proposition that the poorer the psychological health, the more limited are the benefits from treatment. Since observer-rated scales for PHS were developed in 1949, many studies have applied them, and the majority show significant prediction of outcomes of psychotherapy, with correlations between .2 and .35. This article reviews (1) the main methods of measurement, (2) the record of predictive success, (3) validity studies, (4) the relation to psychiatric diagnosis, (5) prediction in forms of treatment other than psychotherapy, and (6) theories of why psychological health predicts outcomes of psychotherapy. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
75.
Examined reviewer recommendations and subsequent editorial decisions for 153 papers submitted for publication. In an earlier article (D. W. Fiske and L. Fogg; see record 1990-23769-001), the authors demonstrated the diversity of reviewer comments and the relative uniqueness of each review. In the current study, overall reviewer recommendation to accept or reject an article predicted 93% of the 153 editorial decisions correctly. Reviewers evaluated papers on the basis of planning and execution flaws or general negative comments, with little weight given to interpretations or results. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
76.
77.
M Albert C Athanassopoulos LB Auerbach D Bauer R Bolton B Boyd RL Burman I Cohen DO Caldwell BD Dieterle JB Donahue AM Eisner A Fazely FJ Federspiel GT Garvey RM Gunasingha V Highland J Hill R Imlay K Johnston WC Louis A Lu AK Mann J Margulies K McIlhany W Metcalf RA Reeder V Sandberg M Schillaci D Smith I Stancu W Strossman MK Sullivan GJ VanDalen W Vernon YX Wang DH White D Whitehouse D Works Y Xiao S Yellin 《Canadian Metallurgical Quarterly》1995,51(3):R1065-R1069
78.
The influence of ointment formulation on the stability, the in-vitro release and the in-vivo absorption through the skin of rabbits was investigated. The choice of the selected ointments has no influence on the drug stability with the exception of an acidified emulsion base. A good correlation between in-vitro release and in-vivo absorption was found revealing that metronidazole was quickly released and effectively absorbed from a polyethylene glycol base. 相似文献
79.
Steven S Fu Miles McFall Andrew J Saxon Jean C Beckham Timothy P Carmody Dewleen G Baker Anne M Joseph 《Nicotine & tobacco research》2007,9(11):1071-1084
We conducted a systematic review of what is known about the relationship between post-traumatic stress disorder (PTSD) and smoking to guide research on underlying mechanisms and to facilitate the development of evidence-based tobacco treatments for this population of smokers. We searched Medline, PsychINFO, and the Cochrane Central Register of Controlled Trials and identified 45 studies for review that presented primary data on PTSD and smoking. Smoking rates were high among clinical samples with PTSD (40%-86%) as well as nonclinical populations with PTSD (34%-61%). Most studies showed a positive relationship between PTSD and smoking and nicotine dependence, with odds ratios ranging between 2.04 and 4.52. Findings also suggest that PTSD, rather than trauma exposure itself, is more influential for increasing risk of smoking. A small but growing literature has examined psychological factors related to smoking initiation and maintenance and the overlapping neurobiology of PTSD and nicotine dependence. Observational studies indicate that smokers with PTSD have lower quit rates than do smokers without PTSD. Yet a few tobacco cessation treatment trials in smokers with PTSD have achieved quit rates comparable with controlled trials of smokers without mental disorders. In conclusion, the evidence points to a causal relationship between PTSD and smoking that may be bidirectional. Specific PTSD symptoms may contribute to smoking and disrupt cessation attempts. Intervention studies that test behavioral and pharmacological interventions designed specifically for use in patients with PTSD are needed to reduce morbidity and mortality in this population. 相似文献
80.
Louis Esperet 《Information Processing Letters》2007,101(5):215-219
A graph G is 2-outerplanar if it has a planar embedding such that the subgraph obtained by removing the vertices of the outer face is outerplanar. The oriented chromatic number of an oriented graph H is defined as the minimum order of an oriented graph H′ such that H has a homomorphism to H′. In this paper, we prove that 2-outerplanar graphs are 4-degenerate. We also show that oriented 2-outerplanar graphs have a homomorphism to the Paley tournament QR67, which implies that their (strong) oriented chromatic number is at most 67. 相似文献