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21.
The adsorption of acetonitrile and reduction of adsorbed molecules at platinized platinum electrode were studied by potentiodynamic and radiometric techniques. During acetonitrile adsorption the reversibly and irreversibly adsorbed species are formed. One electron reduction process occurs in the potential range 0.45-0.15 V. Below 0.15 V the deeper reduction of adsorbed acetonitrile takes place — the final products are ammonia and ethane. The differences of smooth and platinized platinum electrodes properties are briefly discussed. 相似文献
22.
The enthalpies of thermal dissociation (ΔdH) and formation (ΔfH) found in the literature as well as the crystal lattice energies (Ec) of inorganic and organic hexahalogenohafnates (MI2(or MII)HfX2−6; MI and MII denote monovalent and divalent cations respectively and X denotes a halogen) are reviewed and discussed. The enthalpies of formation of the salts were evaluated using the above-mentioned ΔdH values and known enthalpies of formation of products of decomposition. Combination of the enthalpies of formation of hexahalogenohafnates thus obtained or those of the literature with the literature values of the enthalpy of formation of cations and theoretically determined enthalpies of formation of HfX2−6 (or electrostatic lattice energies of the salts) afforded lattice energies of the salts (or enthalpies of formation of gaseous HfX2−6). Values of ΔfH were also assessed taking theoretically obtained electrostatic lattice energies of the salts and enthalpies of formation of HfX2−6 and literature or theoretically determined values of the enthalpy of formation of gaseous cations. The independent sets of crystal lattice energies and thermochemical radii for HfX2−6 were obtained following the Kapustinskii—Yatsimirskii approach. Combination of the latter method with the thermochemical cycle afforded information on the influence of the dimensions of ions on the thermodynamic stability of hexahalogenohafnates with respect to dissociation and oxidation processes. The thermochemical quantities of experimental and theoretical origin correlate with each other reasonably well, thus increasing their reliability. 相似文献
23.
Hualong Li Emilie Hsu Jerzy Szpunar Ravi Verma Jon. T. Carter 《Journal of Materials Engineering and Performance》2007,16(3):321-326
In order to determine the deformation modes in AZ31 magnesium alloy at room temperature, computer simulations of deformation
texture development and calculation of formability have been carried out. The simulation results were compared with the measured
texture results. Based on agreement between the experiments and simulations the active deformation modes were determined.
A Visco Plastic Self Consistent model was employed for the simulation of plastic deformation. Simulations and experiments
were performed for different initial textures. The goal of the study was to develop the understanding of deformation texture
evolution and its effects on mechanical properties of magnesium, with an ultimate goal of improving room temperature formability
of magnesium alloys.
This article was presented at Materials Science & Technology 2006, Innovations in Metal Forming symposium held in Cincinnati,
OH, October 15-19, 2006. 相似文献
24.
David B. Knorr Sc.D. Jerzy A. Szpunar Ph.D. 《JOM Journal of the Minerals, Metals and Materials Society》1994,46(9):42-48
Thin films are important in a variety of applications, including optical, magnetic,and electronic devices. The origin of microstructure in films formed by physical vapor deposition depends primarily on the homologous deposition temperature, which determines the grain structure and substructure. Texture is coupled to grain structure development through several kinetic parameters, principally surface diffusivity and interfacial energy. The representation of such fiber textures is facilitated by simplified pole intensity versus tilt angle plots rather than entire pole figures. The reliability of thin film interconnection materials such as aluminum alloys is heavily leveraged on both texture and grain structure. The properties of thin magnetic films depend on both the crystallographic texture and the grain shape anisotropy. 相似文献
25.
Jerzy Surma 《Expert Systems》2015,32(4):546-554
The practice of strategy decision making proves that when the management board is strongly limited in its capacity to take rational actions, specifically in the context of great decision complexity and uncertainty, it is considered good practice to refer to experience through reasoning by analogy. In this paper, we would like to concentrate on supporting strategic decisions in small and medium enterprises (SMEs). The complexity of analogy‐based reasoning has its roots in an attempt to solve new problems based on past cases from a different domain, while we will focus on case‐based approach for a single domain. Additionally, we have chosen case‐based reasoning as a suitable decision‐making paradigm because it is corresponds to managers’ decision‐making behaviour. We present the STRATEGOS case‐based reasoning system for supporting strategic decision making by SMEs management boards and then the system evaluation by the dozens of chief executive officers (CEOs) from SMEs is presented. The results of the survey are promising and show the remarkable correspondence of the proposed solution with expectations and strategic behaviour of CEOs. 相似文献
26.
27.
In the paper, the approximate controllability of linear abstract second-order infinite-dimensional dynamical systems is considered. It is proved using the frequency-domain method, that approximate controllability of second-order system can be verified by the approximate controllability conditions for the corresponding simplified first-order system. General results are then applied for approximate controllability investigation of a vibratory dynamical system modeling flexible mechanical structure. Some special cases are also considered. Moreover, remarks and comments on the relationships between different concepts of controllability are given. The paper extends earlier results on approximate controllability of second-order abstract dynamical systems. 相似文献
28.
Cristian Molinaro Jan Chomicki Jerzy Marcinkowski 《Annals of Mathematics and Artificial Intelligence》2009,57(2):103-124
This paper addresses the problem of representing the set of repairs of a possibly inconsistent database by means of a disjunctive database. Specifically, the class of denial constraints is considered. We show that, given a database and a set of denial constraints, there exists a (unique) disjunctive database, called canonical, which represents the repairs of the database w.r.t. the constraints and is contained in any other disjunctive database with the same set of minimal models. We propose an algorithm for computing the canonical disjunctive database. Finally, we study the size of the canonical disjunctive database in the presence of functional dependencies for both subset-based repairs and cardinality-based repairs. 相似文献
29.
H Adamski J Chevrant-Breton S Odent M Patoux-Pibouin B Le Marec A Laudren M Urvoy 《Canadian Metallurgical Quarterly》1994,121(10):694-699
Oculo-dento-digital syndrome (SODD) as defined by Meyer-Schwickerath in 1957 is a rare entity (84 cases) which belongs to ectodermal dysplasias. It consists of: the characteristic features (long face, pinched nose); syndactyly; ocular, dental and bone abnormalities. This entity is usually transmitted on the autosomal dominant mode. We report two cases (a mother and daughter) with polymalformations which we classed as SODD. Furthermore, agenesis of lacrimal duct and genitourinary abnormalities were noted. The mother had a very particular complex hair shaft dysplasia (incomplete pili torti, "tiger tail" aspect, fractures) with alopecia since she was fifteen years old. The daughter's hair was normal at birth. In SODD, fine and sparse hair is often observed (44 p. 100). Only one patient had hair shaft investigation under polarized light: pili annulati and monilethrix were described but not found in our cases. These two reports incite to the systematic hair shaft study in SODD as other ectodermal dysplasia syndromes. 相似文献
30.
According to Pedraz-Delhaes, users evaluate both the product and the vendor on the basis of provided documentation. Thus, a question arises as to what quality characteristics should be taken into account when making a decision about accepting a given user manual. There are some proposals (e.g., ISO Std. 26513 and 26514), but they contain too many quality characteristics and lack orthogonality. The goal of this paper is to propose a simple quality model for user documentation, along with acceptance methods based on it. The model is to be orthogonal and complete. As a result, the COCA quality model is presented, which comprises four orthogonal quality characteristics: Completeness, Operability, Correctness, and Appearance. To check completeness, the proposed quality model has been compared with many other quality models that are directly or indirectly concerned with user documentation. Moreover, two acceptance methods are described in the paper: pure review based on ISO Std. 1028:2008, and documentation evaluation test (a type of browser evaluation test), which is aimed at assessing the operability of user documentation. Initial quality profiles have been empirically collected for both methods—they can be used when interpreting evaluation results obtained for a given user manual. 相似文献