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221.
Carbon Black (CB)-containing immiscible polymer blends based on high-impact polystyrene/thermoplastic polyurethane (HIPS/TPU) were studied as sensing materials for an homologous series of alcohols, including, methanol, ethanol and 1-propanol. The studied immiscible blend was designed to exhibit a double-continuity structure i.e., the CB particles form chain-like network structures within the TPU phase, which forms a continuous phase within the HIPS matrix. Extruded HIPS/TPU/CB filaments produced by a capillary rheometer process at various shear rate levels were used for the sensing experiments. All filaments displayed a selective resistance changes upon exposure to the various alcohols combined with reproducibility and recovery behaviour. An attempt is made to identify the dominant mechanisms controlling the sensing process in a CB-containing immiscible polymer blend characterized by a double-continuity structure. The distinct structure and composition of the HIPS/TPU interphase region were found to have a crucial role in the sensing mechanism, determining the selectivity of the filaments toward the studied alcohols. Additionally, the sensing performance of HIPS/TPU/CB system is compared to recent results for TPU/CB compounds, polypropylene/TPU/CB and HIPS/ethylene vinyl acetate/CB immiscible polymer blends. 相似文献
222.
In the gold wire bonding of aluminum in microelectronic devices the presence of aluminum oxide on the metallization surface may be expected. Electron transparent couples containing an oxide layer at the interface were heated in a TEM to determine the effects of a passivation layer on intermetallic formation. Intermetallic phases were evidenced by changes in sample appearance and their structure was determined by electron diffraction. The presence of an oxide at the interface hindered second phase formation at temperatures at which they were usually expected to form. In aluminum rich couples, the formation of the AuAl2 intermetallic was not observed to form until about 350°C with the oxide present. In a reverse configuration involving a gold rich couple, an amorphous oxide phase was observed between the Al and the advancing Au2Al front. The movement of the reaction front appeared to be controlled by surface diffusion across this phase. 相似文献
223.
224.
M. Loidl E. Leblanc T. Branger H. Rotzinger T. Daniyarov M. Linck A. Fleischmann C. Enss 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2004,520(1-3):73-75
We report on a feasibility study on precise determination of mass-specific activity of low-energy emitting radioisotopes. Conventional methods of activity measurement suffer from source self-absorption and a strong decrease in detection efficiency for low-energy electrons and photons. We propose a new method based on metallic magnetic microcalorimeters with the source embedded in the detector target in a 4π geometry. First results with a 55Fe source show that electrons and photons are detected with a detection efficiency close to unity and with little loss of energy for electrons. The aim of this study is to provide standards of activity with very low uncertainties in the framework of radiation metrology. 相似文献
225.
S. Zh. Davrenbekov E. S. Mustafin B. K. Kasenov S. T. Edil'baeva Sh. B. Kasenova E. K. Zhumadilov Zh. I. Sagintaeva 《Inorganic Materials》2004,40(9):976-978
NdMCr2O5 (M = Na, K, Cs) and NdMgCr2O5.5 are prepared by solid-state reactions between appropriate oxides and carbonates and are shown to have a tetragonal structure. The heat capacity of these chromites, measured from 298.15 to 673 K, exhibits sharp changes attributable to second-order phase transitions. The C
p
0(T) data are represented by quadratic best fit equations. The electrical resistivity of the chromites is measured between 303 and 493 K. The results attest to semiconducting behavior of the materials in certain temperature ranges. 相似文献
226.
I. A. Grishin V. A. Gur'ev E. B. Intyushin Yu. E. Elliev A. P. Savikin 《Inorganic Materials》2004,40(4):431-433
TeO2–WO3 glasses coactivated with Er3+ and Yb3+ are prepared. The effect of Yb content on the efficiency of Er photoluminescence (PL) in the visible and IR spectral regions is studied. The highest PL efficiency is achieved at an Er : Yb atomic ratio of 1 : 1. The PL lifetime for the Er3+
4
I
13/2 level is determined to be 7–9 ms. 相似文献
227.
The hydrodynamic impact problem is investigated within the framework of potential-flow theory. The vertical load acting on the rigid body is derived based on either momentum or energy conservation, and using the concept of added mass together with a homogeneous Dirichlet condition for the potential on the free surface as usually done to model an impact problem. It is demonstrated that the use of this simplified dynamic free-surface condition, instead of the fully nonlinear one, has a direct influence on the computation of the loads. In particular, the equivalence of momentum and energy analysis is in general not recovered. The situation is then highlighted by performing an asymptotic analysis of the two-dimensional blunt-body asymmetric impact problem. The asymptotic solution is given explicitly and validated through comparisons with experimental results. The energy distribution is then studied. It is shown that the contradiction between momentum and energy analysis can be removed, provided that the flux of energy through the jets is taken into account in the energy balance. If the simplified free-surface condition is indeed valid in the far-field, nonlinear terms must be retained near the body, in the spray-root domains. To leading order, the energy distribution during the gravity-free inertia stage does not depend on the blunt-body shape. The general analysis based on momentum or energy conservation suggests that this result also applies for arbitrary body shape as soon as a homogeneous Dirichlet condition can be applied as a dynamical free-surface boundary condition. In this case, and for a constant vertical impact velocity, half the work performed by the body would seem to be transferred to the fluid as kinetic energy within the spray. 相似文献
228.
Alexander E. Meyerovich 《Journal of Low Temperature Physics》2004,134(1-2):163-168
Similarities between alkali gases in optical lattices with non-integer occupation of the lattice sites and quantum crystals are explored. The analogy with the vacancy liquid provides an agternative explanation to the Mott transition for the recent experiment on the phase transition in the lattice. The vacancy liquid can undergo BEC with T c within experimental reach. Direct and vacancy-assisted mechanisms of the band motion for hyperfine impurities are discussed. The presence of vacancies can resugt in the spatial decomposition of the system into pure hyperfine components. Below BEC for the vacancies, the impurity component resembles 3He in 3He-Hell mixtures. 相似文献
229.
Broadband chaotic oscillations were monitored in a depressed potential collector of a traveling-wave oscillator (TWO). This signal appears due to the oscillations of a virtual cathode, which is formed in the spent electron beam under the action of retarding fields existing in the multistage depressed collector. 相似文献
230.
M. I. Danielyan K. S. Kulakov S. L. Kulakov V. L. Tumanov M. E. Kompan 《Technical Physics Letters》2007,33(7):597-599
A considerable (~1.4-fold) increase in the average output power of a chemical current source has been achieved by means of a periodic pulsed manipulation of the load. A scheme used for the pulse-train loading is presented and mechanisms ensuring an increase in the average output power of the current source are considered. 相似文献