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71.
Terje O. Espelid Jarle Berntsen Knut Barthel 《International journal for numerical methods in engineering》2000,49(12):1521-1545
The linear equations governing the propagation of inertia‐gravity waves in geophysical fluid flows are discretized on the Arakawa C‐grid using centered differences in space. In contrast to the constant depth case it is demonstrated that varying depth may give rise to increasing energy (and loss of stability) using the natural approximations for the Coriolis terms found in many well‐known codes. This is true no matter which numerical method is used to propagate the equations. By a simple trick based on a modified weighting that ensures that the propagation matrices for the spatially discretized equations become similar to skew‐symmetric matrices, this problem is removed and the energy is conserved in regions with varying depth too. We give a number of examples both of model problems and large‐scale problems in order to illustrate this behaviour. In real applications diffusion, explicit through frictional terms or implicit through numerical diffusion, is introduced both for physical reasons, but often also in order to stabilize the numerical experiments. The growing modes associated with varying depth, the C‐grid and equal weighting may force us to enhance the diffusion more than we would like from physical considerations. The modified weighting offers a simple solution to this problem. Copyright © 2000 John Wiley & Sons, Ltd. 相似文献
72.
Trond Kvamsdal Knut Morten Okstad 《International journal for numerical methods in engineering》1998,42(3):443-472
In this paper we investigate an approach for a posteriori error estimation based on recovery of an improved stress field. The qualitative properties of the recovered stress field necessary to obtain a conservative error estimator, i.e. an upper bound on the true error, are given. A specific procedure for recovery of an improved stress field is then developed. The procedure can be classified as Superconvergent Patch Recovery (SPR) enhanced with approximate satisfaction of the interior equilibrium and the natural boundary conditions. Herein the interior equilibrium is satisfied a priori within each nodal patch. Compared to the original SPR-method, which usually underestimates the true error, the present approach gives a more conservative estimate. The performance of the developed error estimator is illustrated by investigating two plane strain problems with known closed-form solutions. © 1998 John Wiley & Sons, Ltd. 相似文献
73.
Vicik R Busemann M Gelhaus C Stiefl N Scheiber J Schmitz W Schulz F Mladenovic M Engels B Leippe M Baumann K Schirmeister T 《ChemMedChem》2006,1(10):1126-1141
A comprehensive screening of N-acylated aziridine (aziridide) based cysteine protease inhibitors containing either Boc-Leu-Caa (Caa=cyclic amino acid), Boc-Gly-Caa, or Boc-Phe-Ala attached to the aziridine nitrogen atom revealed Boc-(S)-Leu-(S)-Azy-(S,S)-Azi(OBn)(2) (18 a) as a highly potent cathepsin L (CL) inhibitor (K(i)=13 nM) (Azy=aziridine-2-carboxylate, Azi=aziridine-2,3-dicarboxylate). Docking studies, which also accounted for the unusual bonding situations (the flexibility and hybridization of the aziridides) predict that the inhibitor adopts a Y shape and spans across the entire active site cleft, binding into both the nonprimed and primed sites of CL. 相似文献
74.
通过2种不同的均匀化热处理及随后的冷轧,使一种3xxx系模型合金获得不同尺寸和分布的弥散析出相,并使铝基体含有不同含量的Mn。系统研究不同均匀化热处理组织和冷轧变形量对退火过程中模型合金的回复与再结晶行为的影响。根据实验结果,绘制出弥散析出相和再结晶过程的相互作用时间-温度-转变曲线(TTT)。TTT曲线显示固溶体中Mn的含量和弥散析出相的颗粒密度对软化行为有强烈的影响。在再结晶退火过程中或再结晶退火之前析出的高密度、细小、弥散析出相显著阻碍软化过程,并形成粗大的再结晶组织。在没有细小、稠密的弥散相影响下的再结晶退火,可以获得均匀、细小的等轴晶。而且,弥散析出相对再结晶过程的阻碍作用取决于再结晶过程的持续时间和弥散析出相的数量。在持续时间长的再结晶过程中,细小、稠密的弥散相对再结晶有着强烈的影响,而在其他情况下影响则有限。不管再结晶过程中是否受到弥散相析出的影响,在再结晶退火之前已经存在于组织中的细小、稠密的弥散相(平均尺寸0.1μm)也会导致再结晶退火之后形成粗大的再结晶组织。 相似文献
75.
Gustafsson A Hillerich K Messing ME Storm K Dick KA Deppert K Bolinsson J 《Nanotechnology》2012,23(26):265704
Cathodoluminescence at 8?K is used to compare the optical properties of AlGaAs-capped GaAs nanowires, grown by metal-organic vapour phase epitaxy and seeded by gold particles prepared by different methods. Six different methods were used to fabricate and deposit gold seed particles onto GaAs substrates: colloid particles, aerosol particles and particles defined by electron beam lithography. The nanowires were grown with and without an in?situ annealing step prior to the nanowire growth. The morphology showed no significant differences between the nanowires. The emissions from ensembles of nanowires have the same peak position, irrespective of seed particle type. Without the in?situ annealing step prior to the nanowire growth, there are significant differences in the emission intensity and emission patterns from nanowires grown from different seed particles. When an in?situ annealing step is included, all the resulting nanowires show identical optical emission intensity and emission patterns. This shows the importance of using an in?situ annealing step prior to growth. This study demonstrates that different preparation methods for gold seed particles can be used to produce GaAs nanowires with highly similar optical properties. The choice of particle preparation method to be used can therefore be based on availability and cost. 相似文献
76.
Torleif André Tollefsen Andreas Larsson Maaike Margrete Visser Taklo Antonia Neels Xavier Maeder Kristin Høydalsvik Dag W. Breiby Knut Aasmundtveit 《Metallurgical and Materials Transactions B》2013,44(2):406-413
Au-Sn solid–liquid interdiffusion (SLID) bonding is an established reliable high temperature (HT) die attach and interconnect technology. This article presents the life cycle of an optimized HT Au-Sn SLID bond, from fabrication, via thermal treatment, to mechanical rupture. The layered structure of a strong and uniform virgin bond was identified by X-ray diffraction to be Au/ζ (Au0.85Sn0.15)/Au. During HT exposure, it was transformed to Au/β (Au1.8Sn0.2)/Au. After HT exposure, the die shear strength was reduced by 50 pct, from 14 Pa to 70 MPa, which is still remarkably high. Fractographic studies revealed a change in fracture mode; it was changed from a combination of adhesive Au/Ni and cohesive SiC fracture to a cohesive β-phase fracture. Design rules for high quality Au-Sn SLID bonds are given. 相似文献
77.
Abstract: Atlantic salmon were subjected to minimal preslaughter crowding stress (Control), short‐term crowding for 20 min (SS‐group), or long‐term crowding for 24 h (LS‐group). The fish were filleted prerigor, cut into 270 g pieces, and packaged in modified atmosphere (60% CO2 and 40% N2). Fillet quality analyses were determined during 22 d of storage at 0.3 °C. Bacterial growth and unpleasant sensory properties increased earlier in the LS‐group. The negative effects of long‐term preslaughter stress were more pronounced for raw than cooked samples, and more pronounced for odor than flavor. Sequence analyses of bacterial DNA at the end of storage revealed that 100% of the bacteria were comprised by Photobacterium phosphoreum of the SS‐ and LS‐group, whereas the Control group also contained 21% of Carnobacterium maltaromaticum (lactic acid bacteria, LAB). Counting of LAB, using Man‐Rogosa‐Sharke agar, similarly showed higher numbers of the Control group after 15 d of storage. A total bacterial count of log 6 CFU/g was observed after 15 d of storage of the LS‐group, which was 3 and 7 d earlier compared with the Control and SS‐group, respectively. Fillet color, texture, and liquid losses were not negatively affected by preslaughter crowding stress. From the sensory and bacterial analyses, it is concluded that long‐term crowding stress accelerates bacterial growth and development of unpleasant sensory properties, hence reduces the shelf life of prerigor modified atmosphere packaged (MAP) salmon. Practical Application: Stressful handling of Atlantic salmon before slaughter resulted in faster reduction of fresh taste and smell, faster bacterial growth, and hence shorter shelf life. The deteriorative effects were more pronounced of raw compared to cooked salmon. Therefore, salmon should be handled carefully in connection with slaughter to avoid impaired welfare and fillet quality, in particularly for fish that is consumed raw, such as sushi. 相似文献
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