室温固相反应法制备纳米氧化锆及表征

以ZrOCl2.8H2O和NH4HCO3为原料,在适量表面活性剂(PEG-400)存在下,先在室温下充分混合研磨进行固相反应,得到的反应混合物再用水洗去其中的可溶性无机盐并烘干,即得氧化锆前驱体。前驱体经530℃下热解3h即得氧化锆产品,采用TG/DTA,XRD和TEM对前驱体及产品进行了表征。结果表明,所得产品氧化锆为结晶良好、以四方相为主的混合晶相,其平均粒径约为25nm。     

PowerBuilder中的用户事件及其应用

PowerBuilder为窗口、用户对象等提供了大量的预定义系统事件，但应用程序有时为了某种特殊要求需要使用用户自定义的用户事件。就此介绍了PowerBuilder中用户事件的定义、触发及其应用实例。     

钢丝圈的失效分析

对72B纺织用钢丝圈进行失效分析，发现钢丝圈使用性能不合格的主要原因是热处理炉仪表指示温度偏差太大及热处理工艺规范不合理，使得球化退火后的金相组织出现粗晶铁素体，淬火和回火后的金相组织出现铁素体、粒状渗碳体，使材料塑性增加，满足不了使用性能。     

Dielectric breakdown of a residual SF6 plasma at 3000 Kunder diatomic equilibrium

A residual plasma at 3000 K and under diatomic equilibrium is left inside an axially blown gas blast SF₆ circuit breaker after the thermal extinction of an arc. The breakdown of such a residual plasma depends on the electron generation and loss mechanisms. Altogether six ionization and chemical reactions relevant to the time scale of breakdown have been taken into account. It has been found that the critical field strength for breakdown is proportional to the pressure and is equal to 2.0 V/(m.Pa). This field strength is in agreement with the experimental results     

SYSNTHESIS AND CHARACTERIZATION OF A NEW COMPOUND K_6Ti_2Nb_(14)O_(42)IN K_2O-TiO_2-Nb_2O_5SYSTEM

A new compound K_6Ti_2Nb_(14)O_(42)was found inthe ternary system K_2O-TiO_2-Nb_2O_5.The compound was char-acterized and investigated by electron,probe,X-ray powderdiffraction and differential thermal analysis.The transpar-ent crystal of light yellow color in form of hexagon-thinplate can be grown by flux method.Further,its crystal struc-ture was determined by four-circle diffratometer K_6Ti_2Nb_(14)O_(42)crystallizes in he(?)(?)(?)onal system with unitcell parameters a=9.1106(5)×10~(-10)m·c=12.0136(9)×10~(-10)m,Z=l andspace.group P6_3/mcm(193).     

基于参考轨迹的自适应模糊Smith控制器

本文提出一种基于参考轨迹的自适应模糊Smith控制器,其模糊决策依据系统响应的参考轨迹,实现对Smith控制器参数的自整定.研究表明,该系统有较高的稳态精度和较强的鲁棒性.     

燃料油硫含量分析准确度影响因素的探讨

研究了硫含量测定的影响因素，探讨了提高汽油中硫含量分析准确度的主要措施．试验结果表明：通过选取适宜的取样量，合适的灯芯疏密、粗细程度和灯芯位置高度及灯芯管内径，调节气流的大小，控制好火焰的形状和大小，可使燃料油中硫含量分析的准确度得到显著提高。     

Molecular dynamics studies of atomic-scale tribological characteristics for different sliding systems

A slider-slab sliding model for hard-to-soft and soft-to-soft sliding systems with abrasive and non-abrasive wear conditions is used to investigate atomic-scale friction. The molecular dynamics simulation uses the Morse potential to calculate interatomic forces between atoms. Separation distance between the slider and the slab is changed to simulate repulsive and attractive interactive force fields exerted on interface between two sliding components. Effects of the interaction potential parameters on the sliding friction are investigated. The relationship of frictional force, normal force and temperature rise of the slider and the slab during sliding are established. Comparison of the hard-to-soft and the soft-to-soft sliding system are carried out and shows different tribological phenomena.     

有机硅—聚氨酯嵌段共聚物合成结构及性能的研究——(1)有机硅预聚体的合成

合成了一系列低分子α,ω-二羟基二甲基硅氧烷齐聚物及1,3-二(3-羟丙基)四甲基二硅氧烷.鉴定了预聚体的结构,选择了最佳合成方法.     

高线二期工程数据采集方式的改进

本文介绍了广钢高线二期工程数据采集系统的改进方案。具体阐述了改进的方法、步骤以及注意事项。 改进后的数据采集系统投入使用一年多来,一直运行稳定,在工艺调整、设备监控,减轻劳动强度等方面发挥了重 要的作用。