Development of high-performance liquid chromatography criteria for determination of grades of commercial olive oils. Part I. The normal ranges for the triacylglycerols

Criteria for authentic olive oils were developed from isocratic high-performance liquid chromatography analyses of 99 olive oils from the major Mediterranean producers in the 1983–1986 crop years. Authentic olive oils include extra virgin, virgin and pure or refined oils, but exclude all reesterified and adulterated oils. The extra virgin through pure grades will have a combined area for the LOO (C_18:2C_18:1C_18:1), LOP (C_18:2C_18:1C_16:0), OOO (C_18:1C_18:1C_18:1), POO (C_16:0C_18:1C_18:1), POP (C_16:0C_18:1C_18:1), and SOO (C_18:0C_18:1C_18:1) peaks between 82.0 and 92.6% of the total area (L, linoleic; O, oleic; P, palmitic; S, stearic). Authentic oils will have ratios of LOO/LOP and OOO/POO that coincide with a line defined by OOO/POO=0.7844(LOO/LOP)+0.0968; correlation coefficient is 0.885. Authentic oils will not have a trilinolein (LLL) peak over 0.5% in area. Neither triolein (OOO) nor any other single peak suffices to characterize an olive oil sample as one of the authentic grades.     

Aromatization of n-butane over new LD-HBS catalysts. Effect of the gallium oxide support

It is shown that even pure quartz, other silicas or aluminas can enhance the aromatization activity of a ZSM-5 zeolite. Incorporation of gallium oxide onto these supports increases further the production of aromatics. The use of supported gallium oxide co-catalyst obtained by co-evaporation of a colloidal silica and a Ga salt has led to extremely high aromatization performance for the hybrid catalyst.     

Polymer electrolytes

Summary The room temperature conductivity of lithium salts dissolved in polyethylene oxide, proposed as polymer electrolytes, is shown to decrease drastically upon storage. The crystallization process, which is responsible for that ageing, can be blocked, if two further components are added : an elastomer copolymer butadiene-acrylonitrile and a macromer of polyoxyethylene. In addition, a crosslinking process must be carried out.     

网格环境下基于传输代价的副本优化策略*

在深入分析影响副本策略性能的各种因素的基础上,将多种因素和传输代价联系起来进行建模,提出一种副本优化策略。优化策略基于传输代价,综合考虑文件访问次数、大小、存在时间等多种因素,并充分利用文件访问次数的集合特征,提供了一个动态、全局的副本管理方法。在网格仿真器OptorSim中对基于传输代价的优化策略进行了实现和评估分析。实验分析证明,优化后的副本策略较现有策略有明显优势。     

“舒特”攻击行动描述与效能评估探要

文章基于UML概念建模语言对“舒特”攻击行动进行了形式化描述,构建了“舒特”攻击行动效能评估指标体系,运用模糊层次分析法对“舒特”攻击行动的效能进行了评估,同时给出了应对“舒特”攻击的建议。     

Characterisation of inelastic power-law fluids using falling sphere data

Two simple methods are presented for the characterization of inelastic power law fluids from falling sphere data. The methods involve the application of shear rate or shear stress correction factors which have been derived theoretically using Slattery's solution for creeping flow about spheres. Flow curves obtained using these methods are in excellent agreement with those measured on a Weissenberg rheogoniometer for 0.83 ≤ n ≤ 1.0. The experimentally determined drag coefficients are found to be in good agreement with the predictions of Slattery's creeping flow first approximation solution. The wall correction factors of Faxen and Francis appear to be valid for inelastic non-Newtonian fluids up to a diameter ratio of at least 0.08.     

面向制造任务的云制造虚拟车间构造方法

针对云制造模式下快速选择和组织相关制造资源、保证制造任务执行的问题,提出一种面向制造任务的云制造虚拟车间构造方法。该方法将制造过程抽象为制造任务执行链,链中的节点对应制造设备云服务或检验云服务,链中的有向边对应物流云服务;并通过行业域、地域和类型域来组织管理云服务,以构造规模较小的候选云服务集,同时减少功能匹配、性能匹配、价格匹配和时间匹配的计算量,达到快速构建云制造虚拟车间的目的。算例分析表明,相比其他方法,该方法能够在更短的时间内完成云服务的选择,并保证所选云服务的服务质量（QoS）在相关域中是更好的。     

田间除草机器人研究进展综述

聚焦田间杂草清除领域,首先介绍了除草机器人的产生背景及其应用价值,并回顾了除草机器人国内外发展现状.然后,重点分析了除草机器人的结构组成及相关技术,并展望了除草机器人的未来发展趋势.最后,作了总结.     

Design of a Sliding Mode Controller with Fuzzy Rules for a 4-DoF Service Robot

In this study, a novel control strategy that combines a fuzzy system and the sliding mode controller is proposed for improving stability and achieving high-accuracy control in service robots. Based on the kinematic and dynamic models of a 4-degrees of freedom manipulator, and the observed tracking error using a low-cost inertial sensor, the proposed fuzzy sliding mode controller (FSMC(IMU)) is designed to generate appropriate torques at robot joints. The FSMC(IMU) controller parameters are adjusted through a fuzzy rule that determines the state of the system. The error in trajectory tracking is reduced through this. The gain value K can be finely adjusted by fuzzy control by observing the degree of vibration after entering the sliding mode surface. The larger the observed vibration value, the faster the fuzzy controller follows the given input trajectory by selecting a smaller gain value K and reducing jitter due to the sliding mode control’s discontinuous switch characteristics. When the degree of error is small, it achieves faster and more accurate control performance than when the observer is not used. The stability of the FSMC(IMU) system is verified via disturbance experiments. The experimental data are compared with the conventional sliding mode controller and proportional-derivative control. The experimental results demonstrate that the proposed FSMC(IMU) controller is stable, fast, and highly accurate in controlling service robots.

     

德惠断陷下白垩统碎屑岩储层特征及控制因素分析

德惠断陷下白垩统登娄库组、营城组、沙河子组储层物性差,勘探风险大.利用岩心观察、铸体薄片鉴定、扫描电镜分析、黏土X线衍射分析等方法,分析储层基本特征、储层成岩作用和控制因素.结果表明:德惠断陷下白垩统碎屑岩储层成分成熟度和结构成熟度较低,储层孔隙类型主要有残余原生孔、次生孔和混合孔,储层物性和孔隙结构较差;压实作用是导致储层物性变差的主要原因,溶蚀作用改善储层物性;纵向上发育2个次生孔隙带,主要形成于中成岩期,次生孔隙带的形成与有机质生烃排酸和断裂有关.研究结果为德惠断陷下白垩统进一步油田勘探提供地质依据,对其他地区类似储层研究有一定借鉴意义.