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Ivan Fortelný Monika Lapčíková František Lednický Zdeněk Starý Zdeněk Kruliš 《Polymer Engineering and Science》2008,48(3):564-571
This article is focused on the phase structure development in immiscible polymer blends during melt mixing. Nonuniformity of the phase structure, i.e., the coexistence of areas containing particles with markedly different size distribution, was detected in quenched and compression molded samples of a number of various blends prepared by long and intensive mixing in the chamber of a Plasticorder. The same effect was found also for polystyrene/polyamide blends prepared in a twin‐screw extruder. It was shown that neglecting nonuniformity of the phase structure can lead to considerable error in evaluation of the effect of system parameters on the blend morphology. The reasons for the effect were discussed and it was found that inhomogeneous flow field in mixers is a plausible explanation of the nonuniform phase structure. POLYM. ENG. SCI., 2008. © 2008 Society of Plastics Engineers 相似文献
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V. Ocelík V. Z. Bengus E. B. Korolkova K. Csach J. Miškuf P. Duhaj 《Journal of Materials Science》1991,26(24):6699-6705
The fracture stress and the critical stress intensity factor of the Fe40Ni40B20 amorphous metallic ribbons 20 μm thick were measured in the temperature range 4.2–300 K and at deformation rates from 3.3×10−6 to 1.25×10−3 m−1 with the aim to obtain more information on the condition for the onset and development of the inhomogeneous plastic deformation
and fracture. 相似文献
5.
P. Podhájecký B. Klápště P. Novák J. Mrha R. Moshtev V. Manev A. Nassalevska 《Journal of power sources》1985,14(4):269-275
A dozen CuO samples prepared under various conditions and from different starting materials were evaluated as cathode materials for a primary Li/CuO cell. The “thin electrode” method was used for rapid evaluation of the samples. Both coulombic efficiency and discharge voltage depend considerably on the method of synthesis. No correlation was found between the specific surface area and the resistivity of the samples on the one hand and the cathode performance on the other. Best results were obtained from CuO prepared by the oxidation of Cu2O under controlled temperature and time of oxidation. 相似文献
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JA Tumlin JP Lea CE Swanson CL Smith SS Edge JS Someren 《Canadian Metallurgical Quarterly》1997,99(6):1217-1223
1. PD 81,723 has been shown to enhance binding of adenosine to A1 receptors by stabilizing G protein-receptor coupling ('allosteric enhancement'). Evidence has been provided that in the perfused hearts and isolated atria PD 81,723 causes a sensitization to adenosine via this mechanism. 2. We have studied the effect of PD 81,723 in guinea-pig isolated atrial myocytes by use of whole-cell measurement of the muscarinic K+ current (I[K(ACh)]) activated by different Gi-coupled receptors (A1, M2, sphingolipid). PD 81,273 caused inhibition of I[K(ACh)] (IC50 approximately 5 microM) activated by either of the three receptors. Receptor-independent I[K(ACh)] in cells loaded with GTP-gamma-S and background I[K(ACh)], which contributes to the resting conductance of atrial myocytes, were equally sensitive to PD 81,723. At no combination of concentrations of adenosine and PD 81,723 could an enhancing effect be detected. 3. The compound was active from the outside only. Loading of the cells with PD 81,723 (50 microM) via the patch pipette did not affect either I[K(ACh)] or its sensitivity to adenosine. We suggest that PD 81,723 acts as an inhibitor of inward rectifying K+ channels; this is supported by the finding that ventricular I(K1), which shares a large degree of homology with the proteins (GIRK1/GIRK4) forming I[K(ACh)] but is not G protein-gated, was also blocked by this compound. 4. It is concluded that the functional effects of PD 81,723 described in the literature are not mediated by the A1 adenosine receptor-Gi-I[K(ACh)] pathway. 相似文献
8.
P. Lobotka I. Vávra Š. Gaži A. Plecenik J. Dérer 《Journal of Low Temperature Physics》1997,106(3-4):381-386
A Josephson junction Nb/Si/Nb with a 10 nm thick amorphous silicon barrier is studied. The upper electrode contains a 2 nm
thick sublayer of amorphous phase adjacent to the barrier, as revealed by cross-sectional TEM. Thus, the junction can be considered
as a S-I-N-S system with the N layer represented by amorphous niobium. Peculiarities in the I–V and Δ(T) dependencies are
observed and explained as a consequence of a proximity effect present in the upper electrode. 相似文献
9.
Dr. P. Bošnjakovié Dipl.-Ing. B. Djokié 《Electrical Engineering (Archiv fur Elektrotechnik)》1992,75(2):131-135
Contents This paper analyzes a problem of phase shifting and deseribes a novel method for electronic reactive energy measurement. The proposed measurement structure, composed of an integrator as a phase shifting circuit and a frequency controlled analog-to-pulse-rate converter, provides for the measurement completely in accordance with IEC definition of reactive energy, which is performed with simple but high performance metering device.
Die Blindverbrauchsmessung anhand eines netzsynchronisierten Analog-Frequenz-Wandlers
Übersicht In diesem Artikel wird das Problem der Phasenverschiebung analysiert und eine neue Meßmethode für elektronische Blindverbrauschsmessung aufgezeigt. Die vorgeschlagene Strucktur, bestehend aus einem Integrator als Phasenschieber und netzkontrolliertem Analog-Frequenz-Wandler, ermöglicht die Verwirklichung eines einfachen aber präzisen Elektrizitätszählers zur Messung der Blindenergie, dessen Arbeitsprinzip mit den IEC Empfehlungen vollkommen übereinstimmt.相似文献
10.
The - transformation of Si3N4 during liquid-phase sintering appears to be controlled by the growth of the -Si3N4 grains in the direction perpendicular to thec-axis in the case of MgO additive. The diffusion through the liquid is the rate-controlling step in the case of the Y4Al5O12 additive. The density of the sintered body at the solid skeleton stage was influenced by the change in the - transformation rate and/or by a change of the transformation mechanism. The indirect proportionality between the -phase content in the starting powder and the density at the solid skeleton stage was found. The microstructure of the sintered body is influenced by both the -phase content in the starting powder and the chemical composition of the additive. Fine, uniform microstructure with a high aspect ratio of -grains is obtained, when the -phase content in the starting powder is as small as possible and when the - transformation is controlled by grain growth. 相似文献