从催化裂化柴油中分离高纯度2,6-二甲基萘

以大庆石油化工总厂炼油厂催化柴油为原料 ,通过精馏分离得到二甲基萘 (DMN)窄馏分 (2 5 8～ 2 70℃ ) ,经糠醛溶剂抽提 ,减压蒸馏后 ,在 -10～ -2 5℃冷冻 2～ 5h ,离心分离制得纯度约 80 %的粗 2 ,6 DMN ,再经无水乙醇在 -10～ -2 5℃重结晶 ,得到纯度大于等于 98%的 2 ,6 DMN。     

TFT-AMLCD绝缘层a-SiNx∶H的制备

用等离子体化学气相沉积法(PECVD)在玻璃基板上淀积了厚度约1μm的非晶氮化硅(a-SiNx∶H)薄膜,在最佳工艺下得到薄膜的性能参数,折射率为1.8左右,光吸收系数为1.2×102～2×102cm-1,相对介电常数为7～8.4,电荷面密度为2.5×1012～3.1×1012cm-2.这种薄膜比较适合于用作薄膜晶体管-有源矩阵液晶显示器(TFT-AMLCD)的栅绝缘层.     

建立军用Foundry的探索

本文从ASIC的基本特点出发,阐述了建立ASIC标准加工线(Foundry)的重要性;国内集成电路产业已经具备建立Foundry的基础,建立有中国特色的Foundry是可以有所作为的。文章介绍了作者在建立军用Foundry方面的探索和初步成果。     

会议电视系统及其发展现状

讨论会议电视系统的组成，种类及设计标准，介绍其发展现状及应用中存在的问题。     

活动式水冷撇渣器的设计及应用

活动式水冷撇渣器是根据高炉冷却壁的工作原理设计的。第一台活动式水冷撇渣器于１９９３年２月２７日在安钢４号高炉投入运行，使用寿命长达１７个月零１８天，通铁量达到４０万ｔ。这种活动式水冷撇渣器具有投产少，收益高，维修方便，安全可靠等优点。     

DNA/lipid complex organogel with shape‐memory behavior

DNA and amphiphilic N,N,N‐trimethyl‐N‐hexadecylammonium bromide (THAB) were stoichiometrically mixed together to produce a DNA–lipid complex, which was dissolved in dimethyl sulfoxide (DMSO) at 65°C and then crosslinked with isophorone diisocyanate (IPDI). The obtained organogel swelled reversibly in DMSO, responding to the variation of temperature. Interestingly, we observed that the gel exhibited a temperature‐dependent shape‐memory behavior. Above 65°C, whatever the shape the gel was deformed to, it could retain the new shape as the temperature was decreased to room temperature, while, when the gel was heated to 65°C again, it could recover its initial shape. The shape‐memory characteristic is supposedly originated from the transition between the close‐packed and the destroyed DNA/lipid conformation. The elastic urethane crosslinking bonds between base‐pair sites act as a fixing phase. The gel holds promise in its application as a gentle actuator. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 259–263, 2002     

贵溪冶炼厂闪速炉炉体第二次改造

介绍贵冶闪速炉炉体两次改造 ,炉体冷却元件的设置及设计特点 ,阐明了设置冷却元件必要性及使用的实际效果。     

反编译程序图设计与控制流分析

反编译是一种能将低级语言翻译到高级语言的工具。本文着重介绍反编译代码存储的程序图方法，以及在程序图基础上，对代码程序进行控制流分析、控制结构提取，给出了结构提取的算法；控制流分析过程中的程序图变换。     

双极型静电感应晶体管开关时间的测量与分析

从理论和实验两方面对静电感应晶体管（ＢＳＩＴ）的开关时间进行了分析和测量，提出了简单的分析方法，将影响ＢＳＩＴ开关时间的各个因素归结为结构因子和材料因子，从而简化了分析影响ＢＳＩＴ开关时间的因素，对于ＢＳＩＴ的实际工艺，结构设计有指导意义。     

Assessment of melt cleanliness in A356.2 aluminium casting alloy using the porous disc filtration apparatus technique: Part II Inclusion analysis

The data obtained on inclusion types and concentrations has been analysed in the present part in terms of their effect on filtration time and fluidity (measured by the length of solidified metal in quartz tubes). The dross, i.e., the oxide layer that formed on the surface of the molten metal, was carefully collected and its mass determined; then it was examined in a scanning electron microscope equipped with an energy-dispersive X-ray system. The results show that inclusions are not the only parameter to be considered. More importantly, it is Al2O3 (films or particles), which seems to be the deciding factor. It is found, however, that it is quite difficult to separate the individual role of each parameter using the porous disc filtration apparatus (PoDFA) technique, i.e., sampling, without disturbing the molten metal. Sampling would introduce undesirable oxides into the PoDFA crucible, resulting in an artificial increase in the filtration time. Increasing the holding periods of the molten metal increases the quantity of dross. In all cases, the skimmed dross is wet, i.e., it contains an appreciable amount of molten metal. The main types of oxides in the dross are MgO, MgAl2O4, Al4C3 and Al2O3. This revised version was published online in November 2006 with corrections to the Cover Date.