东方型300MW循环流化床锅炉开发设计

从东方型300MW循环流化床锅炉的主要技术特点、结构和系统布置等方面,介绍了东方锅炉（集团）股份有限公司在国产化300MW循环流化床锅炉的开发设计上取得的成果,体现了东方自主开发型300MW循环流化床成熟可靠、系统简单,调试运行方便等特色。     

In situ reaction and solid solution induced hardening in (Ti,Zr)B2-(Zr,Ti)C composites

(Ti,Zr)B₂ - (Zr,Ti)C ceramics were synthesized by reactive hot-pressing and solid solution coupling effect using ZrB₂ and TiC powders as starting materials. Effects of sintering temperature on phase relations, microstructure and mechanical properties were reported. The equimolar ZrB₂ and TiC reactants ensured a complete in situ reaction to form (Ti,Zr)B₂ and (Zr,Ti)C solid solutions. The (Ti,Zr)B₂ - (Zr,Ti)C composite sintered at 1750°C was fully densified, and exhibited a high hardness of 29.1 GPa due to fine-grain hardening and solid solution hardening. The optimized comprehensive mechanical properties such as a hardness of 27.9 GPa, a strength of 705 MPa and an indentation fracture toughness of 5.3 MPa m^1/2 were achieved in (Ti,Zr)B₂ - (Zr,Ti)C composites sintered at 1800°C for 1 hour.     

两种组织类型的X70钢级管线钢的带状组织浅析(下)

根据抽检试验和工厂首批出证试验的结果,探讨和分析了铁素体+少珠光体型及针状铁素体型X70钢级管线钢带状组织的特点,带状组织形成与控轧及控冷工艺和钢的化学成分尤其是Mo的含量的关系,以及带状组织程度对钢管母材夏比冲击韧性、DWTT试验SA值、抗HIC性能的影响。     

一种检测运行栈与静态数据区重叠的新方法

嵌入式系统中由于内存限制,容易出现运行栈和数据区重叠的错误。已有的两种检测该错误的方法在准确性和易用性方面存在缺陷,不适用于基于软件模拟器的大规模回归测试。文章通过改变运行栈与静态数据区的布局,将运行栈与静态数据区重叠的错误转化为运行栈超越内存地址空间的错误。新方法大大简化了这种运行时错误的检测和调试。     

低温甲醇洗系统贫富甲醇换热器泄漏原因分析及处理

介绍了晋煤天溪煤制油分公司低温甲醇洗系统贫富甲醇换热器的泄漏情况。分析了贫富甲醇换热器泄漏初期生产运行指标的异常现象和造成泄漏的原因,认为泄漏是不同物质对设备的腐蚀、冲刷造成的,并针对泄漏的具体情况,提出了不同的检修处理措施:管束泄漏量低于10%时,可采用焊接锲形堵头将泄漏列管两端进行封堵;管束泄漏量高于10%时,如换热器设计余量足,可将封头内部隔板取出,短接进出口;将换热管材质由10#钢换为06Cr19Ni10不锈钢。     

高钛型高炉渣光催化材料研究进展

本文简介了攀钢高钛型高炉渣的利用现状及存在的问题,综述了国内高钛型高炉渣制备光催化剂研究现状,认为高钛型高炉渣是一种具有光催化降解能力的材料,探索不同的方式进行改性以增强其光催化效应是未来制备优质高炉渣光催化材料的研究方向。同时,提出了高钛型高炉渣光催化材料应用方向和可能生产的环保产品。     

内蒙古阿巴嘎旗更新世阿巴嘎组火山岩岩石化学特征及成因

阿巴嘎旗位于内蒙古中东部,区内广泛发育上更新统阿巴嘎组。通过对区内火山岩岩石地球化学特征及其成因进行分析,结果表明：岩石组合由橄榄玄武岩、伊丁石化玄武岩和少量火山碎屑岩组成;岩石具有富钛,富镁,钠高钾低的特点,岩浆结晶分异程度较低,岩浆物质来源较深,其物源具有幔源成因的特点;该套火山岩为板内玄武岩。     

Unique orientation of lamellae in film processed poly (phenylene sulfide)

The morphology of poly(phenylene sulfide), PPS, obtained as processed film has been studied using wide angle X-ray scattering (WAXS), scanning electron microscopy (SEM), and differential scanning calorimetry (DSC). A unique morphology has been identified in the original film. The spherulites are very small in size and possess a cylindrical symmetry with their lamellae oriented on the edge. In these processed PPS films, the a-axis of the lattice is preferentially aligned perpendicular to the film plane, while the b and c axes are predominantly in the film plane. In the PPS isothermally crystallized from the melted, original film, there is no such preferential orientation. Thermal analysis of the original and melt crystal-lized PPS shows that while the degree of crystallinity is about the same, the nature of the amorphous phase in the two materials is different. In the original film, we did not observe a heat capacity increment at a glass transition temperature by DSC, indicating that all of the amorphous phase belongs to the category of rigid amorphous phase. In the melt crystallized PPS, a distinct glass transition was seen, though only a portion of the amorphous phase becomes mobile at T_g. The differences in orientation and mobility of the amorphous phase in the original film compared to melt crystallized PPS are explained by the different thermal processing procedures used for the two materials.     

马来酸酐熔融接枝LDPE的性能

采用熔融接枝法制备了低密度聚乙烯(LDPE)与马来酸酐(MAH)接枝物,通过调整反应物的用量及反应条件控制接枝率。随着MAH及引发剂用量的增加,接枝率呈先增大后降低的趋势。低剪切速率时,接枝物的最大初始剪切黏度达4750 Pa·s,远高于纯LDPE;高剪切速率时,接枝物的剪切黏度与纯LDPE趋于相同,约500 Pa·s。接枝物的拉伸强度在8 MPa左右,同纯LDPE接近,断裂伸长率略有下降。