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排序方式: 共有517条查询结果,搜索用时 234 毫秒
41.
Oleksandr Chernyavskiy Luca Vannucci Paolo Bianchini Francesco Difato Mustafa Saieh Lucie Kubínová 《Microscopy research and technique》2009,72(6):411-423
We investigated possibilities of the combination of the one- and two-photon excitation microscopy for examination of the experimental melanoma tissue in vivo, in mice under general anesthesia, and ex vivo on freshly harvested specimens. Our aim was to obtain sufficiently informative images of unstained tumor tissues and their modifications after hyperthermia treatment. The mouse experimental melanoma structure was studied and compared with normal tissue from the same animal by using confocal and nonlinear microscopy techniques based on (i) one-photon excitation (1PE) fluorescence, (ii) 1PE reflectance, (iii) second harmonic generation imaging, and (iv) two-photon excitation autofluorescence. We checked different spectral conditions and other settings of image acquisition, as well as combinations of the above imaging modalities, to fully exploit the potential of these techniques in the evaluation of treated and untreated cancer tissue morphology. Our approach enabled to reveal the collagen fiber network in relation with the other tissues, and to identify invasive tumor cells. It also proved to be useful for the examination of interrelationships between functional and morphological aspects based on optical properties of the tissues, especially in studies of changes between the tumor and control tissue, as well as changes induced by physical treatments, e.g., delivery of microwave hyperthermia treatment. These differences were also evaluated quantitatively, when we found out that the maximum Euler–Poincaré characteristic reflects well the melanoma morphological structure. The results showed that the proposed investigative approach could be suitable also for a direct evaluation of tissue modifications induced by clinical interventions. Microsc. Res. Tech., 2009. © 2009 Wiley-Liss, Inc. 相似文献
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Saptarshi Sasmal K. Ramanjaneyulu Balthasar Novák V. Srinivas K. Saravana Kumar Christian Korkowski Constanze Roehm N. Lakshmanan Nagesh R. Iyer 《Construction and Building Materials》2011,25(1):175-182
The paper discusses the aspects of repair and retrofitting technique adopted for a damaged reinforced concrete beam-column joint specimen under cyclic loading. A specimen designed based on Indian Standard specifications with consideration of seismic load but without adopting ductile detailing (NonDuctile) was investigated under reverse cyclic loading. Then, the damaged nonductile specimen was repaired with epoxy mortar and grouted using low viscous polymer, and retrofitted using fiber reinforced plastic (FRP) wrapping in beam and column components and steel plate jacketing in joint region. The experimental results showed that the retrofitted specimen not only regained its original strength and stiffness but also has overcome the deficiencies of nonductile detailing. The present study shows that a proper repair and adequate retrofitting technique can be used for strengthening and improvement of damaged regions in reinforced concrete structures. 相似文献
45.
Zdeněk Sobalík Kamil Jíša Dalibor Kaucký Alena Vondrová Zdeňka Tvarůžková Jana Nováková 《Catalysis Letters》2007,113(3-4):124-129
The decomposition of nitrous oxide was studied over Fe-ferrierite, Me-ferrierites and Fe/Me-ferrierites (Me: Pt, Rh and Ru).
Flow as well as batch experiments were carried out and showed a synergy between Fe and Me ions. Ions of noble metals in Fe-ferrierite
increased the catalytic activity in the sequence Pt < Rh ≅ Ru. Addition of NO substantially decreased the decomposition of
N2O over Rh/ferrierite and Ru/ferrierite, but not over bimetallic ferrierites. NO
x
species created during the decomposition of nitrous oxide alone as well as with addition of NO, and employment of nitrous
oxide labeled with 18O allowed us to assume a changing decomposition mechanism in the presence of Me ions in Fe-ferrierites. 相似文献
46.
This paper presents a thermodynamic investigation of the benzene physical and chemical organogels, using differential scanning calorimetry (DSC) and intends to draw an appropriate relationship between the gel network structure and the properties. Physical gels, formed by an aluminium soap of fatty acid, and chemical gels, created by in situ cross‐linking of a siloxane copolymer are investigated. The effects of the type and quantity of the gelators and their corresponding network mesh size distribution in the gels on crystallization, melting, and their kinetics are examined. It appears that the kinetics of crystallization of the entrapped solvent is significantly affected by the quality of the gel network scaffolding and can be treated successfully by the Avrami equation of crystallization. From the melting behavior of the entrapped solvent crystallites, quantitative information about the number of solvent molecules bound per molecule of the gelator has been extracted. DSC proves to be a reliable technique to evaluate the population distribution of solvent molecules trapped in the physical and chemical organogel network scaffolding. The state of the solvent may be treated as a probe to understand the structure of the gels. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 94: 1253–1264, 2004 相似文献
47.
J. Novák J. Šoltýs P. Eliáš S. Hasenöhrl I. Vávra 《Materials Science in Semiconductor Processing》2010,13(3):167-172
The growth of InMnAs quantum dots by low pressure MOVPE technique on patterned (1 0 0) GaAs substrates was studied. The patterning in the form of ridges with sidewalls having (2 1 1) and (3 1 1) facets was prepared by wet chemical etching via a GaAs/AlAs sacrificial etching mask structure. AFM studies showed that the dots formation and distribution were very similar for both types of facets under study. InMnAs dot density on the (3 1 1) plane is about 5–7 times lower in comparison to that on the (1 0 0) planar substrate. The dots on sidewalls are larger in comparison to average dots formatted on planar GaAs (1 0 0) substrate. The lateral dimensions of these dots are in the interval 100–180 nm. In addition, dot distribution along the sidewall (from top to bottom) is not uniform. A higher dot concentration was observed close to the intersection of (3 1 1) facets with concave bottom part of the valleys between ridges. Finally, no dots were grown on the (1 0 0) plane created by self-faceting on the top of the triangular ridges. This is probably a consequence of the high quality of the (1 0 0) facet formed by lateral overgrowth. 相似文献
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49.
Jana LudvíkováKvěta Jirátová Jan KlempaVlasta Boehmová Lucie Obalová 《Catalysis Today》2012,179(1):164-169
Catalytic activity of the Co-Mn-Al mixed oxide catalysts (Co:Mn:Al molar ratio of 4:1:1) supported over titania was examined in total oxidation of ethanol. The prepared catalysts were characterized by chemical analysis (AAS), surface area measurements, and temperature programmed techniques (TPR, TPD). In ethanol oxidation, the catalysts activity gradually increased with increasing active phase content. Low concentration of Co-Mn-Al oxides in the catalyst negatively affected formation of reaction byproducts: carbon monoxide production steeply increased when Co + Mn metals concentration were lower than 5 wt.%. On the other hand, formation of the second main reaction intermediate, acetaldehyde was limited, when acidity of the catalyst was not high, i.e. concentration of Co-Mn metals over titania was low. 相似文献
50.
The nonlocal probabilistic theory developed in Part I is applied in numerical studies of plain concrete beams and is compared to the existing test data on the modulus of rupture. For normal size test beams, the deterministic theory is found to dominate and give adequate predictions for the mean. But the present probabilistic theory can further provide the standard deviation and the entire probability distribution (calculated via Latin hypercube sampling). For very large beam sizes, the statistical size effect dominates and the mean prediction approaches asymptotically the classical Weibull size effect. This is contrary to structures failing only after the formation of a large crack, for which the classical Weibull size effect is asymptotically approached for very small structure sizes. Comparison to the existing test data on the modulus of rupture demonstrates good agreement with both the measured means and the scatter breadth. 相似文献