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91.
The present work investigates the relationships between the microstructural state and fracture properties in commercial polypropylene‐based materials. In this case an isopolypropylene homopolymer and three ethylene propylene block copolymers (EPBC) with different ethylene content (EC) have been studied. A variety of morphologies were obtained by a combination of several processing methods (injection molding, injection molding‐annealing, and compression molding) and thickness. Fracture behavior of deeply double‐edged notched specimens was evaluated by scanning electron microscopy (SEM) and by the essential work of fracture (EWF) method, analyzing the influence of processing, thickness (t), EC, and orientation respect to melt flow direction (MD and TD). The testing direction and EC are the most relevant variables that affect the ability of the crack tip to deform plastically during the crack propagation, determining the final fracture behavior. The fracture parameters obtained with the EWF method, specific EWF, we, and plastic item, βwp, have proved to be very sensitive to the processing induced morphology, finding interesting relationships between such morphologies (characterized by crystallinity index, orientation level, and skin/core ratio) and the fracture parameters of the plaques. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 2714–2724, 2006 相似文献
92.
This retrospective analysis was conducted between May 1997 and May 2000 at the Centro de Atención Nutricional Infantil de Antímano, CANIA, in Caracas, Venezuela to assess the efficacy of two treatments (ambulatory versus day-care) of mild and moderate malnourished children. Inclusion criteria were: children under 10 years old with mild and moderate malnourishment, who attended a minimum of 3 control visits during a period of 12 months. One hundred fourteen malnourished children were included: fifty seven in ambulatory treatment and fifty seven in day-care treatment paired per nutritional diagnosis, gender and age (thirty nine mild and eighteen moderate malnourished children). The nutritional recovery criterion was weight for height above tenth percentile. No relation was found between treatment approaches and nutritional recovery at 3 and 6 months of treatment. In the group of mild malnourished children, the percentage of recovered patients at 3 months of treatment, that kept their recovered condition at 6 months was 83% (15/18) in the ambulatory treatment and 82% (18/22) in the day-care treatment Age of children, associated disease, acute morbidity, dietetic risk and mother's education and age were not associated with nutritional recovery at 6 months of treatment (p > 0.05). The day-care approach resulted as effective as ambulatory in mild malnourished children. In moderate malnourished new studies will need to be conducted with greater number of patients. 相似文献
93.
Jhon Harley Muñoz Romero Cindy Alejandra Sepúlveda Cadavid Natalie Cortés Julián Esteban López Correa 《臭氧:科学与工程》2020,42(1):36-42
ABSTRACTIn this study, the efficiency of gaseous ozone (O3) injected in the soil as an oxidizing agent for the inactivation of F. oxysporum was evaluated under laboratory conditions. The results show the treatment reached an inactivation efficiency of 76% after an applied dose of 0.40 g O3 kg ?1 soil. This shows that the injection of O3 can be a viable alternative to control pathogenic organisms in the soils. Nevertheless, it is clear that more studies on determining the effects of this treatment on soil quality are needed. 相似文献
94.
95.
Henri Berthiaux Antonio Guttierrez Lavin Julio Bueno De Las Heras Marisol Muñiz Alvarez 《加拿大化工杂志》2007,85(2):158-170
Despite of its general use in industry, particle sedimentation is still a not well understood unit operation. Hydrodynamics is complex in essence, mainly because the possible volumes are depending on the operating conditions, which in turn has consequences on the stability of the equipment in unsteady state conditions. 相似文献
96.
Crystallization of hydrogenated sunflower-cottonseed oil 总被引:1,自引:0,他引:1
G. Rivarola J. A. Segura M. C. Añón A. Calvelo 《Journal of the American Oil Chemists' Society》1987,64(11):1537-1543
Crystal structures formed during solidification of hydrogenated cottonseed oil, sunflowerseed oil and their blends were analyzed
by using an X-ray diffraction technique, differential scanning calorimetry (DSC) and polarized light microscopy. Temperatures
and times of crystallization under conditions which tend to produce β′ type structures were determined in terms of refrigeration
parameters. Microscopy with polarized light also helped clarify some aspects of the tridimensional network of crystals that
contribute to the consistency of products made from hydrogenated oils. 相似文献
97.
CuS pineal microspheres congregated from interleaving nanoflakes with thickness of 40 to 200 nm were synthesized by a pyridine-solvothermal process via the reaction between cupric chloride(CuCl2·2H2O) and thioacetamide(TAA,CH3CSNH2).The products were characterized by X-ray diffraction and scanning electron microscopy.UV-Vis absorption spectrum,excitation and photoluminescence spectra of CuS pineal microspheres were obtained at room temperature to investigate their optical properties.A possible growth mechanism on the formation of CuS pineal microspheres is proposed.The factors influencing the evolution of morphologies of CuS crystals including the dosage of the reactants,surfactant,and sulphur-source were also analyzed. 相似文献
98.
R. A. Torres J. Arellano-Ceja M. E. Hernández-Hernández R. González-Núñez 《Polymer Bulletin》2007,59(2):251-260
Summary The effects of blending sequence and the addition of an interfacial agent (triblock copolymer styrene-butylene ethylene/styrene,
Kraton G1652) on the morphology and the mechanical properties of Polycarbonate (PC)/Polypropylene (PP) blends prepared by
injection molding were studied. This study presents an analysis of impact resistance, tensile properties and morphology of
the raw materials and the blends at different compositions. The blends, before being injected, were prepared in a twin-screw
extruder by different sequences of blending. The results indicate that the blending sequence and the presence of humidity
significantly affect the properties and morphology of the blends. For ternary blends (PC/PP/Kraton), only one-step mixing
before injection molding proved to be sufficient to improve mechanical properties. Increasing the amount of blending steps
did not present a significant change in properties. With the addition of the interfacial agent, higher impact resistance and
particle size reduction were observed. 相似文献
99.
Antonio G. González Ignacio A. Jiménez Mercedes P. Núñez Angel G. Ravelo Isabel L. Bazzocchi Orlando M. Muñoz Marcelino A. Aguilar 《Journal of chemical ecology》1994,20(4):823-830
Three new dihydro--agarofuran sesquiterpenes from two species ofMaytenus were isolated and their structures were elucidated by means of1H and13C NMR studies. The differences and similarities noted in the chemical content of the dihydro--agarofuran sesquiterpenes from the fourMaytenus species from Chile are in line with the taxonomic characterization of these species; their geographical distribution is also given. 相似文献
100.
The attractiveness of different synthetic host odors and a synthetic aggregation pheromone (grandisoic acid [GA]) to overwintered adult plum curculios (PCs), Conotrachelus nenuphar (Herbst) (Coleoptera: Curculionidae), was examined using two types of traps (sticky panels and black pyramids) placed in border areas surrounding an unsprayed section of an apple orchard in Massachusetts. In 2001, we evaluated the response of PCs to three synthetic fruit volatiles (benzaldehyde [BEN], ethyl isovalerate [EIV], and limonene [LIM]) assessed alone and in combination with GA, as well as the response to GA alone and a no-odor (control) treatment. BEN was the only host volatile that synergized the response of PCs to GA for both trap types. For both trap types, GA was as attractive to PCs as a single component as when in combination with either EIV or LIM. In 2002, four release rates of BEN (0, 2.5, 10, and 40 mg/day) and two release rates of GA (1 and 2 mg/day) were evaluated for attractiveness to PCs using panel and pyramid traps. For panel traps, an increase in amount of GA released (from 1 to 2 mg/day) was associated with a 35% increase in captures. However, PC captures by pyramid traps were similar regardless of the amount of GA released. For panel traps, 10 and 40 mg/day of BEN were the most attractive release rates regardless of the amount of GA released. For pyramid traps baited with GA. PC captures were enhanced by the presence of BEN, regardless of release rate. In 2003, GA at 1 mg/day + BEN at 80 mg/day of release did not enhance PC captures by panel traps relative to lower release rates of BEN. Pyramid traps releasing GA at 1 mg/day performed best when baited with BEN at 10 mg/day of release; a release rate of 80 mg/day of BEN decreased the attractiveness of the binary combination of BEN + GA. Combined results suggest that BEN at 10 mg/day + GA at 1 mg/day of release constitutes an attractive lure that may improve the effectiveness of monitoring traps for PCs. 相似文献