Rh(Ⅲ)—钍试剂—高碘酸钾新体系催化光度法测定痕量铑

在pH3.9醋酸盐缓冲溶液中及加热条件下,Rh(Ⅲ)对高碘酸钾氧化钍试剂这一褪色反应有强烈的催化作用,可藉自来水冷却中止反应,研究了催化光度测定痕量铑的影响因素,建立了一个检出限和测定范围分别为0.06ng/ml和0.12～4.5ng/ml铑的催化光度新方法。     

Performance of positive and negative electrodes in amorphous manganese oxide supercapacitor

Using potassium permanganate and acetic manganese as the reactants, amorphous manganese oxide was prepared with mechanochemical method. XRD was used for microstructure characterization, while cyclic voltammetry and constant current charge-discharge were used for electrochemical performance testing. The positive electrode （PE） and negative electrode （NE） were investigated respectively in amorphous manganese oxide supercapacitor, aiming to find their different performances in charging-discharging. The results show that the crystalline structure is destroyed in both the PE and NE material during charge-discharge process. Thereinto, the NE suffers a bit more seriously. When cycling, the PE potential scope diminishes while the NE potential scope enlarges. The increased inner resistance makes the NE curves almost bended to be a right angle, but not the PE curves. The cell＇s equivalent series resistance （ESR） is more dependent on the NE, and the capacitance is mainly determined by the rapid descent of the NE potential range. The capacitances of the NE are highly rate-dependent, decreasing from 121.3 to 53.1 F/g, by 56.2%, over the range of 5-25 mV/s. However, the PE appears to be weakly dependent and its capacitance is only dropped by 22.1%.     

A THERMODYNAMIC INVESTIGATION ON SPINODAL DECOMPOSITION BOUNDARY IN Cu－Ti ALLOYS

ＡＴＨＥＲＭＯＤＹＮＡＭＩＣＩＮＶＥＳＴＩＧＡＴＩＯＮＯＮＳＰＩＮＯＤＡＬＤＥＣＯＭＰＯＳＩＴＩＯＮＢＯＵＮＤＡＲＹＩＮＣｕ－ＴｉＡＬＬＯＹＳ￥ＷｅｉＹｉｎｇｈｕｉ；ＷａｎｇＸｉａｏｔｉａｎ（ＩｎｓｔｉｔｕｔｅｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎ...     

Redundancy filtering and fusion verification for video copy detection

Multimedia Systems - Recently, the frame fusion based video copy detection scheme provides a possibility to detect copies in a continuous query video stream. However, its computational complexity...     

L波段微波功率合成技术研究

无人机机载功率放大器的性能一直是限制无人机技术发展的主要因素,为此提出了将功率合成技术应用于无人机数据系统的方法解决上述问题。利用微带线技术结合系统性的电路调试方法,辅以Advanced Design System仿真软件优化设计,同时采用实频技术法进行宽带功放设计,成功研制了频段在1.3 GHz~1.7 GHz的功率放大器,单路功率放大器采用级联的技术输出功率为8 W,两路合成后,实测总输出功率为15.67 W,合成效率达97%,性能稳定,达到实用水平。     

三轴旋转式惯导平台框架控制耦合问题研究

在三轴旋转式惯导系统中,框架的控制性能对导航精度影响尤为重要,而耦合是影响惯性平台控制精度的原因之一。针对三轴旋转式惯导平台,对三框架的惯量耦合、动力学耦合进行了分析,并建立了相应的耦合模型,在此基础上得出了耦合给框架控制带来的影响,为三轴旋转式惯导平台的框架控制提供了理论基础。     

Pure spatial rich model features for digital image steganalysis

The SRM (Spatial Rich Model) is a very effective steganalysis method. It uses statistics of neighboring noise residual samples as features to capture the dependency changes caused by embedding. Because the noise residuals are the high-frequency components of image and closely tied to image content, the residuals of different types of image regions have different statistical properties and effectiveness for steganalysis. In this paper, the effectiveness of the residuals is investigated. Then the effectiveness of the statistics collected from different types of neighboring residual samples is investigated from the FLD (Fisher Linear Discriminant) viewpoint, and ineffective, effective and high-effective neighboring residual samples are defined. The ineffective neighboring residual samples are not likely to change during embedding, and if they are counted in statistics, they may mix the features with noise and make the features impure. Pure SRM features are extracted based on neighboring noise residual sample selection strategy. Furthermore, multi-order statistical features are proposed to increase the statistical diversity. Steganalysis performances of the statistical features collected from different types of neighboring residual samples are investigated on three content adaptive steganographic algorithms. Experimental results demonstrate that the proposed method can achieve a more accurate detection than SRM.     

Image inpainting algorithm based on TV model and evolutionary algorithm

With the development of modern image processing techniques, the numbers of images increase at a high speed in network. As a new form of visual communication, image is widely used in network transmission. However, the image information would be lost after transmission. In view of this, we are motivated to restore the image to make it complete in an effective and efficient way in order to save the network bandwidth. At present, there are two main methods for digital image restoration, texture-based method and non-textured-based method. In the texture-based method, Criminisi algorithm is a widely used algorithm. However, the inaccurate completion order and the inefficiency in searching matching patches are two main limitations of Criminisi algorithm. To overcome these shortcomings, in this paper, an exemplar image completion based on evolutionary algorithm is proposed. In the non-textured-based method, total variation method is a typical algorithm. An improved total variation algorithm is proposed in this paper. In the improved algorithm, the diffusion coefficients are defined according to the distance and direction between the damaged pixel and its neighborhood pixel. Experimental results show that the proposed algorithms have better general performance in image completion. And these two new algorithms could improve the experience of network surfing and reduce the network communication cost.     

岩土工程勘察的重点分析

近年来,岩土工程勘察技术发展得非常快,研究领域不断拓展,取得了较多的成就。但是,在发展过程中也存在一些不足。重点分析了岩土工程勘察工作,并结合实际工作提出一些个人意见,以期能为相关工作提供帮助。