全文获取类型
收费全文 | 664篇 |
免费 | 29篇 |
国内免费 | 1篇 |
专业分类
电工技术 | 34篇 |
化学工业 | 220篇 |
金属工艺 | 16篇 |
机械仪表 | 11篇 |
建筑科学 | 22篇 |
矿业工程 | 1篇 |
能源动力 | 24篇 |
轻工业 | 91篇 |
水利工程 | 6篇 |
无线电 | 48篇 |
一般工业技术 | 119篇 |
冶金工业 | 28篇 |
原子能技术 | 23篇 |
自动化技术 | 51篇 |
出版年
2022年 | 11篇 |
2021年 | 13篇 |
2020年 | 4篇 |
2019年 | 16篇 |
2018年 | 13篇 |
2017年 | 10篇 |
2016年 | 21篇 |
2015年 | 18篇 |
2014年 | 29篇 |
2013年 | 34篇 |
2012年 | 43篇 |
2011年 | 46篇 |
2010年 | 34篇 |
2009年 | 30篇 |
2008年 | 45篇 |
2007年 | 33篇 |
2006年 | 25篇 |
2005年 | 31篇 |
2004年 | 20篇 |
2003年 | 19篇 |
2002年 | 14篇 |
2001年 | 9篇 |
2000年 | 17篇 |
1999年 | 12篇 |
1998年 | 16篇 |
1997年 | 12篇 |
1996年 | 13篇 |
1995年 | 13篇 |
1994年 | 5篇 |
1993年 | 6篇 |
1992年 | 10篇 |
1991年 | 9篇 |
1990年 | 5篇 |
1989年 | 9篇 |
1988年 | 5篇 |
1987年 | 6篇 |
1986年 | 3篇 |
1985年 | 5篇 |
1984年 | 3篇 |
1983年 | 3篇 |
1982年 | 8篇 |
1981年 | 2篇 |
1980年 | 2篇 |
1979年 | 4篇 |
1977年 | 2篇 |
1976年 | 1篇 |
1975年 | 1篇 |
1974年 | 2篇 |
1972年 | 1篇 |
1970年 | 1篇 |
排序方式: 共有694条查询结果,搜索用时 31 毫秒
41.
Satoh M Sakaguchi M Kobata M Sakaguchi Y Tanizawa H Miura Y Sasano R Nakanishi Y 《Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan》2003,44(1):7-12
We studied the effect of cleaning and cooking on the residues of flutolanil, fenobucarb, silafluofen and buprofezin in rice. The rice had been sprayed in a paddy field in Wakayama city, with 3 kinds of pesticide application protocols: spraying once at the usual concentration of pesticides, repeated spraying (3 times) with the usual concentration of pesticides and spraying once with 3 times the usual concentration of pesticides. The residue levels of pesticide decreased during the rice cleaning process. Silafluofen, which has a higher log Pow value, remained in the hull of the rice. Fenobucarb, which has a lower log Pow value, penetrated inside the rice. The residue concentration of pesticide in polished rice was higher than that in pre-washed rice processed ready for cooking. During the cooking procedure, the reduction of pesticides in polished rice was higher than that in brown rice. 相似文献
42.
Kanda M Ushiyama K Igusa K Murayama M Horie M Hirokado M Miyazaki T 《Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan》2003,44(2):110-113
A simple and rapid determination of anticoccidial drug residues, diclazuril (DCZ) and nicarbazin (NCZ), in chicken tissues has been developed. DCZ and NCZ were extracted with acetonitrile from chicken liver, muscle, and fat. The extract was rinsed with n-hexane saturated with acetonitrile and then evaporated. The residue was dissolved in 1.4 mL of acetonitrile-methanol (1:1), then 1.0 mL of n-hexane saturated with acetonitrile-methanol (1:1) was added, and the mixture was partitioned by the addition of 0.6 mL of water. DCZ and NCZ in the aqueous layers were determined by HPLC on an Xterra RP-18 column with acetonitrile-0.5% ammonium acetate containing 0.01 mol/L tetra-n-butylammonium hydrogen sulfate (43:57) as the mobile phase. The mean recoveries (n = 5) of DCZ and NCZ spiked in chicken tissues at the maximum residue levels were 92.0-95.6% (CV 2.4-3.0%) and 87.3-89.4% (CV 1.7-2.8%), respectively. The detection limits of DCZ and NCZ were 0.01 and 0.004 microgram/g, respectively. 相似文献
43.
Tomoyuki Kakigi Nozomi Miyoshi Kazuki Fujii Tatsuya Urakawa Akio Matsuura Takaharu Miura Masakazu Washio 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2007,265(1):118-124
Poly (tetrafluoroethylene-co-perfluoroalkylvinylether) (PFA) was irradiated by soft electron beam (soft-EB) under nitrogen gas atmosphere in solid-state and its molten state, respectively. The changes of thermal property and chemical structures of irradiated PFA in solid-state and molten state were studied by differential scanning calorimetric analysis (DSC) and solid-state 19F magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectroscopy. By DSC analysis, the melting temperature shifted to lower temperatures, and crystallinity decreased with increasing soft-EB dose. By solid-state 19F MAS NMR spectroscopy, the new signals was observed and the detected new signals in irradiated PFA at 315 °C and at 30 °C were due to the tertiary carbon group with branching site (Y-type crosslinking site), perfluoro-propylene site and chain end methylene groups, respectively.Moreover, the molar ratio of perfluoroalkylvinylether (FAVE) structure to -CF2- units decreased with increasing dose. 相似文献
44.
Determination of bisphenol A in canned vegetables and fruit by high performance liquid chromatography 总被引:4,自引:0,他引:4
Terumitsu Yoshida Masakazu Horie Youji Hoshino Hiroyuki Nakazawa 《Food Additives & Contaminants》2001,18(1):69-75
A high performance liquid chromatograph y (HPLC) method was developed for the determination of bisphenol A (BPA) that had migrated into canned fruit and vegetables. BPA was extracted with acetonitrile from the solid portion of canned food, and with an OASIS HLB cartridge from the aqueous portion, respectively. Both extracts were cleaned up on a Florisil cartridge. The HPLC separation was carried out on a Wakosil II 3C18 RS column (4.6 × 150mm) with acetonitrile-water (40:60, v/v) as a mobile phase with a flow rate of 0.8 ml/min. BPA was detectable by UV detector at 228 nm and determined with the similarity of chromatographic peak spectrum by multiwavelength detector (similarity index was 0.99 or above). The quantification limits were 10 ng/g for the solid portion and 5 ng/ml for the aqueous portion, respectively. BPA was mainly detected in the solid portion of canned food and found at the maximum level of 11 μg per can. To verify migration into the solid portion of canned food, a partitioning experiment was carried out. 相似文献
45.
46.
Masakazu Ejiri Haruo Yoda Hiroshi Sakou Yuzaburo Sakamoto 《Machine Vision and Applications》1989,2(3):155-166
Combining the knowledge-based processing with image processing is considered a key issue in the future of visual inspection of complex patterns such as multilayered semiconductor wafers. However, present technology restricts this combination, mainly because of the exhaustively long time usually required for each type of processing. To cope with this situation, a unique knowledge-directed image processing method is proposed, in which every image processing step is controlled in real time by parametric knowledge driven by design patterns. The resulting structure of the image processor is a pipeline, in which each piece of knowledge is embodied as a combination of a hardware processing unit and control unit. In this paper the types of knowledge and their implementation are explained, and an inspection machine for logic IC wafers based on this pipelined knowledgedirected image processing is introduced. 相似文献
47.
The effect of the constituting amino acid residue [Glu(OBzl)] number on the chiral recognition ability was investigated. Chiral recognition sites were prepared from oligopeptide derivatives (constituting amino acid residue number = three–five) by adopting alternative molecular imprinting. It was made clear that with a constituting amino acid residue number of four, the tetrapeptide derivative of Glu(OBzl) is the best candidate material to generate a chiral recognition site among eight types of oligopeptide derivatives in the study. The affinity constant between Ac‐L ‐Trp and a chiral recognition site ranged from 3.4 × 103 to 1.08 × 104 mol?1 dm3, depending on the number of Glu(OBzl) residues in an oligopeptide derivative. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 95: 1302–1309, 2005 相似文献
48.
The dehydrofluorination of poly(vinylidene fluoride) (PVDF) powder and films was studied using several kinds of base solution. Especially the reactivity of 1,8-diazabicyclo[5.4.0]-7-undecene (DBU) in ethanol, KOH in 2-propanol and aqueous NaOH solution with tetrabutylammonium bromide was investigated by the change in infrared (IR) and ultraviolet-visible (UV-VI) absorptions of PVDF films. The elimination reactions by DBU or KOH were considered to be accompanied by substitution reaction. The electrical conductivity of dehydrofluorinated PVDF films increased markedly by doping with iodine, and the activation energies of conduction were found to be between 0.4 and 0.5 eV. When a drawn PVDF film was dehydrofluorinated and doped with iodine, anisotropy in conductivity was observed. 相似文献
49.
Hiromi Yamashita Yo Fujii Yuichi Ichihashi Shu Gou Zhang Keita Ikeue Dal Ryung Park Keiko Koyano Takashi Tatsumi Masakazu Anpo 《Catalysis Today》1998,45(1-4):221-227
Highly dispersed titanium oxide catalysts have been prepared within zeolite cavities as well as in the zeolite framework and utilized as photocatalysts for the reduction of CO2 with H2O to produce CH4 and CH3OH at 328 K. In situ photoluminescence, ESR, diffuse reflectance absorption and XAFS investigations indicate that the titanium oxide species are highly dispersed within the zeolite cavities and framework and exist in tetrahedral coordination. The charge transfer excited state of the highly dispersed titanium oxide species play a significant role in the reduction of CO2 with H2O with a high selectivity for the formation of CH3OH, while the catalysts involving the aggregated octahedrally coordinated titanium oxide species show a high selectivity to produce CH4, being similar to reactions on the powdered TiO2 catalysts. Ti-mesoporous molecular sieves exhibit high photocatalytic reactivity for the formation of CH3OH, its reactivity being much higher than the powdered TiO2 catalysts. The addition of Pt onto the highly dispersed titanium oxide catalysts promotes the charge separation which leads to an increase in the formation of CH4 in place of CH3OH formation. 相似文献
50.
Sachiro Kakinoki Makoto Kitamura Mitsuhiro Yuge Masakazu Furuta Masahito Oka Yoshiaki Hirano Kenji Kono Isao Kaetsu 《Polymer Bulletin》2007,58(2):393-400
Summary Poly(proline) and random copolypeptide composed of Pro and Ala residues were synthesized, and their solution properties and
molecular conformation were investigated. Aqueous solutions of the polypeptide were irradiated with γ-rays above the transition
temperature. It was shown that the transition temperature of the aqueous solution of the copolypeptide is influenced by Ala-residue
content and γ-ray irradiation. 相似文献