民勤枸杞主要营养、功能成分、重金属及农药残留量分析

本文为了探讨民勤枸杞的营养、活性成分和安全性评价,通过使用高效液相、气相色谱法和其他测定方法分析民勤枸杞的基本营养和功能成分、氨基酸组成、重金属和农药残留量。民勤枸杞的基本营养成分（以每100 g干重计）蛋白质、粗脂肪和碳水化合物含量分别为13.71 g、3.09 g和60.80 g;功能成分多糖、类胡萝卜素、甜菜碱、抗坏血酸、总酚和总黄酮含量分别为2.11 g、569.81 mg、1.57 g、45.08 mg、81.95 mg和70.23 mg。民勤枸杞主要基本营养成分为碳水化合物和蛋白质,并含有丰富的功能性氨基酸天冬氨酸,脯氨酸和谷氨酸。民勤枸杞中色氨酸和芳香氨基酸等必须氨基酸含量丰富;天冬氨酸含量最为丰富;赖氨酸是第一限制必须氨基酸。民勤枸杞含有相对较高的脂肪、类胡萝卜素和抗坏血酸含量;其重金属和农药残留量没有超绿色食品枸杞标准限制。研究结果可为民勤枸杞质量定位提供理论依据。     

Faecal Composition and Nitrogen Excretion of Rats Fed on Diets Containing Sweet Lupin (Lupinus angustifoliusL) or its Fractions

Five N balance studies were conducted to determine the faecal composition and N excretion of feeding raw Lupinus angustifolius seed meal and its fractions for growing rats using a semi-synthetic lactalbumin-based diet as control. Diets were formulated to have equal amounts of energy. The protein was incorporated at the level of 10% bulk and contained unsupplemented lupin seed meal (LMU) and fully supplemented lupin seed meal (LMFS) at 360 g kg⁻¹ diet, aqueous extract non-dialysed (LPAND) at 196 g kg⁻¹ aqueous extract dialysed soluble at pH 7·0 (LPAD) at 148 g kg⁻¹ aqueous extract dialysed insoluble at pH 7·0 (LPADI) at 124 g kg⁻¹, buffer dialysed soluble at pH 7·0 (BUSOL) at 136 g kg⁻¹, buffer dialysed insoluble at pH 7·0 (BUDI) at 119 g kg⁻¹ and lupin meal residue after aqueous and buffer extraction (LMR) at 170 g kg⁻¹ diet. Rats were pair-fed for 10 days with all the above diets which had been supplemented with essential amino acids up to the target requirements for rats. Faecal wet and dry weight were increased in rats fed on LMU, LMPS and LMR diets compared to those obtained from the control diet based on lactalbumin (milk protein) LACT. The higher faecal weight was largely due to water content. The higher faecal N excretion observed in LMU, LMFS, LPAND, LPAD, BUSOL, BUDI and LMR compared to that of LACT diet was significantly lower and thus which was assumed not to be due to a decrease in the digestibility of the dietary protein, which was over 90% as compared to that in the control group. Analysis suggested that an increase in endogenous N excretion is involved in the rise of its excretion in the faeces, and indicates a long-term effect of this seed as a protein and or fibre source in monogastrics.     

Melt Production and Antimicrobial Efficiency of Low-Density Polyethylene (LDPE)-Silver Nanocomposite Film

Colloidal silver nanoparticles with a size of 5.5 ± 1.1 nm were prepared by chemical reduction using polyethylene glycol (PEG). Silver nanoparticles were incorporated into low-density polyethylene (LDPE) by melt blending and subsequent hot pressing at 140 °C to produce nanocomposite film with an average thickness of 0.7 mm. PEG was added at 5% weight of polymer as a compatibilizer agent in order to prevent agglomeration and provide uniform distribution of nanoparticles in polymer matrix. Antimicrobial activity of silver nanocomposites against Escherichia coli ATCC 13706, Staphylococcus aureus ATCC12600, and Candida albicans ATCC10231 was evaluated by semi-qualitative agar diffusion test and quantitative dynamic shake flask test. Mechanical properties of nanocomposites were not significantly different from silver-free LDPE-containing PEG films (p > 0.05), and silver nanoparticles did not form chemical bonding with the polymer. LDPE-silver nanocomposite samples by more than 6.69 ppm silver nanoparticles showed considerable antimicrobial clear zone. LDPE-silver nanocomposite affected growth kinetic parameters of the examined bacteria and is more efficient on S. aureus than E. coli. Polyethylene-silver nanocomposites containing 22.64 ppm silver nanoparticles could reduce 57.8% growth rate and 23.3% maximum bacterial concentration and increase 35.8% lag time of S. aureus. This study shows the potential use of LDPE-silver nanocomposite as antimicrobial active film. Antimicrobial efficiency of silver nanocomposite depends on silver nanoparticles concentration; however, high level of silver nanoparticles may lead to weakening of mechanical properties.     

Exchange-Coupled IrMn/CoFe Mulitlayers for RF-Integrated Inductors

The high-frequency characteristics of the RF integrated inductors with antiferromagnetic/ferromagnetic (AF/F) multilayers (MLs) are studied. Each AF layer is 8-nm IrMn and F is Co₅₀Fe₅₀ with a 200-nm splitting into N = 1 to 5 repeats of MLs. This exchange coupled {IrMn/CoFe(d nm)}_N MLs are deposited on top of the two-port inductors with five-turn square spiral coils, a dimension of 100 mum times 100 mum and line/space of 5 mum/2 mum. The inductor surface and magnetic layer is separated by 1-mum-thick SiO₂. The enhancement of inductance (DeltaL) is 20% compared to an air-core of the same coil size. The resonance peak gradually shifted to a higher frequency with increasing N, and reached at a maximum of 4.3 GHz when N = 5. This is in good agreement with our magnetic data which revealed that the anisotropy field (H_k) and ferromagnetic resonance frequency (f_FMR) of {IrMn/CoFe(d nm)}_N MLs are increased with increasing N. The quality factor, Q is improved by 6.8% at 1.5 GHz for the {IrMn/CoFe(40 nm)}_N=5 integrated inductors compared to air-core inductors.     

Chemical composition and inhibitory parameters of essential oil and extracts of Nandina domestica Thunb. to control food-borne pathogenic and spoilage bacteria

The aim of this study was to examine the chemical composition of the essential oil isolated from the floral parts of Nandina domestica Thunb. by hydrodistillation, and to test the efficacy of essential oil and various organic extracts against a panel of food-borne pathogenic and spoilage bacteria such as Bacillus subtilis ATCC6633, Listeria monocytogenes ATCC19166, Staphylococcus aureus KCTC1916, S. aureus ATCC6538, Pseudomonas aeruginosa KCTC2004, Salmonella typhimurium KCTC2515, Salmonella enteridis KCCM12021, Escherichia coli 0157-Human, E. coli ATCC8739, E. coli 057:H7 ATCC43888 and Enterobacter aerognes KCTC2190. The chemical composition of essential oil was analysed by GC-MS. It was determined that 79 compounds, which represented 87.06% of total oil, were present in the oil. The oil contained mainly 1-indolizino carbazole (19.65%), 2-pentanone (16.4%), mono phenol (12.1%), aziridine (9.01%), methylcarbinol (4.6%), ethanone (3.3%), furfural (2.96%), 3,5-dimethylpyrazole (1.29%) and 2(5H)-furanone (1.32%). The oil (1000 ppm/disc), and various organic extracts of hexane, chloroform, ethyl acetate and methanol (1500 ppm/disc) exhibited promising antibacterial effect as a diameter of zones of inhibition (9-18 and 7-13 mm) and MIC values (62.5 to 1000 and 250 to 2000 microg/ml), respectively against the tested bacteria. Also the oil had strong detrimental effect on the viable count of the tested bacteria. These results indicate the potential efficacy of plant-based natural products such as essential oil and organic extracts of N. domestica to control food-borne pathogenic and spoilage bacteria.     

Pressure measurements in laboratory-scale blast wave flow fields

The present study examines the effects that temporal and spatial averagings due to finite size and finite response time of pressure transducers have on the pressure measurements in blast wave flow fields generated by milligram charges of silver azide. In such applications, the characteristic time and length scales of the physical process are of the same order of magnitude as the temporal and spatial characteristics of the transducer. The measured pressure values will then be spatially and temporally averaged, and important parameters for the assessment of blast effects may not be properly represented in the measured trace. In this study, face-on and side-on pressure transducer setups are considered. In the experiments, face-on and side-on readings at the same distance from the charge as well as time-resolved optical visualization of the whole flow field are obtained simultaneously for the same explosive event. The procedure of data extraction from the experimental pressure traces is revisited and discussed in detail. In the numerical modeling part of the study, numerical blast flow fields are generated using an Euler flow solver. A numerical pressure transducer model is developed to qualitatively simulate the averaging effects. The experimental and numerical data show that the results of pressure measurements in experiments with small charges must be used with great caution. The effective averaging of the pressure signal may lead to a significant underestimation of blast wave intensities. The side-on setup is especially prone to this effect. The face-on setup provides results close to those obtained from optical records only if the pressure transducer is sufficiently remote from the charge.     

An experimental study on micro-EDM in low-resistivity deionized water using short voltage pulses

Deionized water has been used as dielectric fluid for micro-electrical discharge machining (micro-EDM) because it gives higher material removal rate and lower tool wear than hydrocarbon oil. Moreover, it is a relatively low-cost and eco-friendly substance. Therefore, deionized water tends to be more favorable for micro-EDM. However, it causes weak electrochemical reaction during micro-EDM due to its slight conductivity. This leads to the unanticipated additional material removal from the workpiece which affects the machining shape and quality. The study in this paper aims to suppress the electrochemical reaction in die-sinking micro-EDM using deionized water by employing short voltage pulse. Experiments were carried out to fabricate micro-holes using the developed nanosecond pulse circuit. Different pulse parameters were applied to identify the main factor affecting the electrochemical reaction rate. Machining gap was found to be thinner and workpiece surface adjacent to the rim of micro-holes were found to be free of defects caused by material dissolution when pulse duration reached a critical value. Moreover, the influence of pulse parameters on material removal rate and machined shape was also investigated. Besides, energy-dispersive X-ray spectroscopy analysis showed that the machined surface using deionized water was less affected from material migration during micro-EDM process in comparison to hydrocarbon oil.     

Enhancement of mechanical and thermal properties of polycaprolactone/chitosan blend by calcium carbonate nanoparticles

This study investigates the effects of calcium carbonate (CaCO(3)) nanoparticles on the mechanical and thermal properties and surface morphology of polycaprolactone (PCL)/chitosan nanocomposites. The nanocomposites of PCL/chitosan/CaCO(3) were prepared using a melt blending technique. Transmission electron microscopy (TEM) results indicate the average size of nanoparticles to be approximately 62 nm. Tensile measurement results show an increase in the tensile modulus with CaCO(3) nanoparticle loading. Tensile strength and elongation at break show gradual improvement with the addition of up to 1 wt% of nano-sized CaCO(3). Decreasing performance of these properties is observed for loading of more than 1 wt% of nano-sized CaCO(3). The thermal stability was best enhanced at 1 wt% of CaCO(3) nanoparticle loading. The fractured surface morphology of the PCL/chitosan blend becomes more stretched and homogeneous in PCL/chitosan/CaCO(3) nanocomposite. TEM micrograph displays good dispersion of CaCO(3) at lower nanoparticle loading within the matrix.