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991.
The volatile components of roasted coffee, isolated by normal-pressure steam distillation, were separated into basic and neutral fractions. The neutral fraction was analysed on a UCON HB 5100 glass capillary column (200 m x 0.31 mm W.) coupled to a low-resolution mass spectrometer. One hundred and twenty compounds were identified, of which twenty-six had not been previously reported in coffee aroma. Identification of the structures of the newly identified compounds was accomplished by comparison of their mass spectra with reference spectra. GLC retention times were used to confirm identifications. The new compounds identified for the first time in roasted coffee include 15 furans, 6 pyrroles, 3 thiophenes, and 2 ketones. Of the 15 furans eight methylvinylfurans, dimethyl-vinylfurans and alkenylfurans, which had not been previously found in roasted foodstuffs, should be specially mentioned.Mass-spectral data of the newly identified substances are tabulated. Fragmentation patterns of N-acetyl-2-methylpyrrole, N-furfuryl-2-methylpyrrole, 2-vinyl-3-methylfuran and 2-vinyl-3,5-dimethylfuran are discussed. Comments are made with respect to possible formation patterns and precursors in green coffee beans.  相似文献   
992.
Non-invasive blood perfusion measurement systems have been developed and tested in a phantom tissue and an animal model. The probes use a small sensor with a laminated flat thermocouple to measure the heat transfer and temperature response to an arbitrary thermal event (convective or conductive) imposed on the tissue surface. Blood perfusion and thermal contact resistance are estimated by comparing heat flux data with a mathematical model of the tissue. The perfusion probes were evaluated for repeatability and sensitivity using both a phantom tissue test stand and exposed rat liver tests. Perfusion in the phantom tissue tests was varied by controlling the flow of water into the phantom tissue test section, and the perfusion in the exposed liver tests was varied by temporarily occluding blood flow through the portal vein. The phantom tissue tests indicated that the probes can be used to detect small changes in perfusion (0.005 ml/ml/s). The probes qualitatively tracked the changes in the perfusion of the liver model due to occlusion of the portal vein.  相似文献   
993.
This paper discusses the development and implementation of three novel implantable technologies that have advanced the communication abilities of hearing-impaired individuals who cannot benefit from conventional hearing aids. This paper will discuss clinical indications and outcomes and include current technological limitations and future research efforts.  相似文献   
994.
The solubility of mixtures of carbon dioxide and hydrogen sulphide in a 2.5 N monoethanolamine solution has been determined at temperatures of 40°C and 100°C. Partial pressures of CO2 ranged from 0.7 to 5630 kPa, while partial pressures of H2S ranged from 0.7 to 3780 kPa. The present results extend the published data on this system which were limited to partial pressures below 200 kPa. The results have been compared with two methods of prediction based upon a thermodynamic model.  相似文献   
995.
    
Isoelectric solubilization and precipitation (ISP) is a protein recovery process effective at reducing Listeria innocua, a nonpathogenic bacterium typically used as a surrogate for L. monocytogenes in recovered trout protein. The response of L. monocytogenes to ISP processing was determined and compared to the response of L. innocua. Headed and gutted rainbow trout were inoculated with L. monocytogenes (10.16 log CFU/g), homogenized, and pH-adjusted with granular citric acid (pH 2.0 and 2.5) or glacial acetic acid (pH 3.0 and 3.5). Proteins were solubilized and centrifugation was used to remove insoluble components (skin, insoluble protein, so on). The supernatant was returned to the protein isoelectric point (pH 5.5) with NaOH and centrifuged to remove precipitated protein. Microbial load was enumerated on both growth and selective media; recovery was not significantly different (P > 0.05). Surviving cells from each component (protein, insoluble, and water) were compared to initial inoculum numbers. Significant reductions were detected at all pH (P < 0.05). The greatest reductions were at pH 3.0 with acetic acid, with a mean log reduction of 3.03 in the combined components, and a 3.53 log reduction in the protein portion. Data were compared to results from a previous study using L. innocua. Significant differences (P < 0.05) in recovery were found between the 2 species at pH 2.0 and 3.0 with greater recovery of L. monocytogenes, regardless of processing pH or acid type. These results demonstrate the variability in resistance between species and indicate that L. innocua is not an appropriate surrogate for L. monocytogenes for ISP processing with organic acids.  相似文献   
996.
997.
Resistance to driving rain of pitched roof structures ‐ German and European assessment methods for rain penetration into tiled roofs and the resistance to driving rain of covering underlays and self supporting underlays. Resistance to driving rain describes the ability of an external component to offer protection against ingress of water into the component or the building under specified wind force, rainfall and rain duration. Standardised tests already exist for assessing and classifying the resistance to driving rain of components such as windows, external doors and gates, while for covered pitched roof structures no such tests have been established as yet. This applies to the actual roof covering consisting of small‐sized roofing elements such as tiles as well as covering underlays and self supporting underlays, which are exposed to the weather during the construction phase and during alterations or refurbishment. Over recent years great efforts have been made to try and compare the resistance to driving rain of covered pitched roof structures and exposed covering underlays and self supporting underlays used as temporary roof covering.  相似文献   
998.
A simulation model of the microstructure developed during the reaction sintering of ultrafine silicon powders is presented. The model employs interactive subroutines that describe particle compaction, sintering, and nitridation. The particle compaction model is based on a random particle packing model, whereas the sintering and reaction sintering models are based on the modified grain model and the sharp interface model (SIM). Microstructural changes due to the competition between chemical reaction and sintering are taken into account in the model. The results predicated by this model show good agreement with experimental data from previous studies.  相似文献   
999.
Negro-white differences on mental tests are evaluated in this paper, which was prepared at the suggestion of the Society for the Psychological Study of Social Issues (Division 9 of the American Psychological Association). "The evidence against the assumption of native differences in intelligence test performance between Negroes and whites still seems to me to be very convincing." There is "no scientifically acceptable evidence for the view that ethnic groups differ in innate abilities. This is not the same as saying that there are no ethnic differences in such abilities… . The science of psychology can offer no support to those who see in the accident of inherited skin color or other physical characteristics any excuse for denying to individuals the right to full participation in American democracy." (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
1000.
Meanwhile, the long-term practical experience and the scientific research results about the utilisation of organic residues in heated sludge digesters of municipal wastewater treatment plants are sufficient for an interim résumé about co-digestion and for recommendations for the practical approach. In this paper, effects, backlashes and consequences of the co-digestion of organic substrates are described in detail. Concerning the stability of the digestion process and the expected production of digestion residues, co-digestion has proved to exhibit positive effects. Problems might occur regarding the additional nitrogen loads in the reject water from sludge treatment as well as with regard to the enrichment of impurities in the sludge digesters—in particular in the case of the use of food leftovers from restaurants and so-called bio-waste from households. Additional attention has to be paid to the storage of the co-substrates as well as to the optimal utilisation of the energy produced in excess.  相似文献   
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