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211.
We consider the dynamics of a dark soliton in an elongated harmonically trapped Bose-Einstein condensate. A central question
concerns the behavior at finite temperatures, where dissipation arises due to the presence of a thermal cloud. We study this
problem using coupled Gross-Pitaevskii and N-body simulations, which include the mean field coupling between the condensate and thermal cloud. We find that the soliton
decays relatively quickly even at very low temperatures, with the decay rate increasing with rising temperature. 相似文献
212.
V. Thomas Paul S. Saroja P. Hariharan A. Rajadurai M. Vijayalakshmi 《Journal of Materials Science》2007,42(14):5700-5713
This paper presents the results of a study on the microstructural and microchemical variations in a multipass Gas Tungsten
Arc weld (GTAW) of modified 9Cr-1Mo steel. The changes brought about in the steel due to the heating and cooling cycles during
welding and the subsequent effects due to reheating effects during multipass welding are described. Detailed analytical transmission
electron microscopy has been carried to study the type and composition of the primary and secondary phases in this steel.
The systematic changes in microstructural parameters such as Prior Austenite Grain Size, martensite lath size, number density,
size and microchemistry of carbides, have been understood based on the different transformations that the steel undergoes
during the heating and cooling process. Based on the observed microstructure, an attempt has been made to identify distinct
microstructural zones and possible thermal cycles experienced by different regions of the weldment. 相似文献
213.
Z. Ferhat-Hamida H. Phuong-Nguyen P. Bernazzani A. Haine G. Delmas 《Journal of Materials Science》2007,42(9):3138-3154
LLDPE samples synthesized with Ziegler–Natta (ZN) and Metallocene (MT) catalysts have been analyzed to investigate a potential
catalyst-dependent morphology and to find an explanation for the difficult processing of MT. Slow calorimetry at v = 0.02 K/min and IR at RT and in the melt are used. The differences between MT and ZN are assigned to their different composition,
MT not having the linear segments, which are present in ZN. Slow calorimetry is effectively a drawing process of the melt
with chain orientation followed by decay. The later event, characterized by an endotherm, ΔH
network, occurs at higher temperatures for MT, the presence of a regular distribution of methyl groups slowing down the process.
The rocking, gauche, bending and stretching regions of the IR spectra are analyzed. The nascent MT has more strained bands
in the rocking region. The wagging region reveals the more homogeneous environment of MT through the maximum absorbance at
1,368 cm−1. Decomposition of bands is made for the rocking and wagging regions. The orthorhombic crystallinity, αc (FTIR), measures the sum of long- and short-range orthorhombic order, the latter being obtained by αc (FTIR)-αc (X-rays). The values of αc (FTIR) for MT and ZN are very similar in conditions of equilibrium. The justifications for the molecular origin of ΔH
network are presented: (i) the slow relaxation of long chains strained and oriented in the melt measured by other techniques, (ii)
The correlation, for gels of a linear sample, made in different solvents, between the maximum drawability, λmax, and ΔH
network in a slow T-ramp. The range is 80–270 for λmax and 40–120 J/g for ΔH
network. (iii) The comparison of two traces of the same sample, between 140 °C and 270 °C, show that comparable events in the melt
appear in the integrated absorbance and in the slow calorimetry signal. Analysis on thin films of the little-studied CH2 stretching region reveals that their extinction coefficient, ε, and the shape of the bands are highly sensitive to the sample
history, ε diminishing by a large factor in slowly crystallized samples. Events in the slow T-ramp, followed by a fast crystallization, on the other hand, leads to materials with standard characteristics. Slow calorimetry
traces display more events (endothermic and exothermic) for MT than for ZN, a finding consistent with more flow irregularities
during processing. Equilibrium conditions and better processing could be reached for MT by extending time in the melt or using
higher temperatures. 相似文献
214.
Daniel X. Gouveia Odair P. Ferreira Antonio G. Souza Filho M. G. da Silva J. A. C. de Paiva Oswaldo L. Alves Josué Mendes Filho 《Journal of Materials Science》2007,42(2):534-538
The thermal decomposition properties of Mg–Fe hydrotalcites were studied through in situ 57Fe Mössbauer spectroscopy and in situ X-ray diffraction. Abrupt changes in the quadrupolar splitting measured in the Mössbauer spectra revealed a phase transition from the starting lamellar structure to a new crystalline arrangement. By analyzing the Mössbauer parameters we show that the material is highly disordered in the 300–400 °C temperature range. This hypothesis is confirmed by the X-ray results whose diffractograms indicated the collapse of the lamellar structure and the formation of a solid solution. 相似文献
215.
Dielectric and thermal characteristics of gel grown single crystals of ytterbium tartrate trihydrate
Dielectric and thermal characteristics of gel grown single crystals of ytterbium tartrate trihydrate have been carried out.
The dielectric constant has been measured as a function of frequency in the range 2 kHz–1 MHz and temperature range 30–300 °C.
The dielectric constant increases with temperature, attains a peak near 215 °C, and then decreases as the temperature exceeds
215 °C. The dielectric anomaly at 215 °C is suggested to be due to phase transition brought about in the material. The dielectric
behaviour of the material is correlated with the results on thermal analysis. Thermogravimetric and differential thermal analysis
have been used to study the thermal characteristics of the material. The experimental results show that the material is thermally
stable up to 200 °C. The decomposition process occurs in two stages until ytterbium oxide is formed at 700 °C. The non-isothermal
kinetic parameters e.g., activation energy and the frequency factor have been evaluated for each stage of thermal decomposition
by using the integral method, applying the Coats–Redfern approximation. 相似文献
216.
Christian P. Romero Jonathan I. Avila Edgardo Cisternas Guerau B. Cabrera Alejandro L. Cabrera Kristiaan Temst Margriet J. Van Bael 《Journal of Materials Science》2007,42(18):7667-7672
Hydrogen desorption curves were obtained from a sample composed of a square arrangement of Co dots with average diameter of
4.4 μm, separated by a distance of 11.6 μm. A macroscopic sample of Co dots grown on a 2.5 × 2.5 cm Si substrate was made
by standard lithographic techniques and used in these experiments. Thermal programmed desorption (TPD) was performed under
ultra-high vacuum conditions. Hydrogen TPD curves were obtained from a 1 × 1 cm Co dots samples displaying a maximum of intensity
at 425 K. Hydrogen TPD curve was also obtained from 1 cm× 1 cm samples of Co films and Co foils for comparison. The hydrogen
TPD curves have decreasing intensity from the Co foils to the Co dots and finally to the Co films. This indicates that there
are more sites for hydrogen adsorption on the Co dots than in the Co films. This is a surprising result because there is approximately
8.7 times less Co atoms exposed in the Co dots that in the Co film sample. A desorption energy of 27 kcal/mol was obtained
for the Co dots suggesting that hydrogen is adsorbed on an hcp hollow site of the Co dot crystalline structure. 相似文献
217.
We propose a method of fabricating surface barrier diodes with overlapped metal junction, which provides for a significant decrease in the reverse currents and an increase in the breakdown voltage. 相似文献
218.
Fiber cross sections for use in textiles and composites are becoming more and more complex. Shape impacts fiber or filaments properties and therefore the yarn and fabric characteristics. This paper presents the influence of the fiber cross section on the fabric surface characteristics. The material used was polyester staple fibers, of four different shapes: round, scalloped oval, cruciform and hexachannel. All fibers had the same cut length with different fineness. Yarns obtained from these fibers had nominally the same yarn count, torsion value and structure. Plain jersey fabrics were knitted from each of the yarns under identical conditions and then relaxed prior to testing. Friction behavior was evaluated and a roughness-friction criterion developed. An indirect measurement of the real area of contact was obtained in order to provide roughness and friction properties. The influence of fiber cross section on yarn bending rigidity and on the state of the knitted fabric surface was characterized. 相似文献
219.
220.
Aerosol-gel process is a deposition method based on the sol-gel polymerization of a liquid film produced from an ultrasonically sprayed aerosol. This process offers an attractive alternative for the deposition of photocurable SiO2—TiO2 ORMOSIL films. 3-(trimethoxysilyl) propylmethacrylate and tetraisopropyl-orthotitanate complexed with methacrylic acid were used as sol-gel precursors. Doping with a terbium:sulphosalicylic acid complex was also studied to test the deposition of spectroscopically active photocurable films. FTIR spectroscopy has been used to study the precursor solutions and ORMOSIL films. It is shown that titanium precursor incorporation enhances the solution reactivity, which yields optical quality thin films. Photopolymerization and photoluminescence properties of the films are reported and discussed with respect to the experimental parameters. The results allow envisaging the UV-imprinting fabrication of Aerosol-gel-derived active waveguides. 相似文献