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71.
V.K. Pandey M. Parmeswaran S.D. Soman H.J. Dacosta 《The Science of the total environment》1982,25(3):277-285
In a grave illness the homeostasis of some elements may be upset either by the disease process per se, or by the therapy adopted. Patients with pyogenic, viral and tubercular meningo-encephalitis were targets of interest. 108 subjects' serum and cerebrospinal fluid (CSF) compartments were assayed for magnesium, calcium, zinc and copper, by atomic absorption spectrometry. Results showed that the serum pool was more intensely altered than the CSF pool in the case of magnesium and calcium but the reverse occurred for zinc and copper. No organism-dependent change was noted, but comatosed patients were the worst effected. These findings are discussed with respect to the relative brain and CSF content of each element and the patho-physiology which could alter the compartments studied. 相似文献
72.
Detection of tyrosine phosphorylated peptides by precursor ion scanning quadrupole TOF mass spectrometry in positive ion mode 总被引:9,自引:0,他引:9
Phosphorylation is a common form of protein modification. To understand its biological role, the site of phosphorylation has to be determined. Generally, only limited amounts of phosphorylated proteins are present in a cell, thus demanding highly sensitive procedures for phosphorylation site determination. Here, a novel method is introduced which enables the localization of tyrosine phosphorylation in gel-separated proteins in the femtomol range. The method utilizes the immonium ion of phosphotyrosine at m/z 216.043 for positive ion mode precursor ion scanning combined with the recently introduced Q2-pulsing function on quadrupole TOF mass spectrometers. The high resolving power of the quadrupole TOF instrument enables the selective detection of phosphotyrosine immonium ions without interference from other peptide fragments of the same nominal mass. Performing precursor ion scans in the positive ion mode facilitates sequencing, because there is a no need for polarity switching or changing pH of the spraying solvent. Similar limits of detection were obtained in this approach when compared to triple-quadrupole mass spectrometers but with significantly better selectivity, owing to the high accuracy of the fragment ion selection. Synthetic phosphopeptides could be detected at 1 fmol/microL, and 100 fmol of a tyrosine phosphorylated protein in gel was sufficient for the detection of the phosphorylated peptide in the unseparated digestion mixture and for unambiguous phosphorylation site determination. The new method can be applied to unknown protein samples, because the identification and localization of the modification is performed on the same sample. 相似文献
73.
Micromechanical structures that have squeeze-film damping as the dominant energy dissipation mechanism are of interest in this paper. For such structures with narrow air gap, the Reynolds equation is used for calculating squeeze-film damping, which is generally solved with trivial pressure boundary conditions on the side walls. This procedure, however, fails to give satisfactory results for structures under two important conditions: 1) for an air gap thickness comparable to the lateral dimensions of the microstructure and 2) for nontrivial pressure boundary conditions such as fully open boundaries on an extended substrate or partially blocked boundaries that provide side clearance to the fluid flow. Several formulas exist to account for simple boundary conditions. In practice, however, there are many micromechanical structures such as torsional microelectromechanical system (MEMS) structures that have nontrivial boundary conditions arising from partially blocked boundaries. Such boundaries usually have clearance parameters that can vary due to fabrication. These parameters, however, can also be used as design parameters if we understand their role on the dynamics of the structure. We take a MEMS torsion mirror as an example device that has large air gap and partially blocked boundaries due to static frames. We actuate the device and experimentally determine the quality factor Q from the response measurements. Next, we model the same structure in ANSYS and carry out computational fluid dynamics analysis to evaluate the stiffness constant K, the damping constant D, and the quality factor Q due to the squeeze film. We compare the computational results with experimental results and show that without taking care of the partially blocked boundaries properly in the computational model, we get unacceptably large errors. 相似文献
74.
This study reports the glacier changes of Chandra–Bhaga basin, northwest Himalaya, India, from 1980 to 2010. Satellite remote-sensing data from the Landsat Multispectral Scanner (MSS) and Thematic Mapper (TM), the Linear Imaging Self Scanning Sensor (LISS) and Advanced Wide Field Sensor (AWiFS) of the Indian Remote Sensing (IRS) series, and the Shuttle Radar Topography Mission (SRTM) digital elevation model (DEM) were used to study the changes in glacier parameters such as glacier area, length, snout elevation, and the impact of glacier topographical parameters (glacier slope, aspect, and altitude range) on the glacier changes. It was found that the total glaciated area had shrunk to 368.2 km2 in 2010 from 377.6 km2 in 1980, a loss of 2.5%. The average position of glacier terminuses retreated by 465.5 ± 169.1 m from 1980 to 2010 with an average rate of 15.5 ± 5.6 m year?1. The decadal scale analysis showed that the average rate of retreat had increased the most in the recent decade. A moraine-dammed lake located in the study region was found to have expanded in area from (0.65 ± 0.01) km2 in 1980 to (1.26 ± 0.03) km2 in 2010. Glaciers with steep slope and less altitude range have lost more area than the glaciers having gentle slope and greater altitude range. 相似文献
75.
In 2012, the government of Bihar revived 34 non-functioning public tubewells using solar panels. The performance of 16 of these wells over 12 months was tracked and analyzed using data from tubewell operators and 240 farmers. Access to affordable irrigation from solar pumps led to a 9–10% increase in productivity of rice and wheat. Furthermore, in a severe drought, farmers could grow paddy in the entire area irrigated by solar pumps, when nearly 40% of other land was left fallow. Solar pumps can help increase crop productivity, reduce the cost of irrigation, and make agriculture more resilient to climate change. 相似文献
76.
Hevea brasiliensis ) esterified with acetic anhydride, maleic anhydride and phthalic anhydride was studied for moisture adsorption behaviour.
FTIR spectroscopic technique was used to analyse the chemical changes in the wood through the correspondent reactions. Spectra
indicated increasing intensity of the C=O and C-O stretching bands, and reduction in O-H stretching vibrations that reflects
formation of less hygroscopic ester bonds with hydroxyl groups of cell wall polymers. Moisture adsorption isotherms show low
equilibrium moisture content in esterified wood at all relative humidity values as compared to a control. The adsorption data
was analysed by applying Hailwood-Horrobin theory which separated the adsorbed water into hydrated water and dissolved water
corresponding to mono-layer and multi-layer adsorption. Curve for Mh and Ms were similar in pattern for esterified wood and control with different magnitude. Low Mh and Ms in esterified wood indicate reduction in moisture adsorption sites. Inaccessible fraction of wood for water vapour was increased
by 43%, 32% and 26% in acetic, maleic and phthalic anhydride treated wood, respectively, compared to the control. Acetic anhydride
treatment was found most effective in reducing hygroscopicity of wood.
Hevea brasiliensis ) wurde verestert mit Anhydriden der Maleins?ure, Essigs?ure und Phtals?ure. Das Adsorptionsverhalten bei verschiedenen Feuchten wurde mit FTIR-Methoden untersucht, um die entsprechenden chemischen Abl?ufe zu erfassen. Intensivere C=O, und -C-O- Streckschwingungen sowie reduzierte OH-Schwingungen reflektieren die neu gebildeten, weniger hygroskopischen Esterbindungen. Bei allen modifizierten Proben ergaben sich niedrigere Gleichgewichtsfeuchten. Die Adsorptions-Isothermen wurden mit Hilfe der Hailwood-Horrobin Theorie analysiert, um adsorbiertes (Mh) und gel?stes (Ms) Wasser zu unterscheiden. Der Kurvenverlauf für Mh und Ms für modifiziertes und unbehandeltes Holz war qualitativ ?hnlich, und unterschied sich nur quantitativ. Geringe Werte für Mh und Ms zeigen eine Verringerung der m?glichen Adsorptionsstellen an. Der nicht zug?ngliche Anteil des Holzes, bezogen auf Kontrollproben, verringerte sich auf 43% (Acetanhydrid), 32% (Maleins?ureanhydrid) und 26% (Phthals?ureanhydrid). Acetanhydrid erwies sich als das effektivste Mittel, um die Hygroskopizit?t zu erniedrigen.相似文献
77.
78.
79.
Various glasses in the system (65 – x)[SrO · TiO2]-(35)[2SiO2 · B22O3]-(x)La2O3, where x = 1,5,10 (wt%) were prepared by melting in alumina crucible (1375–1575 K). Heat treatment schedules were selected from DTA plots of respective glasses. X-ray diffraction studies of glass ceramic samples containing different concentrations of La2O3 revealed the formation of Sr2B2O5, Sr3Ti2O7 and TiO2 (rutile) phases. The addition of La2O3 results in the development of well formed, elongated crystallites of different phases. Results of the dielectric behaviour demonstrate higher values of dielectric constant for some of the glass ceramic samples. This can be ascribed to the relaxation polarization at the crystal-glass interface due to conductivity differences between crystalline and glassy phases. 相似文献
80.
Hanne Hjorth Tønnesen Jan Karlsen Sitaram R. Adhikary Rita Pandey 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1989,189(2):116-118
Summary The content of curcuminoids inCurcuma longa L. before, during and after a normal harvesting period was investigated. The plant material was grown in the Kathmandu area. Bis-demethoxycurcumin was found to be the main constituent. No significant change in the curcuminoid content was observed during a 17-week sampling period.
Studien über Curcumin und Curcuminoide. XVII. Veränderung des Gehaltes an Curcuminoiden inCurcuma longa L. (Zingiberaceae) aus Nepal warend der Ernte
Zusammenfassung Der Gehalt an Curcuminoiden inCurcuma longa L. (Zingiberaceae) wurde vor, während und nach der normalen Erntezeit untersucht. Das Pflanzenmaterial stammt aus dim Kathmandu-Tal in Nepal. Der Hauptinhaltsstoff ist Bisdemethoxycurcumin. Im Laufe von 17 Wochen konnten keine signifikante Schwankungen observiert werden.相似文献