合成吡啶类化合物用催化剂的再生行为研究

对合成吡啶类化合物用的失活催化剂上的结焦物进行了元素分析 ,并着重对失活催化剂的再生行为进行了研究。得到了不同失活程度催化剂的再生曲线及相同失活程度、不同再生条件下的再生曲线。经回归求得了一简单的再生反应动力学经验方程式 ,其中反应级数为碳含量的 1.16 5级 ,活化能为 4 2 .5 72kJ/mol,计算值与实验值的平均相对误差为 6 .5 %。     

论西北地区地下水的开发利用与保护

本文通过分析西北地区的水资源时空分布特点和水循环特点、地下水开发利用现状以及开发利用中出现的生态环境问题，总结了西北地区多年来水资源开发利用的成功经验和失败教训，提出今后地下水资源合理开发利用的几点建议：即提高社会对西北地区地下水的认识，适度增大地下水开采；充分发挥地下水的一态环境调节作用，水资源开发与生态环境保护并举；遵循地表水与地下水的多次相互转化规律，提高水资源总体利用率；水资源开发利用与水资源涵养相结合；加强西北地区地下水的调查与研究。     

A new efficient method for one‐pot conversions of aryl carboxylic acids into nitriles without solvent

A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry     

食物营养规划培训效果追踪和影响因素分析

本文采用调查问卷,追踪访问了参加食物营养规划培训班的人员一年后的工作开展、培训知识掌握和应用情况.结果表明,这些人员较好地掌握了培训知识,平均掌握率为70%,培训知识和技能应用率平均为46%;性别、年龄、技术职称和部门来源等对培训知识掌握和应用有一定的影响.     

Modeling wireless fading channels via stochastic differential equations: identification and estimation based on noisy measurements

This paper is concerned with modeling and identification of wireless channels using noisy measurements. The models employed are governed by stochastic differential equations (SDEs) in state space form, while the identification method is based on the expectation-maximization (EM) algorithm and Kalman filtering. The algorithm is tested against real channel measurements. The results presented include state space models for the channels, estimates of inphase and quadrature components, and estimates of the corresponding Doppler power spectral densities (DPSDs), from sample noisy measurements. Based on the available measurements, it is concluded that state space models of order two are sufficient for wireless flat fading channel characterization.     

注射成形粘结NdFeB磁体:工艺·性能·应用

综合介绍了几种适于注射成形粘结NdFeB磁体的磁粉制备方法及特点；讨论了粘结剂、改性剂及磁场取向对注射成形NdFeB磁体最终磁性能的影响及其应用市场。在此基础上，指出了今后开展研究工作的方向。     

镍氢电池负极用低成本储氢合金的研究

研究了ABS型储氢合金在低Co含量条件下，随B组元替代元素Co，Al，Si等含量的变化对合金电化学性能的影响规律，同时研究了A组元中不同La／Ce比对合金电化学性能的影响情况。结果表明，随合金中Co含量的降低，合金的活化性能和放电容量得以改善，但合金的循环寿命下降也比较明显；在试验范围内，随Al元素的加入，合金的循环寿命得以改善，但材料的放电容量和活化性能均有所下降；随合金La／Ce比的降低，合金的放电容量略有下降，但其循环寿命和放电电压平台有较大提高。