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排序方式: 共有635条查询结果,搜索用时 15 毫秒
81.
L. Vimala Devi S. Sellaiyan T. Selvalakshmi H.J. Zhang A. Uedono K. Sivaji S. Sankar 《Advanced Powder Technology》2017,28(11):3026-3038
Monoclinic undoped and Tb doped CuO are prepared by solution combustion method and annealed at different temperatures. The effect of annealing and doping on their structural and optical properties of CuO are examined using XRD, FTIR and DRS. The surface and lattice defects in CuO and Tb doped CuO is analyzed qualitatively and quantitatively using positron lifetime and Doppler broadening spectroscopy. The average positron lifetime and electron momentum (energy) S parameter increases owing to the number of vacancies in the CuO lattice upon doping and decreases with increasing temperature. The migration of vacancies from grain to grain boundary region is observed at 600 °C annealed samples. At 800 °C, the overall behavior of lifetime value denotes that the vacancy type defect is recovered, cluster vacancy and microvoids exists with reducing size. The photocatalytic performance of undoped and Tb doped CuO on degradation of methylene blue (MB) and methyl orange (MO) is investigated under visible light for two different lamp power and dye concentration. The influence of annealing temperature and dopant ion on the efficiency is also elaborated. Enhanced photocatalytic efficiency in Tb doped CuO is observed upon annealing. X-ray photoelectron spectroscopy (XPS) result indicates that the valence states of Cu, O and Tb ions exist at the surface of the particles. Brunauer–Emmett–Teller N2 adsorption–desorption analyses were employed to characterize specific surface area and porosity of Tb doped CuO. The doped CuO with pore size of about ~34 nm have a surface area of 16–28 m2/g. The surface area effect plays an important role in the enhanced catalytic performance on Tb doped catalysts. 相似文献
82.
Recommender system is a tool to suggest items to the users from the extensive history of the user's feedback. Though, it is an emerging research area concerning academics and industries, where it suffers from sparsity, scalability, and cold start problems. This paper addresses sparsity, and scalability problems of model-based collaborative recommender system based on ensemble learning approach and enhanced clustering algorithm for movie recommendations. In this paper, an effective movie recommendation system is proposed by Classification and Regression Tree (CART) algorithm, enhanced Balanced Iterative Reducing and Clustering using Hierarchies (BIRCH) algorithm and truncation method. In this research paper, a new hyper parameters tuning is added in BIRCH algorithm to enhance the cluster formation process, where the proposed algorithm is named as enhanced BIRCH. The proposed model yields quality movie recommendation to the new user using Gradient boost classification with broad coverage. In this paper, the proposed model is tested on Movielens dataset, and the performance is evaluated by means of Mean Absolute Error (MAE), precision, recall and f-measure. The experimental results showed the superiority of proposed model in movie recommendation compared to the existing models. The proposed model obtained 0.52 and 0.57 MAE value on Movielens 100k and 1M datasets. Further, the proposed model obtained 0.83 of precision, 0.86 of recall and 0.86 of f-measure on Movielens 100k dataset, which are effective compared to the existing models in movie recommendation. 相似文献
83.
Aruna Devi Balasubramanian Pallikonda Rajasekaran Murugan Arun Prasath Thiyagarajan 《International journal of imaging systems and technology》2019,29(4):399-418
Computer-aided diagnosis (CAD) is a computerized way of detecting tumors in MR images. Magnetic resonance imaging (MRI) has been generally used in the diagnosis and detection of pancreatic tumors. In a medical imaging system, soft tissue contrast and noninvasiveness are clear preferences of MRI. Inaccurate detection of tumor and long time consumption are the disadvantages of MRI. Computerized classifiers can greatly renew the diagnosis activity, in terms of both accuracy and time necessity by normal and abnormal images, automatically. This article presents an intelligent, automatic, accurate, and robust method to classify human pancreas MRI images as normal or abnormal in terms of pancreatic tumor. It represents the response of artificial neural network (ANN) and support vector machine (SVM) techniques for pancreatic tumor classification. For this, we extract features from MR images of pancreas using the GLCM method and select the best features using JAFER algorithm. These features are analyzed by five classification techniques: ANN BP, ANN RBF, SVM Linear, SVM Poly, and SVM RBF. We compare the results with benchmark data set of MR brain images. The analytical outcome presents that the two best features used to classify the MR images using ANN BP technique have 98% classification accuracy. 相似文献
84.
Devi Salam Shuleenda Roy Amarjit Singha Joyeeta Sheikh Shah Alam Laskar Rabul Hussain 《Multimedia Tools and Applications》2018,77(1):661-662
Multimedia Tools and Applications - 相似文献
85.
Oligomeric Composition of Polyols From Fatty Acid Methyl Ester: The Effect of Ring‐Opening Reactants of Epoxide Groups 下载免费PDF全文
Tuan Noor Maznee Tuan Ismail Nor Azowa Ibrahim Mohd Azmil Mohd Noor Seng Soi Hoong Kosheela Devi Poo Palam Shoot Kian Yeong Zainab Idris Christi M. Schiffman Ibrahim Sendijarevic Emilia Abd Malek Norhazlin Zainuddin Vahid Sendijarevic 《Journal of the American Oil Chemists' Society》2018,95(4):509-523
Commercial availability of fatty acid methyl ester (FAME) from palm oil targeted for biodiesel offers a good feedstock for the production of structurally well‐defined polyols for polyurethane applications. The effect of molecular weight (MW), odd and even carbon numbers, and the linear and branched structure reactants used in the ring‐opening reaction of epoxidized fatty acid methyl ester (E‐FAME) on the properties of polyols was investigated. Conversions of E‐FAME to PolyFAME polyols were confirmed by Fourier transform infrared analysis, oxirane oxygen content, and hydroxyl number. Gel permeation chromatography (GPC) calibrated against polyether polyols as a standard and vapor pressure osmometry were used for MW determination. GPC chromatograms of PolyFAME polyols clearly demonstrated the formation of oligomers during ring‐opening reactions. MW, and odd and even carbon numbers in a structure of linear diols and branched diol used in the syntheses of PolyFAME polyols did not have an effect on crystallinity, glass transition, or melt temperatures measured using Differential scanning calorimetry (DSC). PolyFAME polyols ring‐opened with water, methanol, and 1,2‐propanediol contained secondary hydroxyl groups, whereas PolyFAME polyols ring‐opened with linear diols contained a mixture of primary and secondary hydroxyl groups. It was found that the concentration of primary hydroxyl groups increased significantly by increasing the number of carbons from C2 to C3 in the linear diols. The viscosity of PolyFAME polyols also increased with the MW of linear diols used in the E‐FAME ring‐opening reaction. These findings would be beneficial for formulators in choosing the most cost effective polyols for polyurethane formulations. 相似文献
86.
The present work discusses the combined effect of High Density Polyethylene Homo polymer and Styrene-Butadiene-Styrene on properties of Viscosity Grade 30 asphalt commonly used in India. Six blends of binders were prepared using varying percentages of both polymers and were evaluated for rheological properties. Use of both polymers leads to higher viscosity, while blending with HDPH polymer only leads to marginal increase in viscosity when compared to unmodified binder. Comparison of dynamic modulus and phase angle master curves indicated, significant differences were found among master curves obtained with different aging conditions when compared to unaged condition especially at lower reduced frequencies. 相似文献
87.
S Sailaja Devi M Radhakrishna Reddy P Sambasiva Reddy K Hussain Reddy K Mohana Raju 《Polymer International》2000,49(11):1338-1342
A series of polymer supported cobalt complexes have been synthesized by the reaction of Co(II)‐SALEN (salicylaldehyde ethylenediimine) and other variations thereof with the chelating resin containing vinyl pyridine. The polymer supported complexes have been characterized by electronic and infrared spectra. The presence of polymer supports has a marked influence on the UV–visible bands observed in the electronic spectra of cobalt complexes. These polymer supported complexes are also investigated by cyclic voltammetry. The electronic spectral data and cyclic voltammetric data for free complexes and polymer supported complexes are compared. The discernible differences in the spectral and electrochemical data suggest the presence of pentacoordinate cobalt in the polymer matrix. © 2000 Society of Chemical Industry 相似文献
88.
The polymer systems of vinyl latex, epoxy latex/resin, and phenol formaldehyde were used to modify sand-cement mortar at room temperature. The compressive strength increased with an increase of the latex/resin concentration, with the addition of CaCl2 or CaCO3, and with the addition of superplasticizer. Tensile and flexural strengths also increased with polymer incorporation. The porosity of the modified mortar decreased with the addition of resin. The percentage of water absorption and acid solubility were found to decrease for the latex/resin modified samples. © 1997 John Wiley & Sons, Inc. J Appl Polym Sci 63: 1251–1257, 1997 相似文献
89.
The biodegradability of low density polyethylene (LDPE)/starch and LDPE/starch/starch acetate (STAc) blends was tested and observed to be dependent on STAc content. The binary and ternary blends containing up to a maximum concentration of 30% starch were examined for their thermal, mechanical, and morphological properties. The blends with no STAc or 2.5% STAc show almost no adherence of two phases. With 10% STAc, dispersion of starch was observed to increase with some adherence to LDPE. Tensile strength, elongation at break, and Izod impact strength of the blends decreased with increased starch content. However, incorporation of STAc along with starch improved all these properties, particularly elongation at break and toughness. The melt flow index was also improved on partial substitution of starch by STAc. Maximum biodegradability was observed for the blends containing 30% (starch + STAc). Cell growth was observed to increase with increasing concentration of (starch + STAc) in the blends. © 1999 John Wiley & Sons, Inc. J Appl Polym Sci 74: 2791–2802, 1999 相似文献
90.
Suman Devi Prakash Korake S.N. Achary Narendra M. Gupta 《International Journal of Hydrogen Energy》2014
A series of CdS/Nix nanocomposite photocatalysts, containing ca. 0.6–15 wt% Ni, were synthesized using a one-step hydrothermal method and characterized for their crystallographic, morphological, interfacial, and optical properties. Rietveld refinement of powder XRD data revealed the coexistence of wurtzite (hexagonal) and zinc blende (cubic) phases of CdS in ratios dependent on Ni content. Only a fraction of Ni existed as a secondary phase of NiS while the majority occupied the lattice positions of hexagonal CdS. Whereas up to 10-fold enhancement in H2 evolution compared with pure CdS was observed for samples containing ∼1.5–4.5 wt% Ni, samples with smaller or larger Ni content displayed poor activity for visible-light-induced splitting of water in presence of sulfide–sulphite ions as sacrificial electron donors. In contrary to recent findings, our study reveals that the enhanced CdS photoactivity is not a result of charge transfer between p-type NiS and n-type CdS, Ni-induced visible-region absorbance, or the coating of CdS particles by non-photoactive NiS. Instead, the preparation-dependent hexagonal/cubic CdS phase boundaries and particle morphology may play a crucial role. Additionally, certain Ni-doping-induced sub-bandgap shallow energy levels contribute to charge carrier separation. 相似文献