Effect of orienting fields on agglomeration in dilute dispersions of magnetic fine particles

Static light scattering was used to investigate dilute dispersions of fine gamma -Fe/sub 2/O/sub 3/ magnetic particles. The particles were acicular and on average 0.39 mu m long and 0.056 mu m in diameter. They were dispersed in organic solvents at concentrations of approximately 10/sup -4/ vol%, corresponding to an average interparticle separation of 9 mu m. Computer programs using a coupled dipole algorithm to predict the scattering from the particles were written. Experimental results do not agree with computer calculations of the light scattering from single particles, but are consistent with scattering from thick ropelike agglomerates of particles. The size of these agglomerates was estimated after 10 s to be less than 100 particles, while the thickness of the ropes is at least 5 particles.<>     

Nonlinear static and dynamic analysis of circular plates and shallow spherical shells using the collocation method

The present work investigates the efficacy and applicability of interior global orthogonal point collocation method to the axisymmetric nonlinear analysis of elastic circular plates and shallow spherical shells subjected to uniformly distributed transverse load. Spacewise discretisation has been carried out using a polynomial expansion with the zeros of a Chebyshev polynomial as collocation points. Timewise integration has been carried out with Newmark k-β scheme corresponding to average acceleration method. The static response and snap-through buckling results, as well as, the dynamic response and dynamic buckling results under a uniformly distributed step load have been obtained and found to agree closely with the available results.     

An alternating technique for evaluating weight functions for 3-D surface flaws in finite solid bodies

An efficient method, based on the Schwarz–Neumann alternating technique, is presented for computing weight functions of a general solid (3-D as well as 2-D), with embedded or surface-flaw configurations. The total rate of change of the crack-opening displacements, due to simple perturbations of crack-dimension characteristics, is conveniently decomposed into the infinite-domain and boundary-correction parts. The former is determined from available analytical solutions of ideal-shaped cracks, whereas the latter is computed numerically by imposing nil boundary-traction requirements for the displacement field corresponding to the weight functions. Numerical examples, with solutions for 3-D weighted-average and local stress intensity factors, indicate that the proposed method is very accurate and efficient.     

Shear strength of lead,tin, copper,aluminum., corundum,and fluoroplastic-4 behind a shock wave

On the basis of the results of measurements in the pressure range 3.5–11 GPa for the shear strength of a number of shock-compressed substances carried out taking account of the completion of relaxation processes and establishment of pressure equilibrium the divergence is explained in results published previously for measurements of the dynamic yield point for highly ductile metals of the lead and tin type.Translated from Problemy Prochnosti, No. 10, pp. 50–54, October, 1991.     

ESD–RF co-design methodology for the state of the art RF-CMOS blocks

This paper describes an approach to design ESD protection for integrated low noise amplifier (LNA) circuits used in narrowband transceiver front-ends. The RF constraints on the implementation of ESD protection devices are relaxed by co-designing the RF and the ESD blocks, considering them as one single circuit to optimise. The method is applied for the design of 0.25 μm CMOS LNA. Circuit protection levels higher than 3 kV HBM stress are achieved using conventional highly capacitive ggNMOS snapback devices. The methodology can be extended to other RF-CMOS circuits requiring ESD protection by merging the ESD devices in the functionality of the corresponding matching blocks.     

Fluidized bed heat treatment of cast Al-Si-Cu-Mg alloys

The effects of fluidized bed heat treatment on the microstructural and mechanical properties of Al-Si-Cu-Mg cast alloys, namely, 354 and 319, were studied. The heating rate in fluidized beds (FBs) is greatervis-à-vis conventional electrical resistance furnaces (CFs). The high heating rate in FBs increases the kinetics of metallurgical phenomena such as Si fragmentation and spherodization during solution heat treatment, as well as the precipitation rate of phases such as Al₅Cu₂Mg₈Si₆ and Al₂Cu during aging. It is observed that the dissolution rate of phases such as Mg₂Si and Al₅Cu₂Mg₈Si₆ takes place very rapidly. The solution heat treatment of 319 alloy using FB results in complete dissolution of Mg₂Si and Al₅Cu₂Mg₈Si₆ particles within 45 minutes. However, for phases such as Al₂Cu and Ferich intermetallics, the dissolution rate is relatively slow. Even on prolonged solution heat treatment for 6 hours, these phases do not dissolve completely. It is observed that incomplete dissolution of the Al₂Cu phase does not significantly affect tensile properties of T4-treated alloys. The optimum solution heat-treatment time in FB for both 354 and 319 alloys is 45 minutes at 527 °C and 493 °C, respectively. Thermal analysis shows an exothermic peak owing to recrystallization and coarsening of eutectic grains during solution heat treatment. The high heating rate in FB causes this transformation to take place at a lower temperature than in CF. It is observed that the nucleation rate of Al₅Cu₂Mg₈Si₆ during aging in FB is greater than using CF. Thermal analysis of samples during the ramp-up stage while aging using FB did not show any phase transformation, while those using CF show two endothermic transformations, which are most likely due to the dissolution of GP zones or the co-cluster of solutes. Aging at 200 °C results in a greater number density of precipitates than those at 240 °C. The tensile strength of samples aged at 200 °C is greater than those aged at 240 °C, because the amount of precipitates formed at 200 °C is greater than that at 240 °C. The total heat-treatment time for T6 temper is less than 2 hours in FBs, which is a significant reduction in heat-treatment time, as well as energy consumption.     

Formation of ordered metal nanowire-inorganic salt composites

A new phenomenon accompanying the electrolysis of salts has been observed, whereby an ordered composite is formed under certain conditions (electrolyte composition, current density). The composite comprises an inorganic salt crystal penetrated by metal nano- and microwires. This phenomenon can serve as a basis for the technology of oriented and ordered nanowire array synthesis.     

A framework of virtual prototyping environment for the design and analysis of mechanical mechanism with clearance

Mechanical mechanisms with clearance abound in technological fields such as robotics, machine and steam turbine industry. The dynamic performance of these mechanisms in working condition can be achieved provided that the effects of the different on the mechanisms (such as mechanism dynamics, technological effects and thermal behaviour) are thoroughly understood. Virtual prototyping provides an integration of multi-domain dynamic simulation for the design and analysis process. In the current paper, a framework of virtual prototyping environment for the design and analysis of mechanical mechanism with clearance is presented. A case study with such a simulation strategy is studied for the optimum design and analysis of the technological parameter.     

On the possibility of development of defects in zirconium parts of thermal reactors during storage prior to and after operation

We have established that technological defects (cracks) in zirconium articles can develop in the course of long-term storage prior to their mounting in a reactor, which is caused by the action of residual stresses and hydrogen. We have considered the conditions of after-operation storage of zirconium articles of the fuel core of thermal reactors in water of the cooling ponds of reactors and in spent-fuel storehouses. The possibility of subsequent hydrogenation of these articles during their storage has been shown. Finally, we have studied the effect of hydrogen, absorbed in the course of storage, on the crack resistance of zirconium articles and the development of defects in them due to delayed hydride cracking. __________ Translated from Fizyko-Khimichna Mekhanika Materialiv, Vol. 43, No. 5, pp. 105–109, September–October, 2007.