振动功率流方法诊断梁的损伤

利用振动功率流方法对无限直梁在集中力作用下的损伤进行了诊断研究。损伤部位模拟为转动弹簧,利用断裂力学的有关理论得到其转动刚度。研究了梁在集中载荷作用下的弯曲波运动以及振动功率流的输入和传播,分析了振动功率流与破损位置及其特征尺寸的关系。首先从理论上研究了破损诊断的具体步骤,然后进行了实验研究,结果证明了理论分析的准确性和可靠性。     

煤与PVC共热解固体产物在燃烧中氯的释放特性

通过实验研究了煤与PVC共热解固体产物燃烧时氯的释放特性,结果表明,氯的释放量（率）与燃烧温度、煤与PVC共热解的温度以及共热解时PVC的加入量有关．燃烧温度越高,氯的释放率越大,900℃燃烧时,氯的释放率都在94％以上;热解温度越高。在同一温度燃烧时,氯的释放率越低．400℃时焦中氯的最高释放率达99．86％,而1000℃时焦中氯的最高释放率为94．35％．     

Contribution of extracellular polymeric substances from Shewanella sp. HRCR-1 biofilms to U(VI) immobilization

The goal of this study was to quantify the contribution of extracellular polymeric substances (EPS) to U(VI) immobilization by Shewanella sp. HRCR-1. Through comparison of U(VI) immobilization using cells with bound EPS (bEPS) and cells with minimal EPS, we show that (i) bEPS from Shewanella sp. HRCR-1 biofilms contribute significantly to U(VI) immobilization, especially at low initial U(VI) concentrations, through both sorption and reduction; (ii) bEPS can be considered a functional extension of the cells for U(VI) immobilization and they likely play more important roles at lower initial U(VI) concentrations; and (iii) the U(VI) reduction efficiency is dependent upon the initial U(VI) concentration and decreases at lower concentrations. To quantify the relative contributions of sorption and reduction to U(VI) immobilization by EPS fractions, we isolated loosely associated EPS (laEPS) and bEPS from Shewanella sp. HRCR-1 biofilms grown in a hollow fiber membrane biofilm reactor and tested their reactivity with U(VI). We found that, when reduced, the isolated cell-free EPS fractions could reduce U(VI). Polysaccharides in the EPS likely contributed to U(VI) sorption and dominated the reactivity of laEPS, while redox active components (e.g., outer membrane c-type cytochromes), especially in bEPS, possibly facilitated U(VI) reduction.     

水分胁迫条件下葡萄生理生化反应研究进展

从水分胁迫对葡萄叶、根的形态及气孔行为、光合作用、呼吸作用、质膜透性、氮代谢、碳水化合物代谢、活性氧代谢、内源激素变化等生理生化方面的研究进行了综述,为全面研究葡萄抗旱机理及进一步制定抗旱措施奠定理论基础.     

组成、粘度比及加工条件对PB／CS共混物粘度和形态的影响

研究了组成、粘度比、转速和混合时间对聚丁烯／玉米浆共混物的粘度和形态的影响。结果表明，共混物的粘度均随转速的提高而增大。在高转速下，８０／２０共混物的粘度比其它组成的共混物的粘度增长迅速。在聚丁烯和玉米浆的界面观察到复合乳化结构。分散相液滴尺寸较小时，液滴尺寸的变化对共混物的粘度有很大的影响。     

A π-extended tetrathiafulvene derivative: Synthesis and photoluminescence properties

Solid-state emissive organic materials have received increasing attention due to their prospective applications in large-area. Here, a novel π-extended tetrathiafulvene derivative DPD with donor-π-donor structure has been newly developed to produce the prominent characteristic of aggregation-induced enhanced emission (AIEE) that exhibits higher fluorescence quantum efficiency in solid film compare to its solutions. The AIEE mechanism of DPD was studied in detail through photophysical investigations and can be dominant attributed to the formed excimer state of DPD and J-aggregates in solid state.     

Correlation between structural and optical properties of 30 nm and 60 nm lead sulfide nanowires

PbS nanowires with 30 nm and 60 nm diameter fabricated under the same condition of electrochemical deposition with sulfuric and oxalic anodic alumina membranes (AAM), respectively, have been successfully prepared in order to study their optical properties in relation to their size. Scanning electron microscopy indicates that the 60 nm PbS nanowire arrays have the same shape with the 30 nm. X-ray diffraction result shows that 60 nm PbS nanowires are crystalline and have a highly (200) preferential orientation like 30 nm ones. UV spectrum considers the nanowire size decrease as the absorption peak shifts to the blue. The quantum confinement effects compared between 30 nm and 60 nm PbS nanowire arrays were observed by the measurements of ultraviolet-visible absorption spectroscopy (UV-vis).     

水中油分浓度分析仪新旧检定规程的比较

本文通过比较新旧规程,从规程适用范围、通用技术要求、计量器具控制、计量性能要求等解读其中的主要异常。