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71.
72.
Duringthelastdecade ,thedesignandsynthesisoftripodalligandsandtheirmetalcomplexeshaveattractedconsiderableattentionduetotheirpotentialusesaslumi nescentprobesinmedicineandbiochemistry[1~ 7] ,ascatalysts[8] andelectrochemicalmaterials[9] .However ,thecomplexesofrareearthmetalwithtripodalligandshavefewreported[10 ] .Asanextensionofourstudiesoncomplexesofmetalwithtripodalligands ,anewtripodalligand (tris { 2 [N (pyridine methanoyl)amino]ethyl}amine ,L)anditscomplexeswithrareearthnitratesweresyn… 相似文献
73.
74.
AK Tan 《Canadian Metallurgical Quarterly》1998,39(9):403-405
AIM OF STUDY: This study was done to examine the usefulness of botulinum toxin A injections in treating various neurological disorders such as hemifacial spasm, blepharospasm, focal dystonia and task-specific dystonia. METHODS: This was a prospective, open-labelled trial of patients seen in a Movement Disorders Clinic with dyskinesias potentially treatable with botulinum toxin. All patients were assessed before and after injections using clinical rating scales, and those with focal and task-specific dystonias were also recorded on videotape. RESULTS: There were 102 patients with hemifacial spasm, 3 with blepharospasm, 13 with neck dystonia, 6 with writer's cramp, I with musician's cramp, and I with jaw dystonia. All patients with hemifacial spasm and blepharospasm obtained good results, while 77% of those with cervical dystonia received substantial benefit. Only half of those with writer's cramp improved. Hemifacial spasm seems more prevalent in Singapore compared with Western populations. CONCLUSION: Injections of botulinum toxin are useful in treating the various neurological disorders studied. This is an advancement in the treatment of these dyskinesias which respond poorly to oral medications. 相似文献
75.
A new colour quantisation and quadtree based image compression scheme is proposed. The features of the new scheme are that colour palette ordering and requantisation of the decoded image for palette-based monitor displays are not required. Thus, fast decoding and displaying can be achieved 相似文献
76.
The preparation of a SiC coating on a carbon fiber surface using a sol-gel mixture of tetraethyl orthosilicat (TEOS) and phenolic resin was studied. FTIR and SEM investigations indicated that the SiC coating can be formed by carbothermal reduction of the sol-gel mixture at 1420°C for 15–20 min in an argon atmosphere. TGA of the coated fiber was also performed, showing that the SiC coating improves the thermooxidative stability of the carbon fiber. With the thickness of the obtained coating of 0.47 μm using a C/Si ratio of 4, this treatment does not affect the carbon fiber strength. 相似文献
77.
Y. Liu W. Zhu O. K. Tan X. Yao Y. Shen 《Journal of Materials Science: Materials in Electronics》1996,7(4):279-282
A low-temperature plasma-enhanced chemical vapour deposition (PECVD) technique has been employed to produce ultrafine tin oxide powders. The structural features and phase transition of this material have been characterized using differential thermal analysis (DTA), thermogravimetric analysis (TGA), X-ray diffraction, infrared spectroscopy (IR) and transmission electron microscopy (TEM). The oxygen absorption behaviour and gassensing properties have been investigated by electron paramagnetic resonance (EPR), X-ray photoelectron spectroscopy (XPS) and electrical measurements. Thick film gas sensors made from such ultrafine SnO2 powders yield better sensitivities than those of normal undoped SnO2 gas sensors. A gas-sensing reaction mechanism is also proposed. 相似文献
78.
Real-time accurate hand path tracking and joint trajectory planning for industrial robots (I) 总被引:1,自引:0,他引:1
Previously, researchers raised the accuracy for a robot’s hand to track a specified path in Cartesian space mainly through
increasing the number of knots on the path and the number of the path’s segments, which results in the heavier online computational
burden for the robot controller. Aiming at overcoming this drawback, the authors propose a new kind of real-time accurate
hand path tracking and joint trajectory planning method. Through selecting some extra knots on the specified hand path by
a certain rule and introducing a sinusoidal function to the joint displacement equation of each segment, this method can greatly
raise the path tracking accuracy of robot’s hand and does not change the number of the path’s segments. It also does not increase
markedly the computational burden of robot controller. The result of simulation indicates that this method is very effective,
and has important value in increasing the application of industrial robots.
Foundation item: Foundation of the Robotics Laboratory, Chinese Academy of Sciences (No. RL200002)
Biography of the first author: TAN Guan-zheng, Dr., professor, born in Oct. 1962, majoring in artificial intelligence, robotics and automation. 相似文献
79.
80.
Lu Shen Beng Jit Tan William S. Willis Francis S. Galasso Steven L. Suib 《Journal of the American Ceramic Society》1994,77(4):1011-1016
Amorphous boron nitride thin coatings (∼0.2 μm) have been formed on Nicalon and C-Nicaion (pre-carbon-coated Nicalon) yarns via dip coating in boric acid solution followed by heating and nitriding in NH3 gas at 1000°C. X-ray photoelectron spectroscopy (XPS) and Auger electron spec-troscopy (AES) studies have shown the formation of boron nitride. The coating was boron rich and contains oxygen. The N/B and O/B ratios range from 0.6 to 0.8 and from 0.1 to 0.25, respectively. Tensile strength measurements revealed that the BN-coated C-Nicalon yarn maintained ∼85% of its original strength while BN-coated Nicalon lost ∼85% of its original strength. Auger depth profiles showed that there was a consumption of carbon during the heating and nitridation process for both BN-coated Nicalon and C-Nicalon fibers. However, the depletion of carbon in BN-coated Nicalon fibers was much more severe than that in BN-coated C-Nicalon fibers. 相似文献