硝酸溶液中钼和锆溶解度的测定

一、前言在核裂变过程中,钼和锆是高产额的裂变产物元素,所以在乏燃料中钼和锆的含量较高。核燃料水法后处理工艺的常用介质是硝酸,因此测定硝酸溶液中钼和锆的溶解度是有意义的。对于裂变产物的过程化学的研究工作,溶解度数据也是必要的。关于硝酸溶液中钼和锆的溶解度,前人研究得很少,数据也不全。为此,我们测定了不同浓度的硝酸中不同温度下钼和锆溶解度;还观测了硝酸根和铀浓度对钼和锆的溶解度的影响;获取的数据较全面。     

含氚废水水泥固化实验研究

研究用水泥固化处理氚废水,并选择了最佳配方:水与灰的重量比=0.45～0.5,水泥与石膏重量比=5∶1。用IAEA推荐的方法做浸出实验。为了减少水泥固化体中氚的浸出量,实验了几种涂层材料。沥青涂层可将固化体氚的浸出率降低1～2个量级。     

原子高离化态研究装置

介绍了原子高离化态研究装置,包括重离子加速器、测量装置、数据获取和处理系统。     

碾压混凝土坝施工进度与质量控制的新措施

碾压混凝土重力坝和拱坝由于连续施工的坝体混凝土体积大，施工期间需要采取较为严格的温度控制措施，而所采取的温控措施是否有效，目前尚没有一个能够用于实际施工过程的快速有效的评估方法和方式，不能根据已施工坝体内的实际情况来控制施工进度和质量。利用分布式光纤温度测量系统来快速地获得坝体混凝土内部的大量温度信息，进而实际标定温度仿真程序并通过标定过程模拟拟施工的连续碾压层，以检验其温控措施的有效性。通过坝体内部的温度、温度变化速率和梯度来达到实时控制坝体碾压上升速度、坝面和仓面养护、以及冷缝灌浆处理等目的。     

用边界元法提取VLSI版图电阻

介绍了ＶＬＳＩ版图验证中电阻提取的基本原理和主要方法，给出了一种新颖的基于边界元法的电阻提取算法。该算法采用变节点单元，较好地解决了实际问题中经常出现的角点问题。通过应用该算法对几个实例进行提取，证明使用本文的算法不仅在精度上而且在占用ＣＰＵ时间上都取得了令人满意的效果     

1μm宽硅深槽刻蚀技术

介绍了硅深槽刻蚀的基本原理和影响刻蚀效果的几个主要工艺因素。提出了一种实现１μｍ宽的硅深槽刻蚀工艺途径；并给出了１μｍ宽、８μｍ深、侧壁及底部光洁的硅深槽刻蚀工艺条件。     

全耗尽CMOS／SOI技术的研究进展

ＳＯＩ材料技术的成熟，为功耗低，抗干扰能力强，集成度高，速度快的ＣＭＯＳ／ＳＯＩ器件的研制提供了条件，分析比较了ＣＭＯＳ／ＳＯＩ器件与体硅器件的差异，介绍了国外薄膜全耗尽ＳＯＩ技术的发展和北京大学微电子所的研究成果。     

Selective monitoring of peptidase activities with synthetic polypeptide substrates and polyion-sensitive membrane electrode detection

A novel method to monitor specific peptidase activities in biological samples as complex as undiluted plasma/blood is described. The approach is based on the design of synthetic polypeptide substrates in which di- or triarginine sequences are linked to each other via one or more other amino acids recognized specifically by the peptidase to be determined. Detection of chymotrypsin and renin activities using synthetic substrates P4 (F-R-R-R-F-V-R-R-F-NH2) and P5 (R-R-R-L-L-R-R-L-L-R-R-R), respectively, serves to demonstrate the principles of this new assay system. A polyion-sensitive membrane electrode, prepared by doping polymer films with dinonylnaphthalene-sulfonate (DNNS), is shown to exhibit significant nonequilibrium electromotive force (EMF) responses toward these and other polycationic substrates at microgram/milliliter levels under physiological conditions. The same electrode, however, exhibits much smaller total EMF response toward the shorter fragments of the synthetic peptides generated by peptidase activity; hence, the addition of peptidase to a solution containing the synthetic substrate yields a change in electrode EMF response, the rate of which is proportional to the activity of peptidase present. Other synthetic polycationic peptides as well as natural polycationic peptides (e.g., protamine) that lack specific cleavage sites for chymotrypsin and renin, yet are detected by the DNNS-based membrane electrode, do not elicit any significant change in EMF response in the presence of the peptidases, confirming the feasibility and utility of the proposed bioanalytical method.     

Microstructure of Pd_(77.5)Au_6Si_(16.5) Alloy Droplet Solidified in a Drop Tube Process

The microstructure development of Pd77.5Au6Si16.5 alloy droplet solidified in a drop tube process was studied. It was found that two distinct microstructures, i.e. (Pd,Au)3Si primary phase and Pd+(Pd,Au)3Si eutectic can be obtained when the droplet diameter is within the range between 2.3~0.4 mm. The morpologies of the (Pd,Au)3Si developed from dendrite trunk-like with single branching only into dendrite cluster-like with ternary branching with the decrease of the droplet diameter. When the droplet diameter is about 0.25 mm, the primary phase (Pd,Au)3Si almost disappears and the microstructure mainly shows Pd+(Pd,Au)3Si eutectic. The morphology of the eutectic transforms from fiber-like to plate-like with the decrease of the droplet diameter in the range between 2.3-0.25 mm. When the droplet diameter is about 0.19 mm, the microstructure is only the single phase of Pd solid solution     

CAD^2B—一个计算机辅助数据库设计系统

本文介绍了一个用Ｔｕｒｂｏ Ｃ语言在ＡＳＴ－２８６机器上实现的计算机辅助数据库设计系统ＣＡＤ＾２Ｂ。该系统提供了人机交互的环境，供设计者进行概念模型设计，并自动完成从概念模型逻辑模型的映射，创建满足规范化要求的关系表。该系统采用的概念模型是引入了事件和时间的扩展了的实体关系模型。该模型既能充分反映应用环境的静态和动态语义，又是向关系模式转化的基础。