Effects of added Cd on Cd uptake by oilseed rape and pai-tsai co-cropping

The experiment was designed to study whether the decrease of Cd in the rhizosphere of Zhongyouza Ⅰ,one breed of oilseed rapes （Brassicajunica） that can hyperaccumulate cadmium from the soil, can improve the living condition of less Cd-tolerant plant pai-tsai （Brassia chinensis） with their roots permitted to intermingle and develop coincident rhizosphere. The extent of rhizosphere interactions between Zhongyouza Ⅰ and pai-tsai was controlled by different root barriers, or without barrier. The results show that in the 10 and 20 mg/kg Cd treated soils, pai-tsai gets higher shoot mass and less Cd accumulation in its shoot than in the barrier treatments or in the mono cultures, when its roots are permitted to intermingle with those of Zhongyouza Ⅰ. Meanwhile, soil decontamination rates of Zhongyouza Ⅰ are not affected much by co-cropping with pai-tsai, they are 80.0% and 91.8% of that in the mono cultures of Zhongyouza Ⅰ, respectively. However, the co-cropping method in meliorating the living condition of pai-tsai is not obvious when Cd concentration in soil reaches 40 mg/kg, and soil decontamination rate decreases to 0.14, which is 58.3% of that in the mono culture. These results indicate that the oilseed rape Zhongyouza Ⅰ may alleviate Cd toxicity of surrounding less-tolerant species, and its ability of phytoremediation is not affected much at the same time, especially in the middle polluted soil.     

凝胶燃烧法合成LiCoO2超细粉体的研究

以LiNO3和Co(NO3)2@6H2O为原料,柠檬酸为燃料.采用凝胶低温燃烧技术合成了LiCoO2超细粉体.并利用各种分析技术对柠檬酸和硝酸盐形成的凝胶及凝胶燃烧合成的粉体进行了研究柠檬酸硝酸盐凝胶在350-400℃之间发生燃烧反应,得到黑色疏松粉体X射线衍射分析表明.适当提高柠檬酸在凝胶中的含量.燃烧后得到的粉体晶粒尺寸显著减小未经燃烧的粉体中除含有LiCoO2外.还有CoO,Li2CO3等杂质相.但在450℃下经短时间煅烧后.杂质相消失,其晶相为层状岩盐结构的高温LiCoO2相扫描电镜和透射电镜观察发现.随着煅烧温度的提高.LiCoO2粉体的粒径有所增大.但远小于在相同煅烧条件下用固相反应法制备的LiCoO2粉体.这表明采用燃烧法更适于合成具有单一相结构的,可在低温条件下烧结的超细LiCoO2粉体.     

用局部法评定焊接接头的疲劳性能

采用16Mn钢非承载十字焊接接头疲劳试验结果对使用Dang Van准则的疲劳评定局部方法进行了研究。结果表明，有限元分析中应力集中区单元尺寸对局部参量计算有明显影响，为获得比较合理的预测结果需对焊趾应力集中区所划分的单元尺寸限定，当接头焊趾半径在0．15-0．8mm变化时应选择最小单元尺寸0．32-0．62mm计算局部参量；在此基础上Dang Van准则可以对焊态接头做出合理的评定，但Dang Van建议的卢值偏安全。此外，通过计算发现焊趾半径只影响局部很小区域(约0．5mm内)的应力集中分布，在某一深度(约0．5mm)后存在稳定的应力集中，因而建议采用距应力集中区最大应力处某一深度的应力参数计算Dang Van局部参量可能更为合理，这将减小局部参数对焊趾半径及单元尺寸的依赖性。     

Site occupations and ordering behaviour of O phase in Ti2AlNb—based intermetallics

1　ＩＮＴＲＯＤＵＣＴＩＯＮＴｈｅｏｒｔｈｏｒｈｏｍｂｉｃａｌｌｏｙｓａｒｅｏｆｇｒｅａｔｔｅｃｈ ｎｏｌｏｇ ｉｃａｌｉｎｔｅｒｅｓｔｉｎｈｉｇｈｔｅｍｐｅｒａｔｕｒｅａｐｐｌｉｃａｔｉｏｎｓｓｉｎｃｅｔｈｅｙｈａｖｅａｇｏｏｄｂａｌａｎｃｅａｍｏｎｇｓｔ     

Continuous electromagnetic separation of inclusion from aluminum melt using alternating current

A novel scheme about the continuous electromagnetic purification of aluminum melt was put forward based on the utilization of a square separation pipe and a 50 Hz alternating current to produce electromagnetic force. It is experimentally found that with electrical current of 400 A/cm^2, it takes only 10 s to remove 95% inclusion from aluminum melt. Comprehensive numerical simulations were carried out to investigate the dynamics mechanisms behind the process. The results show that the removal of inclusion is attributed to the cooperative effects of electromagnetic buoyancy and the secondary flow induced by the rotational electromagnetic force, and the removal efficient increases with the size of inclusion and the electrical current imposed. Theoretical predictions on the distribution and removal efficiency of inclusion were supported by the experiments.     

压缩弧光等离子束熔覆层中晶相与非晶相

用压缩弧光等离子束在 45钢表面熔覆Fe Cr Si B粉末涂层 ,采用能谱、透射电镜、电子探针对熔覆层结构进行分析。结果表明 ,熔覆层中晶相与非晶相并存 ,晶相由A(Me)、F(Me)、Me2 3 C6 等相组成 ,且 [2 11]A∥ [2 11]Me2 3 C6 ,(111) A ∥ (111) Me2 3 C6 ,(0 11) A ∥ (0 11) Me2 3 C6 ,即A与Me2 3 C6 保持共格关系 ,而[111]F∥ [32 1]Me2 3 C6 ,(10 1) F∥ (111) Me2 3 C6 。非晶相中Si、Cr等元素含量较高 ,从动力学和热力学两方面对非晶的形成进行了分析     

冶金固废材料化利用的研究进展

冶金固体废弃物的材料化利用能充分发挥二次资源的资源禀赋,提升附加值,不仅是冶金固废大宗量低附加值利用途径的有效补充,而且为材料制备提供了低成本、可持续的新方法.着重阐述了冶金固废中钢渣、高炉渣、高炉尘、电炉尘等的材料化利用研究现状,并对其发展前景进行了展望.     

制药工程专业"化工原理"课程教学改革探索

作为制药工程的专业核心课,"化工原理"是一门重要的基础学科.以培养现代化的创新制药工程技术人才为目标,从教学内容、教学方法和评价手段三个方面进行教学改革的探讨,使学生能用工程观念分析、解决工程实际问题,从而提高学生的综合素质与创新能力,满足社会对制药工程专业综合性人才的需要.     

太赫兹信号在老化硅橡胶中的传播特性仿真研究

绝缘是影响电力系统稳定运行的重要因素,但大多数情况下电气设备很难拆卸,对其绝缘老化程度的检测较为困难.太赫兹波具有可以轻易穿透绝缘材料等非金属材料的特性,这对于硅橡胶复合绝缘子的无损检测具有重要意义.分析了太赫兹信号在理想介质与有损介质中传播的特性,从理论上阐述了其在非理想材料中可能发生的损耗,进而指出可以通过检测太赫兹回波损耗变化来反映硅橡胶介电常数的变化及其老化程度.之后在CST仿真软件上搭建仿真模型,改变材料的相对介电常数以及太赫兹信号的频率,研究其对回波损耗造成的影响,最后得出的结论可以更有效率地指导实际实验的进行.     

输电线路引流板螺栓拧紧工艺的研究

超高压输电线路中常出现耐张线夹引流板因螺栓松动而引起发热的现象.螺栓松动除了受风振影响外,与其安装工艺也紧密相关.检修中发现有些螺栓松脱是因安装扭矩不合适而造成的.本文通过引流板螺栓安装扭矩的设计计算,结合扭矩-预紧力特性试验,对引流板螺栓的扭矩值和拧紧工艺进行了研究.