用季铵盐催化剂合成羧甲基淀粉钠的研究

采用季铵盐作催化剂，使氯乙酸的醇溶液与淀粉钠进行羧甲基化反应，合成了取代度高于相应常规法的羧甲基淀粉钠产品。     

时变可靠性约束下含风电系统旋转备用的随机规划模型

大规模风电并网后,系统运行经济性和可靠性之间的矛盾十分突出,传统确定旋转备用的方法存在较大的局限性。建立的含风系统旋转备用随机规划模型,能够根据系统容量冗余度,灵活分配各时段可靠性权重,实现调度周期内可靠性的协调优化。该模型充分考虑不同机组提供旋转备用的成本差异,允许机组对旋转备用进行报价,以发电成本、直接备用成本和期望停电成本三者之和最小为目标,实现发电侧和用户侧整体经济效益的最大化。应用该模型,可以对含风系统的旋转备用进行成本效益分析,为调度机构设置合理的可靠性水平提供决策依据。采用粒子群算法对模型进行求解,并通过算例分析验证了上述模型和算法的有效性。     

Comparative experimental study on reactive crystallization of Ni(OH)2 in an airlift-loop reactor and a stirred reactor

The objective of this work is to study the reactive crystallization in an airlift-loop reactor (ALR) using the precipitation of Ni(OH)2 as a model reaction.The growth of Ni(OH)2 particles in an ALR and a stirred tank was quantified by scanning electronic microscope (SEM),X-ray diffraction (XRD),laser particle analyzer,tap densitometer and optical microscope,and the growth process of Ni(OH)2 particles is analyzed.It is found that the Ni(OH)2 particles prepared in an ALR have a better sphericity than those in a stirred tank and the growth of Ni(OH)2 particle tap density mainly depends on the size of crystallites:the bigger the size of crystallites,the bigger the tap density is.Based on these,the growth process of Ni(OH)2 particles in ALR is elaborated.Crystallites precipitated from solution aggregate to form large particles with much void.These constituting crystallites continue to grow up,that takes up the void inside particles and makes the tap density increase.     

入侵检测系统脆弱性研究

随着入侵检测系统(IDS)技术的逐步发展与成熟,其自身的脆弱性也逐渐成为人们的研究重点之一。本文首先对入侵检测系统进行了简要介绍,强调了IDS 自身安全的重要性,然后从五个方面对IDS的脆弱性进行了分析和研究。     

Synthesis and characterization of biodegradable copolymers based on 6-aminocaproic acid and α-L-alanine

Random copolymers based on 6-aminocaproic acid and α-L-alanine were prepared by melt phase polycondensation method and characterized by FTIR, ¹H NMR, DSC and WAXD. The density, water absorptivity and enzymatic degradation of copolymers were measured. The results show that with increasing of alanine content in comonomers, the density, water absorptivity and rate of enzymatic degradation of copolymers increase, but the intrinsic viscosity and the degree of crystallization decrease. When the molar percentage of alanine increases to 40% in comonomers, copolymer is amorphous.     

电力谐波实验台研究与设计

电力谐波实验台是一种通过模拟实际电网中产生的谐波电流并对其进行实时抑制的实验装置。该实验装置采用公共基础台+功能挂件的设计方式,结构紧凑,集成度高,扩展性好,能够完成电力谐波的产生、在线检测、分析、有源滤波等多项实验。装置软件实现由DSP控制器和上位机两部分组成。DSP控制器采用自适应滤波理论的单神经元电力谐波动态检测算法和滞环控制算法实现系统的补偿。上位机负责计量、监测、显示、储存等功能,是实验装置虚拟仪器的核心部分。该装置系统具有较高的教学使用和科研价值。     

线粒体DNA减少在氡及其子体致人支气管上皮细胞凋亡中的作用

使用溴化乙锭(Ethidium bromide,EtBr)诱导方法构建线粒体数目减少支气管上皮细胞(Human bronchia epithelia with mitochondrial DNA knock-down,ρ?HBE)模型并进行长期氡照射,用克隆形成法测定氡照射后HBE细胞的增殖能力,用流式细胞仪进行细胞凋亡和线粒体膜电位的检测。结果发现,氡照射后,与线粒体DNA数量正常的HBE细胞(ρ+HBE)相比较,ρ?HBE细胞存活分数明显增高,虽然早期凋亡率明显低于正常细胞,但是总凋亡率增加,同时线粒体膜电位也显著降低。结果提示,氡照射后引起的线粒体减少HBE细胞增殖能力提高与总凋亡率的减少有关,并且与线粒体膜电位的变化相关。     

Engineering Smart Nanofluidic Systems for Artificial Ion Channels and Ion Pumps: From Single-Pore to Multichannel Membranes

Biological ion channels and ion pumps with intricate ion transport functions widely exist in living organisms and play irreplaceable roles in almost all physiological functions. Nanofluidics provides exciting opportunities to mimic these working processes, which not only helps understand ion transport in biological systems but also paves the way for the applications of artificial devices in many valuable areas. Recent progress in the engineering of smart nanofluidic systems for artificial ion channels and ion pumps is summarized. The artificial systems range from chemically and structurally diverse lipid-membrane-based nanopores to robust and scalable solid-state nanopores. A generic strategy of gate location design is proposed. The single-pore-based platform concept can be rationally extended into multichannel membrane systems and shows unprecedented potential in many application areas, such as single-molecule analysis, smart mass delivery, and energy conversion. Finally, some present underpinning issues that need to be addressed are discussed.     

Ⅴ级黄土隧道施工控制要点

中国黄土地域分布较广,黄土面积约占我国陆地面积的6.6%,黄土隧道施工的建设无法避免,其施工难度与设计也相对复杂。文章从黄土隧道施工方法、现场管理控制等方面提出了一些建议及施工工艺。