D301树脂分离衣康酸的工艺研究

采用弱碱性阴离子交换树脂Ｄ３０１对发酵法生产的衣康酸进行了分离研究。通过静态交换实验，研究了Ｄ３０１树脂对衣康酸的静态交换动力学，确定了传质机制和影响因素；通过动态交换实验，研究了以硫酸为洗脱剂，以氨水为再生剂的工艺过程，确定了主要工艺参数。     

钛酸钾品须填充UHMWPE复合材料的摩擦磨损性能研究

用钛酸钾晶须(PTW)对超高摩尔质量聚乙烯(UHMWPE)进行填充改性,考察了复合材料的摩擦磨损性能,研究了其结晶情况,观察了磨损表面形貌并分析了其机理.结果表明随着PTW用量的增加,复合材料的硬度、结晶度以及维卡软化点都有所增大.PTW提高了复合材料的耐磨性,但摩擦系数有所上升.PTW的加入使得UHMWPE的磨损机理从黏着磨损和塑性变形改变成疲劳磨损和轻微的塑性变形,提高了其抗磨粒磨损的性能.     

基于自由运动一维标定物的多摄像机参数标定方法与实验

一维标定方法易于实现且标定效率高,为了克服现有一维标定方法的一些不足,本文提出一种用一维标定物标定多摄像机内外参数的方法,首先进行两两标定,在此过程中,假定主点坐标近似已知而仅考虑畸变、焦距、旋转和平移等参数,接着利用基本矩阵及一维标定物上特征点之间的几何约束,估计两摄像机的内外参数,两两标定完成后,采用Dijkstra最短路径法和捆绑调整对多摄像机系统进行全局标定(含主点坐标),仿真和真实实验表明本文的方法是切实有效的.     

A simplified method for analyzing mold filling dynamics. Part II: Extensions and comparisons with experiment

A dimensional analysis based on four parameters has been developed previously to predict injection pressure; clamp force, and bulk temperature for the injection molding of amorphous materials in center-gated disk-shaped cavities. In this paper geometric and semicrystalline-materials approximations are introduced and tested for extending the previous analysis to include multigated thin cavities and semicrystalline materials. The combination of these approximations and the previous analysis, known hereafter as the Radial Flow Method (RFM), greatly simplifies the analysis of mold filling. The geometric approximation, which is based on a simple model for the axial stress distribution in the cavity, is shown to give reasonable predictions when compared with experimental data and a numerical two-directional flow simulation for the filling of an off-center-gated rectangular cavity with acrylonitrilebutadiene-styrene copolymer (ABS). The semicrystallinematerials approximation, in which heat capacity and viscosity changes during crystallization are neglected, is shown to give good agreement with experimental data for the filling of a center-gated disk-shaped cavity with polypropylene. As an illustration, the Radial Flow Method is used to analyze the molding of a large, thin-wall automobile interior trim panel. The inlet melt temperature, mold-wall temperature, part thickness, injection rate, viscosity and gate locations are varied in a series of calculations to determine the relative effectiveness of these variables in lowering the injection pressure and Clamp force. The results obtained with the Radial Flow Method are in good agreement with those obtained by a finiteelement simulation of two-directional flow.     

小型连锁超市优惠券管理系统的开发

本系统适用于小型连锁超市,主要是从总体上对其优惠券进行管理。本系统具有优惠券类别管理、优惠券规则定义、优惠券发放管理、优惠券使用管理、优惠券查询、优惠券统计、会员优惠券管理等功能。本系统界面友好、直观,操作简便,系统中的多级权限管理等也可以保证数据的安全可靠。     

基于ExtJS+SSH架构的民政服务信息系统设计与实现

针对传统民政办公系统结构复杂,不易维护和不易扩展的情况,提出了一种基于Ext JS+SSH(Struts2、Spring和Hibernate)架构的民政服务信息系统。按照Java EE的分层思想,通过Struts2框架实现了MVC模式,将用户界面、业务处理和数据访问三者分离,利用Spring框架统一管理系统对象以降低系统的耦合性,采用Hibernate框架实现业务数据的持久化以降低开发难度。实验结果表明,基于Ext JS和SSH架构的系统具有易维护、可扩展和运行稳定的特性。     

Effects of the reinforcement and toughening of acrylate resin/CaCO3 nanoparticles on rigid poly(vinyl chloride)

Novel composite particles based on nanoscale calcium carbonate (nano‐CaCO₃) as the core and polyacrylates as the shell were first synthesized by in situ encapsulating emulsion polymerization in the presence of the fresh slush pulp of calcium carbonate (CaCO₃) nanoparticles. Subsequently, these modified nanoparticles were compounded with rigid poly(vinyl chloride) (RPVC) to prepare RPVC/CaCO₃ nanocomposites. At the same time, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were investigated, and the synergistic effect of modified nanoparticles with chlorinated polyethylene (CPE) was also studied. The results showed that in the presence of nano‐CaCO₃ particles, the in situ emulsion polymerization of acrylates was carried out smoothly, and polyacrylates successfully encapsulated on the surface of nano‐CaCO₃ to prepare the modified nanoparticles, breaking down nano‐CaCO₃ particle agglomerates, improving their dispersion in the matrix, and also increasing the particle–matrix interfacial adhesion. Thus, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were very significant, and the cooperative effect of the nanoparticles with CPE occurred in the united modification system. Scanning electron microscopy analyses indicated that large‐fiber drawing and network morphologies coexisted in the system of joint modification of nanoparticles with CPE. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 3940–3949, 2007     

基于专家主观信息的学术期刊评价方法研究

该文侧重于学术期刊定性属性的评价方法研究。学术期刊定性属性特征通常具有模糊性,因而往往需要由专家给出主观判断。通过建立基准语言等级评价集合,提出了将专家给出的关于各定性属性的主观评价信息规范化为基准语言等级评价集合并集成的综合评价方法。最后通过计算可以得到学术期刊的综合评价值,进而使得学术期刊评价尽可能的公平化。     

基于模糊层次分析法的应用性技术成果评价

针对现有应用性技术成果的评价指标体系,建立了相应的模糊层次分析法数学模型,此模型可克服传统层次分析法判断矩阵构造主观性强和一致性不易检验等缺点,为应用性技术成果的等级评价提供了一种简便合理的科学评价方法.