Manufacture of carbon fibers from polyacrylonitrile precursors treated with CoSO4

Free‐radical solution copolymerization of itaconic acid and acrylonitrile was carried out in DMSO using azodiisobutyronitrile as an initiator, changing the feed rate of itaconic acid. The resulting polymerization solution was spun to form polyacrylonitrile (PAN) precursors of carbon fibers. The precursors were treated with a CoSO₄ aqueous solution on‐line. The structure and properties of untreated and treated PAN precursors and the resultant carbon fibers were characterized by SEM and TEM, a stabilization process, etc. It is suggested that CoSO₄ acts as a catalyst in the formation of a ladder structure and reduces the temperature of cyclization, and the carbon fibers developed from treated PAN fibers showed improvement in the tensile strength and the Young's modulus. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 153–158, 2002     

Multiresolution analysis in extraction of reference lines fromdocuments with gray level background

Based on wavelets, a theoretical method has been developed to process multi-gray level documents. In this method, two-dimensional multiresolution analysis, a wavelet decomposition algorithm, and compactly supported orthonormal wavelets are used to transform a document image into sub-images. According to these sub-images, the reference lines of a multi-gray level document can be extracted, and knowledge about the geometric structure of the document can be acquired. Particularly, this approach is more efficient to process form documents with gray level background. Experiments indicate that this new method can be applied to process documents with promising results     

四方向上的任意角度扇形数字滤波器的设计

具有任意角度（扇形所围成的角度）和任意方向（扇形所取方向）的扇形数字滤波器在图像数据压缩和地质、地震等方面的数据处理中有着广泛的应用。目前，大多数的工作多集中于水平及垂直方向的９０°扇形数字滤波器的设计，因而有必要研究任意方向上的任意角度的扇形数字滤波器的设计。本文介绍利用ＭｃＣｌｅｌｌａｎ交换法设计具有垂直，水平及±４５°方向上的任意角度的扇形数字滤波器的设计方法，垂直水平方向上的扇形滤波器的设     

用于重离子核反应实验测量的纵向电场气体电离室

本文报道了一种新型的大动态范围，多叠层探测器系统组件之一的纵向电场气体电离室的构造，性能和在中能得离子核反应实验中的应用。     

同轴型光电器件的研究开发

本文简要地介绍了武汉电信器件公司正在研究开发的同轴型光电器件，新的器件的工艺与结构特点以及主要技术指标、使用前景。     

济钢中板工艺技术结构的优化

济南钢铁厂于１９８８年进行了增建４辊精轧机和增设３号加热炉为主体的中板工艺技术改造，在生产中对原料生产、中板轧制、精整等工艺技术结构进行了一系列优化组合，取得了良好的效果。为了适应市场需求将继续对中板进行工艺技术结构优化，调整产品结构。     

金刚石薄膜制备和评价

采用平直钨丝作热解源,并借助钨丝支架的弹性恢复力,较好地解决了热丝热解化学气相沉积法(HFCVD)合成金刚石过程中热解丝的变形问题.样品独立加热,基片温度、钨丝温度、钨丝与样品基片距离均可独立调节.装置改进后,在Si(100)上合成了面积大约45mm×25mm的比较均匀的金刚石膜.用扫描电子显微镜(SEM)、Raman光谱和X射线衍射仪对制备的金刚石膜进行了分析.     

一种有效的振动信号分离算法

振动信号包含随机成分与周期成分 ,其中的随机成分占据了很宽的频域 ,其能量极易引起其它设备特别是电子设备的共振 ,从而导致设备失效。为评估随机成分对设备的影响 ,需要将周期成分从振动信号中去除。为此 ,首先使用ARMA建模法对振动信号中周期成分出现的频率位置进行估计 ,然后设计阻带带宽极窄 (小于 0 .5Hz)的V型滤波器来完成相应的滤波。实验表明本文中的方法能有效地去除振动信号中的周期成分 ,而完整地保留随机成分     

改性玻纤增强尼龙610,1010塑料

研究了采用(准)中粘度级尼龙做基体树脂,加入成核剂改善尼龙的结晶过程,提高结晶速率和初始熔融温度;添加光、热氧稳定剂,防止尼龙在成型加工和使用过程中产生降解与老化,提高塑料制品的质量和减少性能的分散性;采用合理的工艺条件,确保添加剂的均匀分散与减少玻纤的磨损,得到适于军工、航空和机电等领域需要的高性能的受力结构工程塑料。     

Retarded coarsening phenomenon of γ′ particles in Ni-based alloy

An anomalous coarsening behavior has been observed after aging an alloy Ni-14.5 at .%Al-5.9 at. % Mo at 1453 K. It was found that the initial cubic γ′ (ordered Ll₂ Ni₃Al phase) particles began to split into smaller ones after short aging (t < 3 min). After continued aging, the particles agglomerated into large groups of many particles, and the distribution of the particles became non-uniform. The kinetics of coarsening did not obey the typical linear dependence between the cube of the particle size and aging time. Instead, a retardation of the coarsening process was found. Convergent beam electron diffraction (CBED) was applied to measure the distribution of the lattice strains around particles. The result indicated that there was an inhomogeneous distribution of lattice strain in the matrix around the coherent particles.